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Fabrication and characterization of Zr microplasma sprayed coatings for medical applications

100%

Voinarovych S. G. , Alontseva D. L. , Kyslytsia O. N. , Kaliuzhnyi S. , Khozhanov A. R. , Krasavin A. , Kolesnikova T.

Advances in Materials Science

2021

tom Vol. 21, nr 2(68)

93--105

This paper presents new results of studying the influence of parameters of microplasma spraying (MPS) of Zr wire on the structure of Zr coatings. The coating experiments were accomplished in a two level fractional factorial design. Individual particles of sprayed Zr wire and their splats on the substrate were collected under various spraying parameters (amperage, spraying distance, plasma gas flow rate and wire flow rate) and evaluated by Scanning Electron Microscopy (SEM) to establish the effect of particle size and shape on the coating microstructure. The particles were characterized by measurement of their sizes and the obtained results were evaluated in terms of their degree of melting. This was compared with the experimentally observed coating microstructure type and finally correlated to the investigated coating porosity to select the specific MPS parameters of Zr coatings depositing onto medical implants from Ti alloy. It was found that the main parameters influencing the size of the sprayed Zr particles and the porosity of the Zr coatings are the plasma gas flow rate and amperage. It was demonstrated that it is possible to control the porosity of Zr microplasma coatings in the range from 2.8% to 20.3% by changing the parameters of the MPS. The parameters of microplasma spraying of Zr wire were established to obtain medical implant coatings with porosity up to 20.3% and pore size up to 300 μm.

Microplasma-sprayed multilayer coatings for electric heating elements

84%

Kaliuzhnyi S. , Alontseva D. , Voinarovych S. , Kyslytsia O. , Khozhanov A. , Łatka L. , Faizrakhmanov Z. , Bektasova G.

Materials Science Poland

2022

tom Vol. 40, No. 4

158--170

The paper presents new results on the application of microplasma spraying (MPS) for manufacturing electric heating elements (EHEs) consisting of a St3 steel plate (the substrate) with a sprayed electrically insulating Al2O3 sublayer (400±50 μm thick) and TiO2 electric heating tracks (4 mm width; 150±50 μm thickness). Measurements of the temperature of the multilayer coating with a thermal imager enabled determination of the temperature distribution over the surface of the EHE. The electric strength and conductivity tests showed the efficiency of the sprayed EHEs up to a temperature of 200°C. The results of analysis of the causes of material losses during MPS of electric heating tracks (TiO2) are presented, and the optimal parameters for efficient MPS of coatings in the form of narrow tracks on steel substrates are determined. Using regression analyses, the equation for the influence of MPS parameters on the coating transfer efficiency (CTE) is obtained. Process parameters such as the electric current and the plasma-forming gas flow rate have been found to have the greatest influence on the CTE. In the experiment, a high efficiency of the sprayed material during MPS of electric heating tracks of TiO2 powder was established (the maximum CTE reached 89%), which indicates the prospects for using MPS technology in the production of EHEs for DC electric heating and for maintaining the temperature of product surfaces up to 200°C.

The influence of plasma-sprayed coatings on surface properties and corrosion resistance of 316L stainless steel for possible implant application

84%

Woźniak A. , Staszuk M. , Reimann Ł. , Bialas O. , Brytan Z. , Voinarovych S. , Kyslytsia O. , Kaliuzhnyi S. , Basiaga M. , Adamiak M.

Archives of Civil and Mechanical Engineering

2021

tom Vol. 21, no. 4

223--243

Herein, we analyzed the morphology of atmospheric plasma-sprayed (APS) coating on medical 316L stainless steel and its influence on the physical and electrochemical properties of implant application. Five types of coatings were examined: hydroxyapatite (HAp), titanium (Ti), zirconium (Zr), Ti/HAp and Zr/HAp. The base properties of the coatings were analyzed via chemical and phase composition, surface topography, surface wettability and in particular the corrosion resistance in Ringer solution in immersed conditions and potentiodynamic test, and EIS analysis. APS coating of pure HAp on 316L stainless steel showed poor cohesive bonding to the substrate material, whereas the application of Ti and Zr interlayer prior to HAp deposition improved surface morphology and coating properties. The beneficial effect of Ti and Zr interlayer under HAp layer on binding was demonstrated. HAp containing coatings (HAp, Ti/HAp and Zr/HAp) show Ca/P ratio greater than 1.8, which may positively influence the differentiation of osteogenic cells and good adhesion to bones. Among the studied materials, the composite coatings with Zr or Zr/HAp showed favorable physicochemical properties and the highest corrosion resistance in Ringer solution.