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2 International Letters of Natural Sciences

2 2014

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Thermal analytical characteristics by TGA-DTA-DSC analysis of Carica papaya leaves from Kachchh

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Ram V. R. , Ram P. N. , Khatri T. T. , Vyas S. J. , Dave P. N.

tom 21

An experimental study on Carica papaya leaves was carried out in Thermo gravimetric analyzer (TGA), Differential Thermal Analyzer (DTA) and Differential Scanning Calorimetric (DSC) analyzer to investigate the effects of reaction atmosphere on thermal chemical characteristics. Experimental results show that In DSC curve, Endothermic peak at 101 °C is attributed to dehydration/Water loss from surface and pores of the powder sample. Step at 215 °C is associated with second order phase transition such as Glass Transition and it should be further confirmed in second heating (During heat- cool- heat cycle). Endothermic peak at 336 °C is associated protease thermal decomposition /Beta Cyclodextrin breakdown. In the TGA Curve, The initial 4 % weight loss is due to water loss from surface/pores of powder sample. Second weight loss between 200-450 °C is associated to degradation of cellulose and hemicellulose.

XRF analysis of Carica papaya leaves of semi arid region of Kachchh

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Ram P. N. , Ram V. R. , Khatri T. T. , Vyas S. J. , Dave P. N.

2014

tom 19

The objective of the present investigation was to study the chemical composition of leaves of Carica papaya belonging to family Caricaceae growing in semi-arid region of Kachchh district, Gujarat, India. The leaves of C. papaya were subjected to Energy Dispersive X-ray Fluorescence (EDXRF) and were analyzed for different mineral composition. As the X-ray Fluorescence is one of the most reliable and accurate, as well as it is also a consistent and non-destructive method for analysis of major and trace elements using a single pressed pellet. During the study it was found that Oxygen, Calcium, Magnessium, Potassium were noted in higher amounts, compared to that of other elements like Silicon, Sulphur, Phosphorus, Chloride, Strontium, Stanous, Aluminium, Cromium and Mangenese, whereas the elements which were not detected in leaves of C. papaya are Vanadium, Titanium, Cobalt and Tantalum.