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The modern approach to manufacturing of carbon-rhenium nanocomposites

Dobrzańska-Danikiewicz A. D., Wolany W.

Journal of Achievements in Materials and Manufacturing Engineering

2022

Vol. 115, nr 2

57--63

Purpose: The aim of the paper is to present the high-temperature method of producing MWCNTs-Re nanocomposites, the selection of satisfactory production conditions and the presentation of the results of microscopic and spectroscopic studies of nanocomposites produced by this method. Design/methodology/approach: Two methods of manufacturing carbon-rhenium nanocomposites were tested: ineffective chemical synthesis and high-temperature reduction using H2, which was proven successful and allowed the production of nanocomposites with the expected properties. The received nanocomposites were investigated using Transmission Electron Microscope (TEM), and Scanning Electron Microscope (SEM), as well as were subjected to spectroscopic examination. Findings: The article presents three steps of MWCNTs-Re nanocomposites fabrication using the high-temperature method, functionalization, impregnation and reduction. As part of own work, satisfactory conditions for producing those nanocomposites using a materials science and heuristic analysis were selected. Research limitations/implications: The proposed high-temperature method allows to join rhenium nanoparticles with MWCNTs permanently. It is reasonable to test in the future whether the method is also effective for other carbon nanomaterials and/or nanoparticles of other metals. Practical implications: MWCNTs-Re nanocomposites can be used as sensors of gases that are harmful to the environment. It was also confirmed that the MWCNTs-Re_4 nanocomposite has catalytic properties. Originality/value: The paper presents a modern approach to the manufacturing of MWCNTs-Re nanocomposites, which assumes the use of a high-temperature furnace to heat the material in a hydrogen atmosphere.

The Influence of the Sample Preparation on the Result of Coal Propensity to Spontaneous Combustion in the High-temperature Adiabatic Method

Obracaj Dariusz, Korzec Marek, Vu Tien Tung

Inżynieria Mineralna

2021

no. 2

65--78

The liability of coal to spontaneous combustion is the principal cause of mine fires. Spontaneous combustion is one of the main threats in Polish and Vietnamese coal mines. The article presents an analysis of the spontaneous combustion of coal in mines of both countries. It is related to the natural prone of coal to spontaneous heating and consequently to its self-ignition. Despite the relevant recognition of the methods of preventing this threat, in mines, spontaneous combustion occurs during the exploitation of coal seams with low and very high self-ignition tendency. Apart from the technical factors related to the design of coal seam mining, the properties of coal have a significant impact on the occurrence of spontaneous combustion. Their correct recognition is essential to the precautions against spontaneous combustion for minimalizing the risk of a mine fire. Therefore, it is necessary to study the factors influencing the propensity of coal to spontaneous heating. A review of the methods used to determine the propensity of coal to spontaneous combustion is presented in the article. Based on the high-temperature method of determining the propensity of coals to spontaneous combustion, the influence of selected factors related to samples' preparation for testing on the determination result was investigated. The influence of the fractional decomposition and the moisture content in the prepared samples on the determination result was demonstrated. The presented research results may improve research procedures for determining the propensity of coal to spontaneous combustion.