A facile thermal decomposition route to synthesise CoFe2O4 nanostructures

• Autorzy: Kalpanadevi, K. , Sinduja, C. R. , Manimekalai, R.
• Języki publikacji: EN

Abstrakty

EN

The synthesis of CoFe2O4 nanoparticles has been achieved by a simple thermal decomposition method from an inorganic precursor, cobalt ferrous cinnamate hydrazinate (CoFe2(cin)3(N2H4)3) which was obtained by a novel precipitation method from the corresponding metal salts, cinnamic acid and hydrazine hydrate. The precursor was characterized by hydrazine and metal analyses, infrared spectral analysis and thermo gravimetric analysis. Under appropriate annealing, CoFe2(cin)3(N2H4)3 yielded CoFe2O4 nanoparticles, which were characterized for their size and structure using X-Ray diffraction (XRD), high resolution transmission electron microscopic (HRTEM), selected area electron diffraction (SAED) and scanning electron microscopic (SEM) techniques.

Słowa kluczowe

EN

CoFe2O4 nanoparticles; XRD; HRTEM; SAED; SEM

• Czasopismo: Materials Science Poland
• Rocznik: 2014
• Tom: Vol. 32, No. 1
• Strony: 34--38
• Opis fizyczny: Bibliogr. 15 poz., rys., wykr.

Twórcy

autor

Kalpanadevi, K.

• Department of Chemistry, Kongunadu Arts and Science College, Coimbatore, Tamilnadu, India, PIN – 641 029

autor

Sinduja, C. R.

• Department of Chemistry, Kongunadu Arts and Science College, Coimbatore, Tamilnadu, India, PIN – 641 029

autor

Manimekalai, R.

• Department of Chemistry, Kongunadu Arts and Science College, Coimbatore, Tamilnadu, India, PIN – 641 029,

Bibliografia

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Identyfikatory

DOI

10.2478/s13536-013-0153-1