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Thermo-magnetic stability of magnetic Fe3O4 nanoparticles for hyperthermia

100%

Pan Y. M. , Zhang W. , Hu Z. F. , Feng Z. Y. , Zhang X. P.

Materials Science Poland

2020

tom Vol. 38, No. 4

637--643

Monodispersed Fe3O4 magnetic particles adsorbed by amylase (such as citric acid (CA), carboxymethyl chitosan (CMCH) and β-cyclodextrin (CD)) were prepared by means of co-precipitation method. The absorption character of the samples was investigated by FT-IR, TG and VSM. It was found that the carboxyl (COOH groups) of amylase reacted with the hydroxyl (OH groups) on the surface of Fe3O4 particles, resulting in the formation of iron carboxylate that was adsorbed onto Fe3O4. The induction heating properties of the magnetic Fe3O4 nanoparticles in an alternating current magnetic field were also investigated and the thermo-magnetic stability in induction heating was discussed.

Development of HPLC fingerprint for the quality control of Euonymus fortunei and distinguishing it from related species

100%

Ouyang X. L. , Fang X. M. , Pan Y. M. , Wei L. X. , Wang H. S.

Acta Chromatographica

2012

tom Vol. 24, no. 2

301--316

To control the quality of Euonymus fortunei (Turcz.) Hand.-Mazz., a simple and reliable method of high-performance liquid chromatography (HPLC) coupled with photodiode array detector (PAD) was developed for both fingerprint analysis and quantitative determination. Four representative flavonoids, namely, kaempferol-3-O-β-D-glucopyranosyl-(1→4)-α-L-rhamnopyranosyl-7-O-β-D-glucopyranosyl-(1→4)-α-L-rhamnopyranoside (I), kaempferol-3,7-O-α-dirhamnopyranoside (II), apigenin-7-O-β-D-glucopyranoside (III), and kaempferol-3-(4″-O-acetyl)-O-α-L-rhamnopyranoside-7-O-α-L-r hamnopyranoside (IV) isolated from E. fortunei, were used as reference compounds and simultaneously determined by the validated HPLC method. The unique properties of the chromatographic fingerprint were validated by analyzing 11 batches of E. fortunei, E. japonicus, E. laxiflorus, E. myrianthus, and E. hamiltonianus samples. Our results revealed that the chromatographic fingerprint combined with similarity measurement could efficiently identify and distinguish E. fortunei from the other investigated Euonymus species.