Application of ionic liquid-based ultrasonic-assisted extraction followed by rapid resolution LC-ESI/MS to chromone analysis from radix saposhnikoviae

• Autorzy: Han, Z. , Xu, M. , Wang, Y. , Yang, L. , Han, M.
• Języki publikacji: EN

Abstrakty

EN

Ionic liquid-based ultrasonic-assisted extraction (ILUAE) was successfully applied to the extraction of the four chromones (prim-O-glucosylcimifugin, cimifugin, 5-O-methylvisammioside, and sec-O-glucosylhamaudol) from Saposhnikovia divaricata (Radix Saposhnikoviae) for the first time. A series of l-alkyl-3-methylimidazolium ILs differing in anion and cation compositions was evaluated for extraction efficiency, and [C3MIM]Br was selected as the optimal solvent. In addition, ultrasound extraction parameters were optimized, and the chromones were directly quantified and analyzed by rapid resolution liquid chromatography-electrospray ionization/mass spectrometry (RRLC-ESI/MS). The optimal conditions were as follows: 0.4 M concentration of [C3MIM]Br, 20:1 solvent to solid ratio, and ultrasonic time, temperature, and frequency of 5 min, 40 °C, and 50 kHz, respectively. This approach obtained the highest extraction yield of 10.188 ± 0.473 mg g−1 for total chromones. Compared with regular UAE, the proposed approach exhibited a higher efficiency (61.56% increase) and shorter extraction time (nine times shorter). Also, ILUAE was an efficient, rapid, and simple sample preparation technique for extraction of chromones, and the established RRLC-DAD method could serve as a rapid and effective technique for extracting chromones from Radix Saposhnikoviae.

Słowa kluczowe

EN

Saposhnikovia divaricata; chromones; ionic liquids; ultrasonic-assisted extraction

• Czasopismo: Acta Chromatographica
• Rocznik: 2017
• Tom: Vol. 29, no. 3
• Strony: 359--374
• Opis fizyczny: Bibliogr. 39 poz., rys.

Twórcy

autor

Han, Z.

• College of Chinese Medicinal Materials, Jilin Agricultural University, Changchun, 130118, PR China

autor

Xu, M.

• College of Chinese Medicinal Materials, Jilin Agricultural University, Changchun, 130118, PR China

autor

Wang, Y.

• College of Chinese Medicinal Materials, Jilin Agricultural University, Changchun, 130118, PR China

autor

Yang, L.

• College of Chinese Medicinal Materials, Jilin Agricultural University, Changchun, 130118, PR China

autor

Han, M.

• College of Chinese Medicinal Materials, Jilin Agricultural University, Changchun, 130118, PR China

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Uwagi

PL

Opracowanie ze środków MNiSW w ramach umowy 812/P-DUN/2016 na działalność upowszechniającą naukę (zadania 2017).

Identyfikatory

DOI

10.1556/1326.2017.29.3.06