Nowa wersja platformy, zawierająca wyłącznie zasoby pełnotekstowe, jest już dostępna.
Przejdź na https://bibliotekanauki.pl

PL EN


Preferencje help
Widoczny [Schowaj] Abstrakt
Liczba wyników
2006 | 15 | 5 | 677-690
Tytuł artykułu

Solid phase extraction technique-trends, opportunities and applications

Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Solid phase extraction (SPE) is an extraction method that uses a solid phase and a liquid phase to isolate one, or one type, of analyte from a solution. It is usually used to clean up a sample before us­ing a chromatographic or other analytical method to quantify the amount of analyte(s) in the sample. The general procedure is to load a solution onto the SPE phase, wash away undesired components, and then wash off the desired analytes with another solvent into a collection tube. Solid-phase extrac­tions use the same type of stationary phases as are used in liquid chromatography columns. The sta­tionary phase is contained in a glass or plastic column above a frit or glass wool. The column might have a frit on top of the stationary phase and might also have a stopcock to control the flow of solvent through the column. Commercial SPE cartridges have 1-10 ml capacities and are discarded after use. It is usually used to clean up a sample before using a chromatographic or other analytical method to quan­tify the amount of analyte(s) in the sample. Solid phase extraction procedures are used not only to extract traces of organic compounds from environmental samples but also to remove the interfering components of the complex matrices in order to obtain a cleaner extract containing the analytes of interest. The SPE technique is widely applied for isolation of analytes from a liquid matrix and purified extracts. This paper is a review of the literature regarding general information about SPE technique, new trends in SPE technique and its application.
Słowa kluczowe
Wydawca
-
Rocznik
Tom
15
Numer
5
Strony
677-690
Opis fizyczny
p.677-690,fig.,ref.
Twórcy
  • Gdansk University of Technology, 11/12 Gabriela Narutowicza Str., 80-952 Gdansk, Poland
autor
Bibliografia
  • 1. BIZIUK M., Pesticides, occurrence, determination, and dis­posal. WNT: Warsaw 2001 (In Polish).
  • 2. RAWA-ADKONIS M., WOLSKA L., NAMIESNIK J. Modern techniques of extraction of organic from environ­mental matrices. Critic. Rev. Anal. Chem. 33, 199, 2003.
  • 3. CAMEL V. Solid phase extraction of trace elements. Spectrochimica Acta B 58, 1177, 2003.
  • 4. Supelco Bulletin, Sigma-Aldrich Co 910, 1998.
  • 5. FONT G., MANES J., MOLTO J.C., PICO Y. Solid-phase extraction in multi-residue pesticide analysis of water. J. Chromatogr. A 642, 135, 1993.
  • 6. SABIK H., JEANNOT R., RONDEAU B. Multiresidue methods using solid phase extraction techniques for monitor­ing priority pesticides, including triazines and degradation products, in ground water. J. Chromatogr. A 885, 217, 2000.
  • 7. FRITZ J. S., Analytical Solid-Phase Extraction, Villey- VCH: New York 1999
  • 8. FARID A. E. Trends Anal. Chem. 20, 649, 2001
  • 9. HENNION M.C., Solid-phase extraction: method develop­ment, sorbents, and coupling with liquid chromatography. J Chromatogr. A 856, 3, 1999.
  • 10. MASQUE N., MARCE R.M., BORRULL, F. New poly­meric and other types of sorbents for solid-phase extraction of polar organic micropollutants from environmental water. Trends Anal. Chem. 6, 384, 1998.
  • 11. TYSZKIEWICZ H., BIZIUK M., HÜPKA J., ZALESKA A. Determination of organochlorine pesticides in water suspen­sion by means of liquid-liquid extraction, solid phase extrac­tion, solid phase microextraction and direct aqueous injec­tion. Chem. Inz. Ekol. 8, 935, 2001.
  • 12. FERRER I., BARCELO D. Validation of new solid-phase extraction materials for the selective enrichment of organic contaminants from environmental samples. Trend Anal. Chem. 3, 180, 1999.
  • 13. MAJORS R.E. Trends in sample preparation. LC-GC Eu­rope 19, 2, 2001.
  • 14. WELLS D. A. Solid-phase extraction of acidic herbicides. LC-GC 17, 600, 1999.
  • 15. YÜ J., WU C., XING J. Development of new solid-phase microextraction fibers by sol-gel technology for the deter­mination of organophosphorus pesticide multiresidues in food. J. Chromatogr. A 1036, 101, 2004.
  • 16. LINGEMAN H., HOEKSTRA-OUSSOREN S. J. F. Par­ticle-loaded membranes for sample concentration and/or clean up in bioanalysis. J. Chromatogr. A 689, 221, 1997.
  • 17. POOLE F.C. New trends in solid-phase extraction. Trends Anal. Chem. 22, 362, 2003.
  • 18. FRANKIE J. P., ZEEUW R.A. Solid-phase extraction pro­cedures in systematic toxicological analysis. J. Chromatogr. A 713, 51, 1998.
  • 19. CHAI A., KUET L., SENG L. Solid phase extraction clean­up for the determination of organochlorine pesticides in veg­etables. Malaysian J. Chem. 6, 39, 2004.
  • 20. PICHON V. Solid-phase extraction for multiresidue analysis of organic contaminants in water. J. Chromatogr. A 885, 195, 2000.
  • 21. HENNION M.C. Graphitized carbons for solid-phase ex­traction. J. Chromatogr. A 885, 73, 2000.
  • 22. MATISOVA E., KAKALIKOVA L., LESKO J., DE ZEEUW J. Application of porous carbon for solid-phase extraction of dicarboxyimide fungicide residues from wines in combina­tion with high-resolution capillary gas chromatography and gas chromatography-mass spectrometry. J. Chromatogr. A 754, 445, 1996.
  • 23. PICHON V., CHEN L., HENNION M.C., DANIEL R., MARTEL A., LE GOFFIC F., ABIÁN J., BARCELó D. Preparation and evaluation of immunosorbents for selective trace enrichment of phenylurea and triazine herbicides in en­vironmental waters. Anal. Chem. 67, 2451, 1995.
  • 24. MARTIN-ESTEBAN A., FERNÁNDEZ P., STEVENSON D., CÁMARA C. Mixed immunosorbent for selective on­line trace enrichment and liquid chromatography of phenyl- urea herbicides in environmental waters. Analyst 122, 1113, 1997.
  • 25. FERRER I., PICHON V., HENNION M.C., BARCELó D. New polymeric and other types of sorbents for solid - phase extraction of polar organics micropollutants from environ­mental water. J. Chromatogr A. 777, 91. 1997.
  • 26. ENSING K., BERGGREN CH., MAJORS R.E. Selective sorbents for solid-phase extraction based on molecularly im­printed polymers. LC-GC North America 19, 942, 2002.
  • 27. WELLS D. A. Accessory products for SPE using 96-well plates. LC-GC 17, 808, 1999.
  • 28. MOTTALEB M.A., ABEDIN M.Z. Determination of chlo­rinated pesticides in soil by solid phase extraction-gas chro­matography. Anal. Sci. 15, 283, 1999.
  • 29. STAJNBAHER D., ZUPANCIC-KRALJ L. Multiresidue method for determination of 90 pesticides in fresh fruit and vegetables using solid-phase extraction and gas chroma- tography/mass spectrometry. J. Chromatogr. A 1015, 185, 2003.
  • 30. BURKE E.R., HOLDEN A.J., SHAW I.C. A method to de­termine residue levels of persistent organochlorine pesti­cides in human milk from Indonesian women. Chemosphere 50, 529, 2003.
  • 31. FOCANT J. F., PAUW E. D. Fast automated extraction and clean-up of biological fluids for polychlorinated dibenzo-/>- dioxins, dibenzofurans and coplanar polychlorinated biphe- nyls analysis. J. Chromatogr. B 776, 199, 2002.
  • 32. KITAMURA K., MOCHIZUKI A., CHOI J. W., TAKAZA- WA Y., HASHIMOTO S., ITO Y., FUJIMINE Y., MORITA M. Optimization of a method for determining dioxin in whole blood samples based on solvent extraction and sim­plified cleanup. Analyst 129, 315, 2004.
  • 33. WESTBOM R., THORNEBY L., ZORITA S., MATHIAS- SON L., BJORKLUND E. J. Development of a solid-phase extraction method for the determination of polychlorinated biphenyls in water. J. Chromatogr. A 1033, 1, 2004.
  • 34. HOPPER M. Automated one-step supercritical fluid extrac­tion and clean-up system for the analysis of pesticide resi­dues in fatty matrices. J. Chromatogr. A 840, 93, 1999.
  • 35. PIHLSTROM T., OSTERDAHL B. G. Analysis of pesticide residues in fruit and vegetables after cleanup with solid­phase extraction using ENV+ (Polystyrene-divinylbenzene) cartridges. J. Agric. Food Chem. 47, 2549, 1999.
  • 36. COLUME A., CARDENAS S., GALLEGO M., VALCAR- CEL M. A solid phase extraction method for the screening and determination of pyrethroid metabolites and organo- chlorine pesticides in human urine. Rapid Communications In Mass Spectrometry 15, 2007, 2001.
  • 37. HENGEL M.J., SHIBAMOTO T. Gas chromatographic - mass spectrometric method for the analysis of dimethomorph fungicide in dried hops. J Agric. Food Chem. 48, 5824, 2000.
  • 38. MANIRAKIZA P., COVACI A., SCHEPENS P. Single step clean up and GC-MS quantification of organochlorine pesticide residues in spice powder. Chromatographia 52, 787, 2000.
  • 39. RAMOS L., ELJARRAT E., HERNANDEZ L. M., RIVERA J., GONZALEZ M. J. Comparative study of methodologies for the analysis of PCDDs and PDCFs in powdered full-fat milk, PCB, PCDD and PCDF levels in commercial samples from Spain. Chemosphere 38, 2577, 1999.
  • 40. ESKILSSON S. C., BJORKLUND E. Analytical-scale micro­wave-assisted extraction. J. Chromatogr A. 902, 227, 2000.
  • 41. DĄBROWSKA H., DĄBROWSKI Ł., BIZIUK M., GACA J., NAMIEśNIK J. Solid-phase extraction clean-up of soil and sediment extracts for the determination of various types of pollutants in single run. J. Chromatogr. A 1003, 29, 2003.
  • 42. WIGFIELD Y. Y., SELWYN J., KHAN S., MCDOWELL R. Comparison of supercritical fluid extraction and solvent ex­traction of twenty-two organochlorine pesticides from eggs. Chemosphere 32, 841, 1996.
  • 43. JUNKER-BUCHHEIT A., WITZENBACHER M. Pesticide monitoring of drinking water with the help of solid-phase extraction and high-performance liquid chromatography. J. Chromatogr. A 737, 67, 1996.
  • 44. LAWRENCE J. F., MENARD C., HENNION C., PICHON V, LEGOFFIC F., DURAND N. Evaluation of immunoaffinity chromatography as a replacement for organic solvent clean-up of plant extracts for the determination of triazine herbicides by liquid chromatography. J. Chromatogr. A 752, 147, 1996.
  • 45. POLESE L., SANNOMIYA M., SANDER A. P. Extraction and clean-up procedure for analysis of organochlorine pesticide residues in ethoxylated lanolin. Il Farmaco 9-10, 637, 2000.
  • 46. KIM Y., YANG, H., YOUNG L. S., KIM M. Levels of PCDDs and PCDFs in two kinds of fast foods in Korea. Chemosphere 43, 851, 2001.
  • 47. ROSSI S., DALPERO A. P., GHINI S., COLOMBO R., SABATINI A. G., GIROTTI S. Multiresidual method for the gas chromatographic analysis of pesticides in honeybees cleaned by gel permeation chromatography. J. Chromatogr. A 905, 223, 2001.
  • 48. SCHENCK F. J. Determination of organochlorine and or- ganophosphorus pesticide residues in eggs using a solid phase extraction clean up. J. Agric. Food Chem. 12, 6412, 2000.
  • 49. MORELLI-CARDOSO W. M. H., CARDOSO R. T. M., MELLO J. L., ABRANTES S., MENEZES K. M. P. Extrac­tion and clean up method for the determination of twenty or­ganochlorine pesticides residues in tomatoes by GLC-ECD. J. High Resol. Chromatogr. 22, 619, 1999.
  • 50. TORRES C.M., PICO Y., MANES J. Comparision of oc- tadecylsilica and graphitized carbon black as material for solid-phase extraction of fungicide and insecticide residues from fruit and vegetables. J. Chromatogr. A 778, 127, 1997.
  • 51. PLANAS C., SAULO J., CAIXACH J. Automated solid­phase extraction of priority and suspected endocrine disrupt­ing pesticides and metabolites. Organohalogen compounds, sampling, clean up and separation 66, 126, 2004.
  • 52. DOONG R.A., LEE C.Y. Determination of organochlorine pesticide residues in foods using solid-phase extraction clean-up cartridges. Analyst 124, 1287, 1999.
  • 53. BENEY P. J., BREUER G. M., JACOBS G. H, LARABEE - ZIERATH D. Review, evaluation, and application of solid phase extraction methods. Hotline Solid Phase Extraction 6, 1, 1996.
  • 54. HIROTAKA O., KAZUHIKO A., MASAHIRO O., SHI- HJIRO H. Multiresidue analysis of pesticides in vegetables and fruits using two-layered column with graphitized carbon and water absorbent polymer. Analyst 126, 1529, 2001.
  • 55. MUCCIO A., GENERALI T., BARBINI D.A., PELOSI P., AUSILI A., VERGORI F., GIROLIMETTI S. A new sample clean-up procedure based on ion-pairing on RP-SPE cartridges, for the determination of ionizable pesticides. J. Chromatogr. A 765, 61, 1997.
  • 56. FONT G., MANES J., MOLTO J.C., PICO Y. Solid phase extraction in multi-residue pesticide analysis of water. J. Chromatogr A 642, 135, 1993.
  • 57. AQUILAR C., BORRULL F., MARCE R. M. Determina­tion of pesticides in environmental waters by solid-phase ex­traction and gas chromatography with electron-capture and mass spectrometry detection. J. Chromatogr. A 771, 221, 1997.
  • 58. LECHOTAY S. J., VALVERDE-GARCIA A. Evaluation of different solid-phase traps for automated collection and clean-up in the analysis of multiple pesticides in fruits and vegetables after supercritical fluid extraction. J. Chromatogr. A 765, 69, 1997.
  • 59. KEVIN N. T. N., SEAN H. W. P. Supercritical fluid extrac­tion and quantitative determination of organophosphorus pesticide residues in wheat and maize using gas chromatog- raphy with flame photometric and mass spectrometric detec­tion. J Chromatogr. A 907, 247, 2001.
  • 60. SCHACHTERLE S., FEIGEL C. Pesticide residue analysis in fresh produce by gas chromatography-tandem mass spec­trometry. J. Chromatogr. A 754, 411, 1996.
  • 61. MARTÍNEZ E., PAZOS M., CARRO A., LLOMPART M., CELA R. Residues and trace elements - application of stra­tegically designed sample composition to the rapid analyti­cal screening of milk samples for polychlor. J. AOAC Intern. 86, 846, 2003.
  • 62. REDONDO M. J., RUIZ M. J., BOLUDA R., FONT G. Optimization of a solid-phase extraction technique for the extraction of pesticides from soil samples. J. Chromatogr. A 719, 69, 1996.
  • 63. SCHENK F. J., LECHOTAY S. J., VEGA V. Comparison of solid-phase extraction sorbents for cleanup in pesticide residue analysis of fresh fruits and vegetables. J. Sep. Sci. 25, 883, 2002.
  • 64. JUAN C. Y., THOMAS G. O., SEMPLE K. T., JONES K.C. Methods for the analysis of PCBs in human food, faeces and serum. Chemosphere 9, 1467, 1999.
  • 65. SPORRING S., BJORKLUND E. Selective pressurized liquid extraction of polychlorinated biphenyls from fat-con­taining food and feed samples Influence of cell dimensions, solvent type, temperature and flush volume. J. Chromatogr. A 1040, 155, 2004.
  • 66. MULLER A., BJORKLUND E, VON HOLST CH. On-line of pressurized liquid extracts for the determination of poly- chlorinated biphenyls in feedingstuffs and food matrices us­ing gas chromatography-mass spectrometry. J. Chromatogr. A 925, 197, 2001.
  • 67. Application Note ASE 322. Dionex: Sunnyvale CA 1996. Żwir-Ferenc A., BiziukM.
  • 68. GóMEZ-ARIZA J. L., BUJALANCE M., GIRÁLDEZ I., VELASCO A., MORALES E. Determination of polychlo- rinated biphenyls in biota samples using simultaneous pres­surized liquid extraction and purification. J. Chromatogr. A 946, 209, 2002.
Typ dokumentu
Bibliografia
Identyfikatory
Identyfikator YADDA
bwmeta1.element.agro-article-be686895-5818-4a25-af06-6401f19de136
JavaScript jest wyłączony w Twojej przeglądarce internetowej. Włącz go, a następnie odśwież stronę, aby móc w pełni z niej korzystać.