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1 Polish Journal of Environmental Studies

1 2016

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Determining eight biogenic amines in surface water using high-performance liquid chromatography–tandem mass spectrometry

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Quan Z. , Xie G. , Peng Q. , Shan J. , Xing W. , Zhang J. , Li S. , Chan Z. , Chou C. , Zou H.

Polish Journal of Environmental Studies

2016

tom 25

nr 4

A method for determining eight biogenic amines in surface water was established using high-performance liquid chromatography–triple quadrupole mass spectrometry to improve on the detection sensitivity of current methods. The limits of detection and quantification were 0.05 and 0.2 μg L⁻¹, respectively, for histamine, cadaverine, spermine, and spermidine, 1.0 and 3.0 μg L⁻¹, respectively, for putrescine, 1.5 and 5.0 μg L⁻¹, respectively, for tyramine and tryptamine, and 2.0 and 5.0 μg L⁻¹, respectively, for 2-phenylethylamine. The recovery of biogenic amines from spiked water samples was between 97.3 and 108.6% at levels between 0.05 and 15 μg L⁻¹ (R > 0.999). The relative standard deviations were in the range of 0.10-0.29%. This method can achieve rapid and accurate determination of biogenic amines in surface water, and it meets the minimum residue measurement requirements.