Warianty tytułu
Determination of bentazone residue in environmental samples
Języki publikacji
Abstrakty
The aim of investigation was to elaborate an analytical method for determination of bentazone in soil, plant and water samples. The analytical procedure consists of three elementary processes: extraction and reextraction of analyzed substance from matrix, cleaning of extract using SPE (Solid Phase Extraction) column with Florisil active solid and final determination using gas chromatography with ECD and MS detection. The detection limit (LOD) of bentazone was 0.0002 mg/kg (for soil and plant samples) and 0.00005 mg/kg for water samples. The range of fortified recoveries of the method was 92–98%.
Słowa kluczowe
Wydawca
Czasopismo
Rocznik
Tom
Numer
Opis fizyczny
s.1910-1913,wykr.,bibliogr.
Twórcy
autor
- Zakład Herbologii i Technik Uprawy Roli, Instytut Uprawy Nawożenia i Gleboznawstwa – Państwowy Instytut Badawczy, ul.Orzechowa 61, 50-540 Wrocław
autor
autor
Bibliografia
- Aguilar C., Borrull F., Marce R.M. 1997. Determination of pesticides in environmental waters by solid–phase extraction and gas chromatography with electron–capture and mass spectrometry detection. J. Chromatography 771: 221–231.
- Cserhati T., Forgacs E., Deyl Z., Miksik I., Eckhardt A. 2004. Chromatographic determination of herbicide residues in various matrices. Biomed. Chromatogr. 18: 350–359.
- Hogendoorn E.A., Westhuis K., Dijkman E., Heusinkveld H.A.G., den Boer A.C., Evers E., Baumann R.A. 1999. Semi–permeable surface analytical reversed–phase column for the improved trace analysis of acidic pesticides in water with coupled–column reversed phase liguid chromatography with UV detection. Determination of bromoxynil and bentazone in surface water. J. Chromatography 858: 45–54.
- Ogierman L. 1990. Analysis of bentazone herbicide by formation of the methyl derivative in the gas–liquid chromatograph using trimethylanilinium hydroxide. Fresenius J. Anal. Chem. 336: 663–664.
- Peschka M., Petrovic M., Knepper T., Barcelo D. 2007. Determination of two phototransformation products of bentazone using quadrupole time–of–flight mass spectrometry. Anal. Bioanal. Chem. 388: 1227–1234.
- Thorstensen C.W., Christiansen A. 2001. Determination of bentazone, dichlorprop, and MCPA in different soils by sodium hydroxide extraction in combination with soil–phase preconcentration. J. Agric. Food Chem. 49 (9): 4199–4202.
Typ dokumentu
Bibliografia
Identyfikatory
Identyfikator YADDA
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