Synthesis of NiO nanoparticles by sol-gel technique

• Autorzy: Kayani, Z. N. , Butt, M. Z. , Riaz, S. , Naseem, S.
• Języki publikacji: EN

Abstrakty

EN

NiO nanoparticles were fabricated by sol-gel route using ammonium hydroxide and nickel nitrate as precursors. The NiO nanoparticles were calcinated at 400 °C and 1000 °C. The nanoparticles were characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), vibrating sample magnetometer (VSM), thermogravimetry analysis/differential thermal analysis (TGA/DTA). The structural properties were evaluated by X-ray diffraction (XRD). XRD confirmed the formation of well-crystallized and high purity NiO phase. The XRD showed that the peaks were sharpened and the crystallite size increased as the calcination temperature increased. The average crystallite size ranged from 12 nm to 20 nm, when calcined at temperatures 400 °C and 1000 °C, respectively. Fourier transform infrared spectroscopy (FT-IR) revealed the chemical composition and confirmed the formation of NiO nanoparticles. The nanoparticles showed paramagnetic behavior.

Słowa kluczowe

EN

NiO; nanoparticles; calcination; crystallite size; FT-IR

• Czasopismo: Materials Science Poland
• Rocznik: 2018
• Tom: Vol. 36, No. 4
• Strony: 547--552
• Opis fizyczny: Bibliogr. 36 poz., rys., tab.

Twórcy

autor

Kayani, Z. N.

• Physics Department, Lahore College for Women University, Lahore-54000, Pakistan,

autor

Butt, M. Z.

• Physics Department, Lahore College for Women University, Lahore-54000, Pakistan

autor

Riaz, S.

• Center for Solid State Physics, University of the Punjab, Lahore-54590, Pakistan

autor

Naseem, S.

• Center for Solid State Physics, University of the Punjab, Lahore-54590, Pakistan

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Uwagi

PL

Opracowanie rekordu w ramach umowy 509/P-DUN/2018 ze środków MNiSW przeznaczonych na działalność upowszechniającą naukę (2019).

Identyfikatory

DOI

10.2478/msp-2018-0088