This paper presents the characteristics of titanium silicalite catalysts synthesized in the presence of hexaalkyl-1,6-hexanediammonium hydroxides [R3N+(CH2)6N+R3]2OH with the following alkyl groups: -CH3, -C2H5, -C3H7 and -C4H9 (clathrating agents). Syntheses were carried out in the presence of hexaalkyl-1,6-hexanediammonium hydroxides or hexaalkyl-1,6-hexanediammonium bromides in the mixture with sodium hydroxide. Hexaalkyl-1,6-hexanediammonium hydroxides were prepared from corresponding bromides in the reaction with Ag2O). Bromides were obtained in the reaction of corresponding amine and 1,6-dibromohexane. The catalysts were examined by XRF, IR,UV-VIS, SEM and XRD methods.
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