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3 International Letters of Chemistry, Physics and Astronomy

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Mechanical, thermal and morphological behaviours of polybutylene terephthalate/polycarbonate blend nanocomposites

100%

Rajakumar P. R. , Nanthini R.

tom Vol. 4

15-36

Polybutylene Terephthalate (PBT) / Polycarbonate (PC) nanocomposite blend was fabricated using melt blending technique in a twin extruder. The blend composition was optimized at PBT-PC weight ratio of 80-20. The effect of incorporation of various organically modified Montmorillonite (OMMT) and naturally occurring sodium Montmorillonite (MMT) on the mechanical, thermal and morphological properties of the nanocomposites blend has been investigated. It was observed that the Izod impact strength, tensile strength and flexural strength demonstrated a significant increase with the increase in clay loading from 1-7 weight % due to homogeneous dispersion of clay within the blend matrix. Thermo gravimetric analysis (TGA) revealed an increase in thermal stability of the blend with the incorporation of nanoclay. There is also decrease in the melting temperature (Tm) and crystallisation temperature (Tc) as observed from DSC thermograms. DMA add the evidence for TGA, DSC and mechanical results. PBT - PC blend with clay exhibited featureless XRD indicative of exfoliated structure. TEM micrographs also confirm the same that the clay has exfoliated into individual layers.

Infrared spectral analysis of waste pet samples

100%

Vijayakumar S. , Rajakumar P. R.

tom Vol. 4

58-65

There are fifteen waste pet bottles and a commercial grade ABS was collected from local supplier of Chidambaram town. The ABS was used to study the mechanical properties of PET blend composites. This study was performed by FT-IR spectroscopy. From the characteristics infra-red stretching bands the mechanical properties of samples were discussed.

Spectral correlations and antimicrobial activities of some 1-pyrenyl chalcones

51%

Arulkumaran R. , Vijayakumar S. , Sundararajan R. , Sakthinathan S. P. , Kamalakkannan D. , Suresh R. , Ranganathan K. , Rajakumar P. R.

tom Vol. 5

21-38

A series of 1-pyrenyl chalcones have been synthesized by Crossed-Aldol condensation of 1-acetylpyrene and substituted benzaldehydes. The purities of these chalcones have been checked by their physical constants, UV, IR, NMR and MASS spectral data. The spectral data of these chalcones have been correlated with Hammett sigma constants, F and R parameters using single and multi-linear regression analysis. From the results of statistical analysis, the effect of substituents on the spectral group frequencies have been discussed. The anti-microbial activities of these chalcones have been evaluated using Bauer-Kirby method.