Voltammetric determination of Aclonifen at a silver amalgam electrode in drinking and river water

• Autorzy: Novotný V. , Barek J.

Identyfikatory

DOI

10.1515/eces-2017-0019

Warianty tytułu

PL

Woltamperometryczne oznaczanie Aklonifenu za pomocą amalgamatowej elektrody srebrnej w wodzie pitnej i rzecznej

• Języki publikacji: EN

Abstrakty

EN

A method for the determination of pesticide Aclonifen (AC) in drinking and river water by differential pulse voltammetry (DPV) on a meniscus modified silver solid amalgam electrode (m-AgSAE) using solid phase extraction (SPE) as a cleanup and preconcentration procedure is described. The limit of detection (LOD) for direct DPV determination of AC in deionized water is 2.7·10^-8 mol·dm^-3. LOD for DPV determination of AC in tap water after SPE is 1.6·10^-10 mol·dm^-3, the recovery being 55%. LOD for the determination of AC in Vltava river water is 1.9·10^-9 mol·dm^-3, the recovery being 65%. Humic acids interfere with the determination in river water; this problem can be resolved by adjusting the pH of the extracted sample to 6. The advantages of this approach are high sensitivity, low LOD, quick and easy sample preparation and fast determination.

Słowa kluczowe

EN

aclonifen; silver solid amalgam electrode; drinking water; river water; solid phase extraction

PL

aklonifen; amalgamatowa elektroda srebrna; woda pitna; woda rzeczna; ekstrakcja w fazie stałej

• Wydawca: Towarzystwo Chemii i Inżynierii Ekologicznej
• Czasopismo: Ecological Chemistry and Engineering. S
• Rocznik: 2017
• Tom: Vol. 24, nr 2
• Strony: 277--284
• Opis fizyczny: Bibliogr. 29 poz., wykr., tab.

Twórcy

autor

Novotný V.

• UNESCO Laboratory of Environmental Electrochemistry, Department of Analytical Chemistry, Faculty of Science, Charles University, Hlavova 2030, Prague 2, Czech Republic

autor

Barek J.

• Institute for Nanomaterials, Advanced Technology and Innovation, Technical University of Liberec, Bendlova 1407/7 Liberec, Czech Republic

Bibliografia

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Uwagi

PL

Opracowanie ze środków MNiSW w ramach umowy 812/P-DUN/2016 na działalność upowszechniającą naukę (zadania 2017).