Rapid and simultaneous determination of tetrabromobisphenol A and hexabromocyclododecane diastereoisomers in soil by matrix solid-phase dispersion with bamboo charcoal as dispersive adsorbent

• Autorzy: Yuan, J. P. , Cui, Z. J. , Cheng, C. G. , Wang, X. L. , Wang, S. S. , Song, X. L. , Li, F. W.
• Języki publikacji: EN

Abstrakty

EN

A rapid and simple analytical method based on matrix solid-phase dispersion combined with liquid chromatography coupled with tandem mass spectrometry has been developed by using bamboo charcoal as a dispersive adsorbent to simultaneously determine tetrabromobisphenol A (TBBPA) and hexabromocyclododecane diastereoisomers (HBCDs) in soil. The factors influencing the performance of the proposed method were investigated and optimized in detail, and the matrix effects were evaluated. Under optimum conditions, the proposed method showed good linearity within the range of 0.8–80 ng g−1 and limits of detection of 4–75 pg g−1 (S/N = 3). The satisfactory recoveries of TBBPA ranging from 72.8% to 92.5% and HBCDs ranging from 76.8% to 102.2% were obtained with relatively standard deviation (RSD) ranging from 3.4% to 9.8%. The proposed method has been successfully applied to analyze TBBPA and HBCDs in actual soil samples from the Yellow River Delta in China.

Słowa kluczowe

EN

Tetrabromobisphenol A; hexabromocyclododecane diastereoisomers; matrix solid-phase dispersion; bamboo charcoal; soil

• Czasopismo: Acta Chromatographica
• Rocznik: 2017
• Tom: Vol. 29, no. 4
• Strony: 487--492
• Opis fizyczny: Bibliogr. 38 poz., rys., tab.

Twórcy

autor

Yuan, J. P.

• Shandong Provincial Key Laboratory of Applied Technology of Sophisticated Analytical Instruments, Analysis and Test Center, Shandong Academy of Sciences, Jinan 250014, China,
• School of Environmental Science and Engineering, Shandong University, Jinan 250100, China

autor

Cui, Z. J.

• School of Environmental Science and Engineering, Shandong University, Jinan 250100, China

autor

Cheng, C. G.

• Shandong Provincial Key Laboratory of Applied Technology of Sophisticated Analytical Instruments, Analysis and Test Center, Shandong Academy of Sciences, Jinan 250014, China

autor

Wang, X. L.

• Shandong Provincial Key Laboratory of Applied Technology of Sophisticated Analytical Instruments, Analysis and Test Center, Shandong Academy of Sciences, Jinan 250014, China

autor

Wang, S. S.

• Shandong Provincial Key Laboratory of Applied Technology of Sophisticated Analytical Instruments, Analysis and Test Center, Shandong Academy of Sciences, Jinan 250014, China

autor

Song, X. L.

• Shandong Provincial Key Laboratory of Applied Technology of Sophisticated Analytical Instruments, Analysis and Test Center, Shandong Academy of Sciences, Jinan 250014, China

autor

Li, F. W.

• Shandong Provincial Key Laboratory of Applied Technology of Sophisticated Analytical Instruments, Analysis and Test Center, Shandong Academy of Sciences, Jinan 250014, China,

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Uwagi

PL

Opracowanie rekordu w ramach umowy 509/P-DUN/2018 ze środków MNiSW przeznaczonych na działalność upowszechniającą naukę (2018).

Identyfikatory

DOI

10.1556/1326.2016.00122