Influence of Gelation Temperature on the Properties of Sol-Gel-Derived Calcium Hydroxyapatite Ceramics

• Autorzy: Bogdanoviciene, I. , Tonsuaadu, K. , Kareiva, A.
• Języki publikacji: EN

Abstrakty

EN

An aqueous sol-gel chemistry synthesis route has been developed to prepare calcium hydroxyapatite (Ca10(PO4)6(OH)2, CHA) samples at different gelation temperatures. In the sol-gel processes, an aqueous solution of tartaric acid as complexing agent was used. The phase transformations, composition and micro-structural properties of the polycrystalline samples were studied by thermogravimetric analysis (TG), differential thermal analysis (DTA), energy-dispersive spectrometry (EDS), Fourier transform infrared spectroscopy (FTIR), X-ray powder diffraction analysis (XRD) and scanning electron microscopy (SEM). It was clearly demonstrated that temperature of initial stage of the preparation of CHA is a crucial parameter to obtain monophasic calcium hydroxy apatite powders with desired morphological properties.

Słowa kluczowe

EN

biomaterials; calcium hydroxyapatite; sol-gel preparation

• Czasopismo: Polish Journal of Chemistry
• Rocznik: 2009
• Tom: Vol. 83, nr 1
• Strony: 47-55
• Opis fizyczny: Bibliogr. 40 poz., rys.

Twórcy

autor

Bogdanoviciene, I.

autor

Tonsuaadu, K.

autor

Kareiva, A.

• 1Department of General and Inorganic Chemistry, Vilnius University, Naugarduko 24, LT-03225 Vilnius, Lithuania Tel.: [phone]; Fax: [phone],

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