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3 Archives of Metallurgy and Materials

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Material Production and the Effect of the System on Biocompatibility in the Modified Metal Injection Method

100%

Çiçek B. , Sun Y.

Archives of Metallurgy and Materials

2023

tom Vol. 68, iss. 1

195--204

In this study, the bio state of the alloy produced in the modified metal injection system was monitored after sintering. A new system operating with high gas pressure, far from the traditional injection model, has been established for material production. In this system, 316L stainless steel powders were molded using a PEG/PMMA/SA polymer recipe. During molding, approximately 60% 316L and 40% binder by volume were used. The samples obtained were sintered at different temperatures (1100-1300°C) after de-binding. Density measurement (Archimedes) and hardness tests (HV1) of the samples were measured as 6.74 g/cm3 and ~285 HV1, respectively. A potentiodynamic corrosion test was applied to monitor the effect of the amount of oxide in the structure of the 316L stainless steel produced. Corrosion tests were carried out in artificial body solutions. The corrosion rate was measured at the level of 17.08×10-3 mm/y. In terms of biocompatibility, a cytotoxicity test was applied to the samples and the life course of the bacteria was monitored. For the 316L alloys produced, the % vitality reached approximately 103%.

Investigation of Microstructure, Mechanical and Corrosion Properties of Biodegradable Mg-Ag Alloys

70%

Elen L. , Turen Y. , Ahlatci H. , Sun Y. , Unal M.

Archives of Metallurgy and Materials

2022

tom Vol. 67, iss. 3

889-900

In this study, microstructure, mechanical, corrosion and corrosive wear properties of Mg-xAg the as-cast and extruded alloys (x: 1, 3 and 5 wt.%Ag) were investigated. According to the experimental results, as the amount of Ag added in the casting alloys increases, the secondary phases (Mg4Ag, Mg54Ag17) emerging in the structure have become more clarified. Furthermore, it was observed that as the amount of Ag increased, the grain size decreased and thus the mechanical properties of the alloys increased. Similarly, the extrusion process enabled the grains to be refined and the mechanical properties to be increased. As a result of the in vitro tests performed, the Mg-1Ag exhibited very bad corrosion properties compared to other alloys. On the other hand, according to corrosive wear tests results, a high wear rate and friction coefficient were found for Mg-5Ag alloys.

A comparative Study on the Mechanical and Corrosion Properties of the ZM20 and ZM21 Alloys after Casting and Rolling

70%

Gören H. A. , Ünal M. , Türen Y. , Ahlatçı H. , Sun Y.

Archives of Metallurgy and Materials

2022

tom Vol. 67, iss. 4

1387--1394

In this study, the effects of grain refinement and production methods on the corrosion, corrosive wear and mechanical properties of the as-cast and as-rolled Mg-2 wt.% Zn (ZM20) and Mg-2 wt.% Zn-0,51 wt.% Mn (ZM21) alloys were examined by using OM, XRD, SEM, hardness and uniaxial tensile test. Additionally, the potentiodynamic polarization, immersion corrosion test and corrosive wear properties of the ZM20 and ZM21 alloys were compared. According to the XRD results, MgZn and MgZn2 phases were found in the alloys and also MnZn3 phase occurred in the ZM21 alloy with the addition of manganese. Both during solidification forming nucleation points with the added manganese and during rolling the broken secondary phase particles distributed into the matrix prevented grain growth and led to the formation of a more refined structure. The tensile test results showed that the strength of the as-cast ZM21 alloys were better than that of the as-cast ZM20 alloys and further improvement in mechanical properties occurred with the rolling of the both alloys. The most superior hardness was found in the as-rolled ZM21 alloy. In the total 400-m reciprocal corrosive wear test in the 3.5% NaCl solution, the lowest mass loss was in the as-rolled ZM21 alloys. In the potentiodynamic corrosion test, the highest corrosion resistance was occurred by the as-cast ZM20 alloy.