Application of the design of experiments in the epoxidation process of 1,5,9-cyclododecatriene

• Autorzy: Grzegorz Lewandowski , Jan Ćwirko
• Języki publikacji: EN

Abstrakty

EN

An influence of the molar ratio of cis, trans, trans-1,5,9-cyclododecatriene to tert-butyl hydroperoxide, the concentration of the catalyst and the reaction time on the performance of the epoxidation process of cis, trans, trans-1,5,9-cyclodecatriene with tert-butyl hydroperoxide at the presence of molybdenum hexacarbonyl Mo(CO)6 was examined. Examinations were performed using statistical methods of the design of experiments. A mathematical model describing the influence of the parameters on conversion cis, trans, trans-1,5,9-cyclododecatriene was obtained. An analysis of the data and rests was performed and an optimal value of conversion of cis, trans, trans-1,5,9-cyclododecatriene was established.

Słowa kluczowe

EN

epoxidation; design of experiments; 1,5,9-cyclododecatriene; optimization

• Czasopismo: Polish Journal of Chemical Technology
• Rocznik: 2007
• Tom: 9
• Numer: 4
• Strony: 68-71

Daty

wydano

2007-12-01

online

2008-01-30

Twórcy

autor

Grzegorz Lewandowski

• Institute of Organic Chemical Technology, Szczecin University of Technology, ul. Pułaskiego 10, 70-322 Szczecin, Poland

autor

Jan Ćwirko

• Institute of Organic Chemical Technology, Szczecin University of Technology, ul. Pułaskiego 10, 70-322 Szczecin, Poland

Bibliografia

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• ---
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Identyfikatory

DOI

10.2478/v10026-007-0093-9