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EN
This study combined simulation and experimental tests to analyse the cutting performance of three solid carbide end mills with distinct geometries during the milling of the 7075 aluminium alloy. For the tests, three uncoated end mills were employed, which differed in rake angle, clearance angle, and helical pitch. Simulation tests revealed temperature distributions and the resultant cutting forces. The machining with a milling cutter with a higher blade angle was shown to cause an increase in the temperature in the cutting zone. However, during machining with a sharper blade of cutting tool, a decrease of cutting forces was not observed. The simulated temperature distribution on the cutting edge of the cutting tool may justify significant differences in the dynamics of changes in the cutting force components during the period of operational wear.
2
Content available remote Fabrication and Characteristics of Cast Aluminium – Mineral Particles Composite
EN
The paper presents the results of research on the production of cast composites based on aluminum alloys with a mineral filler with a porous structure. AlSi12 silumin and AlSi12 silumin with the addition of 3% magnesium (AlSi12-Mg3) were used as the matrix material, while particles of natural zeolite, expanded perlite and expanded clay with a size of 4 to 6 mm were used as the mineral filler. In order to increase the efficiency of the production process, the mineral particles have been covered with a sodium silicon solution with the addition of silicon powder. The coated particles were then heated at 400 °C for 1 hour to remove moisture from them. The prepared mineral particles were then placed inside a casting mold and flooded with liquid alloy at a temperature of 790 °C. The obtained composites were subjected to macroscopic observations and analysis using computed tomography (CT). Phase analysis was also performed to determine the phase composition of the obtained composites. In order to determine the mechanical and physical properties, the obtained composites were subjected to compressive strength tests and density measurements. As a result of the research, it was found that the use of the AlSi12-Mg3 alloy and coating in the form of a solution of sodium silicate and silicon powder allows for the most effective production of composites. The low density of the produced composites, combined with their favorable structure and strength properties, suggest the possibility of use as light products transferring compressive stresses, as well as energy-absorbing products.
EN
This article contains a review of selected studies conducted in the field of corrosion resistance of precipitation-hardenable 7000 series aluminum alloys. In particular, it discusses the effect of heat treatment and the role of thus formed microstructure on the corrosion behavior of these alloys. The article presents the three types of corrosion that occur most commonly in this group of materials in the context of their microstructure. It points to the importance of the chemical composition of a 7000 alloy, including the precipitates present in the microstructure, for the development of corrosion. The aluminum solid solution can act as an anode or cathode in relation to intermetallic particles. Such corrosion features may result in the destruction of the surfaces of elements made of the 7000 series aluminum alloy. It also raises the issue of the mechanism of corrosive destruction of the aluminum solid solution, which is connected with a crystallographic attack. In the case of this process, the nature of the micro-pits formed as a result of their local dissolution is related to the privileged dissolution of specific crystallographic planes and directions.
PL
Przedstawiono wyniki badań spawania TIG i MIG oraz zgrzewania FSW złączy z blach ze stopu aluminium EN AW6082, EN AW 5754 oraz odlewniczego stopu EN AC-43200. Scharakteryzowano stopy Al-Mg oraz Al-Mg-Si i ich spawalność. W ramach realizowanych badań przeprowadzono dobór warunków spawania i zgrzewania różnoimiennych stopów aluminium. Złącza poddano badaniom wizualnym, metalograficznym makroskopowym, penetracyjnym (złącza spawane) oraz własności mechanicznych w statycznej próbie rozciągania i zginania (złącza zgrzewane FSW). Na podstawie wyników badań realizowanych w Łukasiewicz – GIT oceniono, że jakość złączy spawanych zależy od przygotowania elementów do spawania, natomiast złączy zgrzewanych od parametrów zgrzewania i ustawienia stopów Al w złączu względem ruchu obrotowego narzędzia.
EN
Results of TIG, MIG and FSW welding technologies of joints made of EN AW-6082, EN AW 5754 aluminum alloy sheets and EN AC-43200 casting alloy are presented. This article briefly presents the characteristics of Al-Mg and Al-Mg-Si alloys and their weldability. As part of the research welding conditions for dissimilar aluminum alloys were selected. The joints were subjected to the visual and penetrant tests (TIG, MIG joints), light microscopy examination as well as tensile and bend tests (FSW joints). Based on the test results obtained in Łukasiewicz – GIT, it was found that the quality of arc welded joints depends on the preparation of the elements for welding, while the quality of FSW joints depends on the welding parameters and the positioning of Al alloys in the joint in relation to the rotational movement of the tool.
EN
The paper addresses an important scientific topic from the utilitarian point of view concerning the surface treatment of Al-Si-Cu aluminum alloys by PVD/ALD hybrid coating deposition. The influence of the conditions of deposition of titanium oxide in CrN/TiO2 coatings on their structure and properties, in particular corrosion resistance, were investigated. The TiO2 layer was produced by the atomic layer deposition (ALD) method with a variable number of cycles. Structural investigations were performed using scanning and transmission electron microscopy (SEM and TEM), atomic force microscopy (AFM), and Raman spectroscopy methods. Electrochemical properties were analyzed using potentiodynamic and electrochemical impedance spectroscopy (EIS) methods. The CrN/TiO2 hybrid coating with titanium oxide deposited at 500 ALD cycles showed the best corrosion properties. It was also found that the prerequisite for obtaining the best electrochemical properties was the amorphous structure of titanium oxide in the tested hybrid coatings. The high tribological properties of the tested coatings were also confirmed.
EN
The paper aims to review the corrosion properties of selected aluminum alloys applied in the automotive industry which are used in heat exchangers, bodyworks and car wires. Particular attention was focused on application of selected chemical compounds which added to corrosive environment in certain amounts lead to decrease of corrosion rate of protected aluminium alloy. Considered different environmental conditions which are simulating real vehicle exploitation. At review analyzed ability to application mentioned compounds on automotive parts, because there is needed fill of following requirements: environmentally friendly, relatively inexpensive and characterized by long-term performance under certain conditions. Main conclusion of review is that there are needed extension of research regarding to application of inhibitive compounds especially on the surface of cars wires.
EN
Convection caused by gravity and forced flow are present during casting. The effect of forced convection generated by a rotating magnetic field on the microstructure and precipitating phases in eutectic and hypoeutectic AlSiMn alloys was studied in solidification by a low cooling rate and low temperature gradient. The chemical composition of alloys was selected to allow joint growth or independent growth of occurring α-Al, α-Al15Si2Mn4 phases and Al-Si eutectics. Electromagnetic stirring caused instead of equiaxed dendrites mainly rosettes, changed the AlSi eutectic spacing, decreased the specific surface Sv and increased secondary dendrite arm spacing λ2 of α-Al, and modified the solidification time. Forced flow caused complex modification of pre-eutectic and inter-eutectic Mn-phases (Al15Si2Mn4) depending on the alloy composition. By high Mn content, in eutectic and hypoeutectic alloys, stirring caused reduction in the number density and a decrease in the overall dimension of pre-eutectic Mn-phases. Also across cylindrical sample, specific location of occurring phases by stirring was observed. No separation effect of Mn-phases by melt flow was observed. The study provided an understanding of the forced convection effect on individual precipitates and gave insight of what modifications can occur in the microstructure of castings made of technical alloys with complex composition.
EN
During mold filling and casting solidification, melt flow caused by gravity is present. Otherwise, forced flow may be a method applied for casting properties improvement. The flow effect generated by an electromagnetic field on the growing phases and a whole microstructure in Al-Si-Mn alloys was studied by slow solidification conditions. The hypereutectic and eutectic alloys were chosen to allow independent growth or joint growth of forming: Si crystals, Mn-rich α-Al15Si2Mn4 phases and Al-Si eutectics. In eutectic alloys, where Mn-phases precipitate as first and only one till solidus temperature, flow decreased number density of pre-eutectic α-Al15Si2Mn4. In the hypereutectic alloys, where Mn-phases grow in common with Si crystals, forced convection increased the overall dimension, decreased number density of pre-eutectic Mn phases and strengthened the tendency to growth in the outside of the sample. In the alloys, where Si crystals grow as first, stirring reduce number density of Si and moved them into thin layer outside cylindrical sample. Also by joint growth of Si crystals and Mn-phases, in hypereutectic Mn/Si alloy, flow moved Si crystals outside, reduced number density and increased the dimension of crystals. Stirring changed also AlSi eutectic spacing, specific surface Sv of α-Al and secondary dendrite arm spacing λ2. The results gave insight of what transformation under stirring take place in simple Al-Si-Mn alloys, and helps to understand what modifications in technical alloys may occur, that finally lead to changes in castings microstructure and properties. The possibility to control dimension, number density and position of Mn-phases and Si crystals is completely new and may help by metallurgical processes, continuous casting of billets and in the production of Si for the solar photovoltaic industry.
EN
Due to the high demand for secondary alloys in the automotive and aerospace industry, this work investigates the effect of higher iron content on the quality of AlSi7Mg0.6 sand castings. Secondary-recycled Al-Si alloys contain an increased amount of impurities due to their remelting of scrap metal. One of the most unwanted impurities found in these alloys is iron. Iron leads to the formation of various Fe-rich intermetallic phases, whose morphology influences the mechanical properties even at low Fe content. It also promotes the formation of casting defects, such as porosity and shrinkage. The formation of porosity in secondary Al-alloys is another major aspect that can affect the final properties of castings. Since these materials are mainly used to produce castings for the automotive industry, such as engine blocks, cylinder heads, and so on, it is necessary to produce castings without any defects. Therefore, the quality of AlSi7Mg0.6 sand casting is investigated at lower iron content (0.128% wt. Fe) and compared to the higher iron content (0.429% wt. Fe), whereby a correlation between iron content and porosity is monitored.
EN
The article analyzes the groundwork on the influence of alloying contaminants on the structure and mechanical properties of aluminum alloys. Aluminum has become widely used in various parts of machine-building due to its physical properties. However, the main task of modern material science is to increase the strength of aluminum alloys. Therefore, today there is the development of materials and alloys based on aluminum with alloying constituents (copper, silicon, magnesium, zinc, mangan), which are administered in aluminum mainly to increase its strength. Especially attractive are properties of aluminum-doped by transition metals, in particular scandium, zirconium, iron, etc. Finally, conclusions are drawn in order to develop a material based on aluminum with increased hardness, durability, and crack resistance.
EN
Cold spraying as a low-temperature coating deposition method is intended for thermally sensitive materials. Due to its precise temperature control, it limits the formation of structural defects, and can therefore be easily applied to spray corrosion protective coatings made from metal or metal-ceramic powders. However, the formation of pure ceramic coatings with the use of cold spraying is still not so common. Titanium dioxide is one of the most interesting ceramics due to its photocatalytic properties. Nevertheless, these types of coating materials usually work in a corrosion favoring humid atmosphere. In the presented paper, amorphous TiO2 powder was deposited onto aluminum alloys and steel substrates and then submitted to potentiodynamic corrosion tests in a 3.5 wt.% NaCl solution. The as-sprayed coating showed phase transition from amorphous TiO2 to anatase, and also revealed porosity. As a result, electrolytes penetrated the coating and caused undercoating corrosion in the tested environment of an aqueous NaCl solution. The analysis of the potentiodynamic curves showed that the presence of the coating decreased corrosion potential on both substrates. It arose from the mixed phases of TiO2, which consisted of photocathode - amorphous material and photoanode - crystalline anatase. The phase mixture induced the galvanic corrosion of metallic substrates in the presence of electrolytes. Moreover, pitting-like corrosion and coating delamination were detected in aluminium alloy and steel samples, respectively. Finally, the corrosion mechanism of the titanium dioxide coatings was characterized and described.
EN
In this work, the effect of single roll drive cross rolling on the microstructure, crystallographic texture, hardness, tensile properties, and fracture behavior of AA7075 aluminum alloy was investigated. It was found that with increasing the thickness reduction, the grain size reduced and the average width of grain for the 40% deformed sample decreased to 3.7 ± 0.4 µm. Due to the nature of the cross-rolling process, several X-type shear bands were observed after 40% deformation. The recrystallization texture is notably intensified to its highest value of 4.4 × R, after only 20% cold deformation due to the occurrence of continuous dynamic recrystallization (CDRX). The intensity of recrystallization texture sharply dropped to its lowest value of 2.7 × R. This was due to the rotation of Goss-orientated new grains in the 20% deformed sample toward copper orientation during 40% rolling. With increasing the thickness reduction, the overall texture intensity significantly reduced owing to the nature of the cross-rolling process in which the rolling direction rotates 90° after each 10% strain. Two texture transitions were observed along τ fiber: rolling (copper) texture to recrystallization (Goss) texture after 20% thickness reduction and recrystallization to the rolling texture after 40% deformation. The hardness and strength increased by increasing the thickness reduction, while the ductility decreased. After a 40% thickness reduction, yield strength significantly increased from 138.3 ± 4.4 MPa (for initial sample) to the highest value of 580.5 ± 11.5 MPa, demonstrating 320% increment, in the 0° direction. This increment for 45° and 90° direction was 265% and 337%, respectively. By 40% rolling, the value of in-plane anisotropy (IPA) remarkably decreased to its lowest value of 3.4% due to texture weakening. With increasing the rolling reduction to 20%, the severity of Portevin–Le Chatelier (PLC) increased in the flow curves due to the occurrence of CDRX and also strengthening of the rotated cube {001} < 110 > and E {111} < 110 > components. With increasing the rolling reduction, the size of cleavage facets and the severity of delamination increased, and the number and depth of dimples decreased.
EN
The paper compares changes in the structure and mechanical properties due to the synergistic effect of alloying elements Zr and Ti. It is assumed that by increasing the content of Zr and Ti in the aluminium alloy, better mechanical properties will be achieved. Paper focuses on description of the differences between the samples casted into the shell mold and the metal mold. Main difference between mentioned molds is a different heat transfer coefficient during pouring, solidification and cooling of the metal in the mold. The main goal was to analyse the influence of Zr and Ti elements and compare the mechanical properties after the heat treatment. Curing and precipitation aging were used during the experiment. The effect of the elements on AlSi7Mg0.3 alloy created differences between the excluded Zr phases after heat treatment. Evaluation of the microstructure pointed to the decomposition of large predominantly needle Zr phases into smaller, more stable formations.
PL
Stopy na bazie glinu ze względu na swoje właściwości znalazły wiele zastosowań i są używane do wyrobu szerokiej grupy produktów – od części karoserii i silników samochodów, przez poszycia i elementy konstrukcyjne samolotów, po części statków kosmicznych.
PL
W artykule przedstawiono wyniki badań dotyczące wytwarzania powłok elektroplazmowych (PEO – Plasma Electrolytic Oxidation) [2] metodą stałoprądową (DC) na stopach aluminium EN AW-1050 oraz EN AW-5083. Proces PEO realizowano w roztworze alkalicznym z zastosowaniem gęstości prądu 15 A/dm2, w czasie 8 min. Wytworzone powłoki uszczelniono, a następnie poddano procesowi lakierowania. Analizowano wpływ parametrów prądowo-napięciowych oraz temperatury na jakość otrzymywanych powłok. Wykonano badania: składu chemicznego, grubości, chropowatości, odporności na korozję oraz przyczepności powłok do podłoża. Wytworzone powłoki poddano również obserwacjom mikroskopowym.
EN
The paper presents the result of electroplasma coatings production on EN AW-1050 and EN AW-5083 aluminum alloys by DC current methods. The process was carried out in alkaline solution using a current density of 15 A/dm2, during 8 min. The produced PEO coatings [2] were sealed and varnished. The influence of current-voltage parameters and temperature on the quality of obtained coatings were investigated. Afterwards, the measurement of: chemical composition, thickness, roughness, corrosion resistance, abrasive wear and coating adhesion to the substrate were done. The produced coatings were also examined using electron scanning microscope.
EN
The tribological performance of 5xxx series aluminum alloys with ternary zirconium is evaluated at ambient conditions under dry, wet and saline environment. The experiment has been done using a Pin-on-Disk apparatus under an applied load of 20N. The sliding distances varies ranging from 116m-2772m at a sliding velocity of 0.385 ms-1. The results show that presence of Mg and Zr into this alloy helps to increase their strength and wear resistance under dry sliding condition. But they significantly suffer under wet and corrosive environment due to formation of β-phase Al3Mg2, to slip bands and grain boundaries which may lead to and stress-corrosion cracking. The variation of friction coefficient is observed in wet and corrosive environment due to the formation of oxidation film, lubrication, and corrosion action in solution. The SEM analysis shows that brittle Al3Mg2 phase initiate the fracture surface for Al-Mg alloy and Zr addition accelerate the brittleness of the alloy owing the fine precipitates of Al3Zr.
EN
The paper presents the possibility of using FSW technology for joining elements of a landing gear beam of the M28 aircraft. The FSW process was performed on a 4-axis numerical machine under industrial conditions. However, before welding was carried out under industrial conditions, preliminary experimental tests were carried out under laboratory conditions. Preliminary research was carried out for AA2024-T3 aluminum sheets of 1 mm and 3 mm in thickness, joined in a lap configuration. The influence of technological and geometric parameters of the process on the quality and strength of the weld was examined. Sheet metal arrangement was analyzed. Tests were carried out for two configurations. The first of which with 1 mm sheet on the top and 3 mm sheet on the bottom and in reverse order. It has been shown that setting a thicker plate on the top gives a 40% better strength. The microhardness and microstructure of the weld were tested. During the laboratory tests, low-cycle fatigue tests of the FSW lap joint were performed. It has been shown that the FSW method can be an alternative to the riveting process in the production of aviation structure elements.
EN
The effect of the complex ligature with nickel and REM (Ce, La) aluminides on the structure formation, the nature of the distribution of the elements, and the microhardness of the structural constituents of Al-5 wt.% Cu aluminum alloy were investigated. On the example of microalloying of the Al-5 wt.% Cu alloy with a master alloy containing Ni and REM (Ce, La) aluminides it was shown that a redistribution of Al and Cu occurs in α-solid solution and eutectic. This is reflected in the refinement of α-solid solution and eutectic at 0.15 wt.% of the master alloy addition and, accordingly, increases the microhardness of α-solid solution by 100 MPa and eutectic by 125 MPa.
EN
The paper covers the research on the process of solutionizing of 7075 aluminum alloy in cold tools during the stamping of a high-strength structural element (B-pillar’s base). For technological reasons, in order to obtain high strength parameters of the 7075 alloy, it is necessary to carry out a solutionization process, which allows to obtain dispersion strengthening during ageing process. Properly performed heat treatment of the alloy increases the strength of the material to approx. 600 MPa. The combination of the process of solutionization with simultaneous shaping is aimed at improving and simplifying technological operations of aluminum alloy stamping, shortening the duration of the manufacturing process and reducing production costs. The manufactured lower part of the B-pillar will be used for the verification of the validity of the developed method. During the experiment, a series of stamping tests were carried out, in which the lubricants, pressure and position of the upper and lower blankholders were the variables. The obtained results allow to estimate the influence of the cooling conditions on the strength of the drawpieces obtained after the process of artificial ageing. In order to verify and analyse the results more quickly, a numerical simulation was carried out.
20
EN
Silver coatings have a very high reflection ability. To avoid their darkening from the hydrogen sulphide in the air, a thin layer of heat-resistant colorless lacquer is applied to the coatings. Silver plating is mainly used in jewelery, optics, electronics and electrical engineering. Depending on their application the thickness of the layer may vary from 2 to 24 μm. It can be done in several ways: chemical, electrochemical, contact, etc. The most common way of silver plating is the electrochemical deposition using cyanide and non-cyanide electrolytes. The cyanide electrolytes produce light, fine crystalline, dense and plastic coatings upon silver-plating. Usually silver coatings are applied with copper or nickel intermediate layer. In order to improve the de-oxidation of the aluminum surface new chemical treatment in acid – alkaline solution was applied. Our previous research shows that the presence of diamond nanoparticles in the electrolyte increase the metal deposition. Samples were prepared from electrolyte containing 10 g/l diamond nanoparticles. Their properties were compared to the properties of reference samples. The diamonds were obtained by detonation synthesis. The aim of this study is to obtain electrochemically deposited silver layer with high density, adhesion and electric conductivity on aluminum alloys substrate. The coating was directly plated without intermediate layer. Non-cyanide electrolyte composition and electrochemical parameters were determined in order to produce Ag coatings on Al alloy substrate without intermediate layer. The coating is with good adhesion, density and thickness of 14-23 μm.
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