X-ray diffraction, scanning electron microscopy and hardness measurements were applied as experimental methods to investigate the structure and properties of the crystalline-amorphous Al-based composites prepared by mechanical alloying and subsequent high pressure high temperature compaction of the powders. It was possible to obtain bulk, fully dense crystalline-amorphous composites and the applied compaction technique allowed preservation of amorphous structure in the composite. Addition of amorphous Al_{60}Nb_{40} phase to AA6061 alloy resulted in significant increase of hardness of the composite (120 HV), comparing to pure Al alloy compacted at the same conditions (75 HV).
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