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Polyurethane shape memory polymer: structure characterization and estimation of energy storage and dissipation during the tension process

Staszczak Maria, Gradys Arkadiusz, Golasiński Karol, Pieczyska Elżbieta A.

Bulletin of the Polish Academy of Sciences. Technical Sciences

2023

Vol. 71, nr 6

art. no. e147343

Shape memory polymers (SMP) are new multifunctional materials raising increasing interest in various functional applications. Among them, polyurethane shape memory polymers (PU-SMP) are particularly attractive due to their combination of shape memory, high strength and biocompatible properties. Developing new applications for PU-SMP requires comprehensive research on their characteristics. This work involved investigating the structure and mechanical behavior as well as characterizing the energy storage and dissipation of a thermoplastic PU-SMP with a glass transition temperature (Tg) of 25_C during tensile loading-unloading. The process of energy storage and dissipation in the PU-SMP was investigated based on the stress-strain curves recorded by a quasi-static testing machine and the temperature changes, accompanying the deformation process, obtained by using a fast and sensitive infrared camera. The results showed that the thermomechanical behavior of the examined PU-SMP depends significantly on the strain rate. At a higher strain rate, there are higher stress and related temperature changes, which lead to greater energy dissipation. However, the energy storage values estimated during the deformation process turned out to be not significant, indicating that the work supplied to the PU-SMP structure during loading is mainly converted into heat. It should also be noted that the structural investigation revealed no crystalline phase in the investigated PU-SMP.

Investigation of strain rate sensitivity of Gum Metal under tension using digital image correlation

Golasiński Karol, Pieczyska Elżbieta, Maj Michał, Staszczak Maria, Świec Paweł, Furuta Tadahiko, Kuramoto Shigeru

Archives of Civil and Mechanical Engineering

2020

Vol. 20, no. 2

339--352

Mechanical behavior of a multifunctional titanium alloy Gum Metal was investigated by conducting tensile tests at various strain rates and applying digital image correlation (DIC) technique. Stress–strain curves confirmed low Young’s modulus and high strength of the alloy. The determined values of yield strength had a tendency to increase, whereas the elongation to the specimen rupture tended to decrease with increasing strain rate. True stress versus strain curves were analyzed using selected lengths of virtual extensometer (VE) placed in the strain localization area. When the initial length of the VE was the same as the gauge length, work hardening was observed macroscopically at lower strain rates, and a softening was seen at higher strain rates. However, the softening effect was not observed at the shorter VE lengths. Evolution of the Hencky strain and rate of deformation tensor component fields were analyzed for various strain rates at selected stages of Gum Metal load-ing. The DIC analysis demonstrated that for lower strain rates the deformation is macroscopically uniform up to the higher average Hencky strains, whereas for higher strain rates the strain localization occurs at the lower average Hencky strains of the deformation process and takes place in the smaller area. It was also found that for all strain rates applied, the maximal values of Hencky strain immediately before rupture of Gum Metal samples were similar for each of the applied strain rates, and the maximal local values of deformation rate were two orders higher when compared to applied average strain rate values.