Czasopismo
2011
|
Vol. 23, no. 2
|
205--213
Tytuł artykułu
Autorzy
Wybrane pełne teksty z tego czasopisma
Warianty tytułu
Języki publikacji
Abstrakty
A rapid and sensitive high-performance liquid chromatographic method has been developed and validated for the simultaneous determination and quantification of cephalosporins (cefpirome, cefaclor, ceftazidime, and cephradine) in pharmaceutical formulations. Separation was achieved in the presence of caffeine as internal standard on a Mediterranea C18 (5 μm, 25 × 0.46 mm) column. The mobile phase was composed of methanol and water (30:70), which was pumped at a flow rate of 1 mL min-1. Effluents were monitored at 265 nm. The assay was linear in the concentration range of 0.5–50 μg mL -1, with the correlation coefficient (r2) greater than 0.9998. The intra-day and inter-day coefficients of variation (CV %) were less than 4% at different concentrations.
Słowa kluczowe
Czasopismo
Rocznik
Tom
Strony
205--213
Opis fizyczny
Bibliogr. 32 poz., rys., tab.
Twórcy
autor
- University of Karachi Department of Chemistry Karachi 75270 Pakistan, nawwaz@gmail.com
autor
- University of Karachi Department of Chemistry Karachi 75270 Pakistan
autor
- University of Karachi Department of Pharmaceutical Chemistry, Faculty of Pharmacy, Research Institute of Pharmaceutical Sciences Karachi 75270 Pakistan
Bibliografia
- [1] Wilson, and Gisvold’s Textbook of Organic and Medicinal and Pharmaceutical Chemistry, 11th edn., J.B Lippincott Company, Philadelphia, PA, 2004, p. 319
- [2] G. Alfred and L.S. Gilman, The Pharmacological Basis of Therapeutics, 9th edn., McGraw-Hill, New York, 1996, 1089
- [3] L.A. Danzer. Clin. Chem., 29, 856 (1983)
- [4] S.A. Patel, N.M. Patel, and M.M. Patel. Indian J. Pharm. Sci., 68, 278 (2006)
- [5] G.A. Saleh, H.F. Askal, I.A. Darwish, and A.-N.A. El-Shorbagi. Anal. Sci., 19, 281 (2003)
- [6] G.A. Saleh, H.F. Askal, M.F. Radwan, and M.A. Omar. Talanta, 54, 1205 (2001)
- [7] M.M. Ayad, A.A. Shalaby, H.E. Abdellatef, and H.M. Elsaid. J. Pharm. Biomed. Anal., 18, 975 (1999)
- [8] M.S. Arayne, N. Sultana, and M. Nawaz. J. Anal. Chem., 63, 881 (2008)
- [9] V.F. Samanidou, E.D. Tsochatzis, and I.N. Papadoyannis. Microchim. Acta, 160, 471 (2008)
- [10] R.V. Oliveira, A.C. De Pietro, and Q.B. Cass. Talanta, 71, 1233 (2007)
- [11] P. Hwai-Tzong, K. Pramila, L. Josephine, and L. Chin-Chung. J. Pharm. Sci., 81, 663 (2006)
- [12] P.M. Baranowska and J. Baranowski. Anal. Chim. Acta, 570, 46 (2006)
- [13] N.O. Can, G. Altiokka, and H.Y. Aboul-Enein. Anal. Chim. Acta, 576, 246 (2006)
- [14] V.O. Regina and B.C. Quezia. Agric. Food Chem., 54, 1180 (2006)
- [15] M. de Diego Glaría, G.G. Moscciati, and R.G. Ramos. J. AOAC Int., 88, 436 (2005)
- [16] V.F. Samanidou, A.S. Ioannou, and I.N. Papadoyannis. J. Chromatogr. B, 809, 175 (2004)
- [17] M. Becker, E. Zittlau, and M. Petz. Anal. Chim. Acta, 520, 19 (2004)
- [18] L.I. Sokolova and A.P. Chernyaev. Pharm. Chem. J., 36, 263 (2002)
- [19] S. Al-Rawithi, R. Hussein, D.A. Raines, I. Al-Showaier, and W. Kurdi. J. Pharm. Biomed. Anal., 22, 281 (2000)
- [20] A. Shalaby. J. Liquid Chromatogr. Relat. Technol., 21, 3161 (1998)
- [21] F. Pehourcq and C. Jarry. J. Chromatogr. A, 812, 159 (1998)
- [22] A.S. Steven, M.F. Thomas, and S. James. Antimicrob. Agents Chemother., 26, 652 (1984)
- [23] J.B. Lecaillon, M.C. Rouan, C. Souppart, M. Febvre, and F. Juge. J. Chromatogr., 228, 257 (1982)
- [24] J.C. Rotschafer, K.B. Crossley, T.S. Lesar, D. Zaske, and K. Miller. Antimicrob. Agents Chemother., 21, 170 (1982)
- [25] A.M. Brisson and J.B. Fourtillan. J. Chromatogr., 223, 393 (1981)
- [26] Nilsaon-Ehle, I.T. Yoshikama, M.C. Schotz, and L.B. Guze. Antimicrob. Agents Chemother., 13, 221 (1978)
- [27] J.S. Wold and S.A. Turnipseed. Clin. Chim. Acta., 78, 203 (1978)
- [28] T. Nakagawa, J. Haginaka, K. Yamaoka, and T. Uno. J. Antibiot., 31, 769 (1978)
- [29] N.S. Aziz, J.G. Gambertoglio, E.T Lin, H. Grausz, and Z L. Benet. J. Pharmacokinet. Biopharm., 6, 153 (1978)
- [30] J.P. Anhalt and T.P. Moyer. Lab. Med., 11, 797 (1980)
- [31] Nilsson-Ehle. Acta Pathol. Microbiol. Scand., 259, 61 (1977)
- [32] T. Yoshikawa, S.K. Maitra, M.C. Schotz, and L.B. Guze. Rev. Infect. Dis., 26, 169 (1980)
Typ dokumentu
Bibliografia
Identyfikatory
Identyfikator YADDA
bwmeta1.element.baztech-7ccfb67a-1cac-409c-9860-a480baa000c7