Methods of incremental manufacturing, i.e. 3D printing, have been experiencing significant growth in recent years, both in terms of the development of modern technologies dedicated to various applications, and in terms of optimizing the parameters of the process itself so as to ensure the desired mechanical and strength properties of the parts produced in this way. High hopes are currently being pinned on the use of highly penetrating types of radiation, i.e. synchrotron and/or neutron radiation, for quantitative identification of parameters characterizing objects produced by means of 3D printing. Thanks to diffraction methodologies, it is feasible to obtain input information to optimize 3D printing procedures not only for finished prints but also to monitor in situ printing processes. Thanks to these methodologies, it is possible to obtain information on parameters that are critical from the perspective of application of such obtained elements as stresses generated during the printing procedure itself as well as residual stresses after printing. This parameter, from the point of view of tensile strength, compression strength as well as fatigue strength, is crucial and determines the possibility of introducing elements produced by incremental methods into widespread industrial use.
The greatest challenge of widely developed incremental manufacturing methods today is to obtain, as a result of the manufacturing process, such components that will have acceptable strength properties from the point of view of a given application. These properties are indirectly determined by three key characteristics: the level of surface residual stress, the roughness of the component and its porosity. Currently, the efforts of many research groups are focused on the problem of optimizing the parameters of incremental manufacturing so as to achieve the appropriate level of compressive residual stress, the lowest possible porosity and the lowest possible roughness of parts obtained by 3D methods. It is now recognized that determining the level of these three parameters is potentially possible using experimental X-ray diffraction methods. The use of this type of radiation, admittedly, is only used to characterize the surface layer of elements, but its undoubted advantage is its easy availability and relatively low cost compared to experiments carried out using synchrotron or neutron radiation.
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