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Diffusive and Displacive Phase Transformations in Nanocomposites under High Pressure Torsion

100%

Straumal B. , Kilmametov A. , Gornakova A. , Mazilkin A. , Baretzky B. , Korneva A. , Zięba P.

2019

tom Vol. 64, iss. 2

457--465

The high-pressure torsion (HPT) of Ti-Fe alloys with different iron content has been studied at 7 GPa, 5 anvil rotations and rotation speed of 1 rpm. The alloys have been annealed before HPT in such a way that they contained different amounts of α/α' and β phases. In turn, the β phase contained different concentration of iron. The 5 anvil rotations correspond to the HPT steady-state and to the dynamic equilibrium between formation and annihilation of microstructure defects. HPT leads to the transformation of initial α/α' and β-phases into mixture of α and high-pressure ω-phase. The α → ω and β → ω phase transformations are martensitic, and certain orientation relationships exist between α and ω as well as β and ω phases. However, the composition of ω-phase is the same in all samples after HPT and does not depend on the composition of β-phase (which is different in different initial samples). Therefore, the martensitic (diffusionless) transformations are combined with a certain HPT-driven mass-transfer. We observed also that the structure and properties of phases (namely, α-Ti and ω-Ti) in the Ti – 2.2 wt. % Fe and Ti – 4 wt. % Fe alloys after HPT are equifinal and do not depend on the structure and properties of initial α'-Ti and β-Ti before HPT.

3D DIC-assisted residual stress measurement in 316 LVM steel processed by HE and HPT

51%

Brynk T. , Krawczyńska A. T. , Setman D. , Pakieła Z.

2020

tom Vol. 20, no. 3

18--29

A method has been developed for determining residual stress based on displacement fields near drilled holes analyzed using 3D digital image correlation. Finite element modeling was used to determine corrections for analytical equations describing displacement fields near the blind holes, which made it possible to determine the residual stress distribution over a wide range of hole depth-to-hole diameter ratios and various areas of displacement field measurements using inverse method iterative calculations. The proposed method eliminates many drawbacks of traditional procedure based on strain gauges as hole eccentricity sensitivity and requirement of the relatively large span between holes. The method and testing setup, build-up of generally available components, were used to determine the residual stress distribution for 316 LVM samples processed by two methods from the large deformation group: hydrostatic extrusion (HE) and high-pressure torsion (HPT), by drilling 1.75 and 0.58-mm-diameter blind holes, respectively. In the case of the measurements performed on the surface of a HE-processed 16 mm bar cut along its diameter, a gradual change was revealed-from a compressive to a tensile residual stress distribution (from ~ − 300 MPa in the center to 400 MPa in 4 mm distance from the edge) in the longitudinal direction, with near-zero values in the radial direction. Moreover, the method was also adapted to perform measurements on the outside surface of the bar, which gave results consistent with those taken along the radius profile (~ 600 MPa longitudinal stress). Measurements on the top surface of a cylinder 10 mm in diameter and 1 mm high processed by HPT showed a high compressive residual stress in the center and a dominant shear component for the holes drilled at different distances from the center.