The self propagation high-temperature synthesis (SHS) was carried out in the equimolar powder mixture of molybdenum and aluminium. The reaction products Mo3Al8 and Mo3Al were analysed to determine chemical composition and microstructure. Density measurements using helium pycnometer permitted determination of molar fractions of molybdenum aluminides in the reaction product. Thus, the equimolar mixture of molybdenum and aluminium yielded about 23mol% Mo3Al8 and about 77mol% Mo3Al. The SHS products were densified by hot pressing (HP).
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