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Solvent-free synthesis of 1-amidoalkyl-2-naphthol and 3-amino-1-phenyl-1H benzo[f]chromene-2-carbonitrile derivatives by Fe3O4@enamine-B(OSO3H)2 as an efficient and novel heterogeneous magnetic nanostructure catalyst

100%

Li F. , Zhang J. , Wang L. , Liu W. , Yousif Q. A.

Polish Journal of Chemical Technology

2020

tom Vol. 22, nr 2

9--19

A green procedure for the one-pot three-component synthesis of 1-amidoalkyl-2-naphthol and 3-amino-1-phenyl-1H benzo[f]chromene-2-carbonitrile derivatives from the reaction of 2-naphtol, aldehydes, and malononitrile/acetamide in the presence of a catalytic amount of Fe3O4@enamine-B(OSO3H)2 as an efficient and novel heterogeneous magnetic nanostructure catalyst is described. The catalyst was characterized using Fourier transform infrared spectroscopy (FTIR), thermogravimetric analysis (TGA), vibrating sample magnetometry (VSM), energy dispersive X-ray spectroscopy (EDX), and X-ray diffraction (XRD). These strategies possess some merits such as simple work-up method, easy preparation of the catalyst, short reaction times, good-to-high yields, and non-use of hazardous solvents during all steps of the reactions. Moreover, due to the magnetic nature of the catalyst, it was readily recovered by magnetic decantation and can be recycled at least six runs with no considerable decrease in catalytic activity.

Influence of grouting pressure volatility on additional response of adjacent pile foundation in shield construction

100%

Zhang C.-C. , Li D.-M. , Zhang J. , Yu T.-S. , Chen Q.

tom Vol. 60 nr 1

33--47

Soil parameters along the heading direction are subjected to spatial variability during shield construction, so grouting pressure requires constant adjustment to ensure ground stress sta- bility. This causes grouting pressure to fluctuate around the design pressure/curve. There- fore, the influence of the grouting pressure volatility on the adjacent loaded-pile foundation should be considered in shield tunneling. In this study, a refined numerical simulation of the shield construction process is conducted using the Fast Lagrangian Analysis of Continua in Three Dimensions (FLAC3D) software. A total of 300 groups of grouting pressure pa- rameters with a skewed normal distribution are input into the numerical model. Then, the influence of the construction parameter uncertainty on the adjacent loaded-pile foundation is analyzed. Finally, the back analysis method is conducted based on the monitored data to evaluate how the construction process affects the pile foundation. The calculation results are compared with those of the traditional finite element method. The results indicate that in the tunneling process, the grouting pressure fluctuation greatly affects the additional bend- ing moment of the adjacent pile foundation. Under the influence of the grouting pressure, the additional axial force and additional bending moment of the pile foundation also follow the skewed normal distribution. The back analysis results of the pile foundation are greater than those of the typical numerical method by about 60% 100%, that is using the back analysis calculation results to evaluate the pile foundation additional response can reduce the risk.