Analysis of chloramphenicol in drinking water using an evaporation preparative step and isotope dilution liquid chromatography–tandem mass spectrometry

• Autorzy: Li, Y. , Liu, X. , Zhang, R. , ZomPa, D. , Luo, P. , Tang, L. , Liu, X. , Zhou, Y. , Wen, S.
• Języki publikacji: EN

Abstrakty

EN

A reliable isotope dilution method for the determination of chloramphenicol (CAP) in drinking water was developed by using an evaporation preparative step. Each sample was monitored by ultrahigh-pressure liquid chromatography (UHPLC) coupled to tandem mass spectrometry (MS/MS) using an electrospray ionization interface (ESI) in negative ion modes. Recoveries of spiked samples were in the range from 93.2% to 95.7% with intra-day relative standard deviation lower than 6.7% and inter-day relative standard deviation lower than 8.2%. Limit of quantification (LOD) was 0.002 ng/mL. The developed method was successfully applied to the analysis of CAP in drinking water of Shannan region of Tibet.

Słowa kluczowe

EN

UHPLC–MS/MS; chloramphenicol; evaporation; isotope dilution; drinking water

• Czasopismo: Acta Chromatographica
• Rocznik: 2018
• Tom: Vol. 30, no. 1
• Strony: 17--20
• Opis fizyczny: Bibliogr. 31 poz., rys., tab.

Twórcy

autor

Li, Y.

• Hubei Provincial Key Laboratory for Applied Toxicology, Hubei Provincial Centre for Disease Control and Prevention, Wuhan, 430079, China

autor

Liu, X.

• Hubei Provincial Key Laboratory for Applied Toxicology, Hubei Provincial Centre for Disease Control and Prevention, Wuhan, 430079, China

autor

Zhang, R.

• Hubei Provincial Key Laboratory for Applied Toxicology, Hubei Provincial Centre for Disease Control and Prevention, Wuhan, 430079, China

autor

ZomPa, D.

• Shannan region Centre for Disease Control and Prevention, Shannan region of Tibet, 856000, China

autor

Luo, P.

• Hubei Provincial Key Laboratory for Applied Toxicology, Hubei Provincial Centre for Disease Control and Prevention, Wuhan, 430079, China

autor

Tang, L.

• Hubei Provincial Key Laboratory for Applied Toxicology, Hubei Provincial Centre for Disease Control and Prevention, Wuhan, 430079, China

autor

Liu, X.

• Hubei Provincial Key Laboratory for Applied Toxicology, Hubei Provincial Centre for Disease Control and Prevention, Wuhan, 430079, China

autor

Zhou, Y.

• Hubei Provincial Key Laboratory for Applied Toxicology, Hubei Provincial Centre for Disease Control and Prevention, Wuhan, 430079, China

autor

Wen, S.

• Hubei Provincial Key Laboratory for Applied Toxicology, Hubei Provincial Centre for Disease Control and Prevention, Wuhan, 430079, China,

Bibliografia

• [1] Yuan, M. ; Sheng, W. ; Zhang, Y. ; Wang, J. ; Yang, Y. ; Zhang, S. ; Goryacheva, I. Y. ; Wang, S. Anal. Chim. Acta. 2012, 751, 128.
• [2] Mbodi, F. E. ; Nguku, P. ; Okolocha, E. ; Kabir, J. Food Addit. Contam., Part A 2014, 31, 1834.
• [2] Nicolich R. S. ; Werneck-Barroso E. ; Marques M. A. S. Anal. Chim. Acta. 2006, 565, 97.
• [3] Rocha Siqueira, S. R. ; Luiz Donato, J. ; de Nucci, G. ; Reyes, F. G. J. Sep. Sci. 2009, 32, 4012.
• [4] Karaseva, N. A. ; Ermolaeva, T. N. Talanta 2012, 93, 44.
• [5] Kaufmann A. ; Butcher P. ; Maden K. ; Walker S. ; Widmer M. Anal. Chim. Acta. 2015, 862c, 41.
• [6] China M. GB5749-2006 2006.
• [7] Schets F. ; Nobel P. ; Strating S. ; Mooijman K. ; Engels G. ; Brouwer A. Lett. Appl. Microbiol. 2002, 34, 227.
• [8] Scortichini G. ; Annunziata L. ; Haouet M. N. ; Benedetti F. ; Krusteva I. ; Galarini R. Anal. Chim. Acta 2005, 535, 43.
• [9] Karaseva N. ; Ermolaeva T. Talanta 2012, 93, 44.
• [10] Ashwin H. M. ; Stead S. L. ; Taylor J. C. ; Startin J. R. ; Richmond S. F. ; Homer V. ; Bigwood T. ; Sharman M. Anal. Chim. Acta 2005, 529, 103.
• [11] Boyd, B. ; Björk, H. ; Billing, J. ; Shimelis, O. ; Axelsson, S. ; Leonora, M. ; Yilmaz, E. J. Chromatogr. A 2007, 1174, 63.
• [12] Akhtar M. H. ; Danis C. ; Sauve A. ; Barry C. J. Chromatogr. A 1995, 696, 123.
• [13] Rejtharová, M. ; Rejthar, L. J. Chromatogr. A 2009, 1216, 8246.
• [14] Han J. ; Wang Y. ; Yu C. ; Li C. ; Yan Y. ; Liu Y. ; Wang L. Anal. Chim. Acta. 2011, 685, 138.
• [15] Wang, L. ; Yang, H. ; Zhang, C. ; Mo, Y. ; Lu, X. Anal. Chim. Acta 2008, 619, 54.
• [16] Liu S. ; Wu X. Z. ; Gao Z. H. ; Jiao F. Analytical Methods 2013, 5, 1150.
• [17] Huang J.-F. ; Zhang H.-J. ; Feng Y.-Q. J. Agric. Food Chem. 2006, 54, 9279.
• [18] Hormazábal V. ; Yndestad M. J. Liq. Chromatogr. Relat. Technol. 2001, 24, 2477.
• [19] Kawano S.-i. ; Hao H.-Y. ; Hashi Y. ; Lin J.-M. Chinese Chemical Letters 2015.
• [20] Lu X. W. ; Dang Z. ; Yang C. Int. J. Environ. Sci. Technol. 2009, 6, 597.
• [21] Rocha Siqueira S. R. ; Luiz Donato J. ; de Nucci G. ; Reyes F. G. R. J. Sep. Sci. 2009, 32, 4012.
• [22] Rønning H. T. ; Einarsen K. ; Asp T. N. J. Chromatogr. A 2006, 1118, 226.
• [23] Aresta A. ; Bianchi D. ; Calvano C. D. ; Zambonin, Cg. J. Pharm. Biomed. Anal. 2010, 53, 440.
• [24] Chu S. ; Metcalfe C. D. ; Chem A. Anal. Chem. 2007, 79, 5093.
• [25] Xia, X. ; Wang, Y. ; Wang, X. ; Li, Y. ; Zhong, F. ; Li, X. ; Huang, Y. ; Ding, S. ; Shen, J. J. Chromatogr. A 2013, 1292, 96.
• [26] Cronly M. ; Behan P. ; Foley B. ; Malone E. ; Martin S. ; Doyle M. ; Regan L. Food Addit Contam Part A Chem Anal Control Expo Risk Assess 2010, 27, 1233.
• [27] Tajik, H. ; Malekinejad, H. ; Razavi-Rouhani, S. M. ; Pajouhi, M. R. ; Mahmoudi, R. ; Haghnazari, A. Food Chem. Toxicol. 2010, 48, 2464.
• [28] Forti A. F. ; Campana G. ; Simonella A. ; Multari M. ; Scortichini G. Anal. Chim. Acta 2005, 529, 257.
• [29] Hou X. ; Li Y. ; Cao S. ; Zhang Z. ; Wu Y. Chromatographia 2010, 71, 135.
• [30] Lee, S. ; Kim, B. ; Kim, J. J. Chromatogr. A 2013, 1277, 35.
• [31] Cervera M. ; Portolés T. ; López F. ; Beltrán J. ; Hernández F. Anal. Bioanal. Chem. 2014, 406, 6843.

Uwagi

PL

Opracowanie rekordu w ramach umowy 509/P-DUN/2018 ze środków MNiSW przeznaczonych na działalność upowszechniającą naukę (2018).

Identyfikatory

DOI

10.1556/1326.2017.28404