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Comparison of results obtained using the injection method of preparation of solid amorphous alloys with and without suction

100%

Klimas J. , Łukaszewicz A. , Szota M. , Nabiałek M. , Dobrzańska-Danikiewicz A.

2014

tom Vol. 67, nr 2

77--83

Purpose: The study compares the structure and properties titanium alloy Ti-6Al-4V produced by injection method allowing the production of massive amorphous materials in two varies – with and without suction. Design/methodology/approach: Samples were produced form titanium alloy Ti-6Al-4V produced by injection method. Structures and properties were compared of the same alloy but with different conditions in production process – with and without suction. To achieve the objective perused the following tests were carried out: study of phase composition by X-ray diffraction, observation of microstructure by using optical microscope and SEM, study of surface geometry – roughness, abrasion resistance tests and microhardness tests. Results: Microstructural studies have allowed to observe that the titanium alloy Ti-6Al-4V produced by injection method in both varies – with and without suction during injection to copper mold, has structure partially crystalized – nanocrystalline. In structure occur the crystal nuclei and lack of arrangement and regularity. The study of microhardness showed 100 HV 0.1 units higher hardness value in the embodiment with suction in comparison to the variant without suction. Titanium alloy Ti-6Al-4V produced with suction has better abrasion resistance in comparison with same alloy without suction. Alloy produced with suction has lower development area. Originality/value: The paper presented studies of massive amorphous and nanocrystalline alloys produced by alternative method – injection casting in two variants – with and without suction. That kind of production allow produced alloys with same chemical composition as commercial but with far better properties.

Spiekanie tytanu i hydroksyapatytu metodą iskrowego spiekania plazmowego

100%

Garbiec D. , Heyduk F.

tom Vol. 79, nr 8

569--574

W artykule omówiono metodę iskrowego spiekania plazmowego SPS (ang. Spark Plasma Sintering). Przedstawiono graficznie proces spiekania wraz ze schematem urządzenia oraz wyjaśniono mechanizm spiekania impulsami prądu stałego. Opracowano proces spiekania proszku stopu tytanu Ti6Al4V oraz proszku hydroksyapatytu (HA) wraz z 5 % dodatkiem srebra. Ocenie za pomocą mikroskopu skaningowego poddano powierzchnię uzyskanych próbek. Na podstawie badań zaproponowano parametry wytwarzania próbek przeznaczonych do badań in-vitro. Wykazano, że minimalną temperaturą przy której można uzyskać powłokę HA charakteryzującą się dobrym połączeniem z podłożem jest 750 °C.

The article discusses the method of Spark Plasma Sintering. Presented graphically sintering process and SPS device diagram. Explained the mechanism of sintering DC pulses. Titanium alloy powder Ti6Al4V and hydroxyapatite powder with 5 % silver sintering process was developed. Evaluated by scanning electron microscopy were obtained surface samples. Based on the research proposed parameters for sample preparation on in-vitro. It was shown that the minimum temperature at which the HA coating can be characterized by good access to the substrate is 750 °C.