Qualitative and quantitative analysis of gallic acid in Alchemilla vulgaris, Allium ursinum, Acorus calamus and Solidago virga-aurea by chip-electrospray ionization mass spectrometry and high performance liquid chromatography

• Autorzy: Dumitru Condrat , Cristina Mosoarca , Alina Zamfir , Florin Crişan , Maria Szabo , Alfa Lupea
• Języki publikacji: EN

Abstrakty

EN

This study presents the results obtained from qualitative and quantitative analysis of gallic acid from hydro-alcoholic extracts (methanol, ethanol) of plants from Plantae regnum. Plant qualitative analysis was performed using a novel mass spectrometric (MS) method based on fully automated chip-nanoelectrospray ionization (nanoESI) high capacity ion trap (HCT) while quantitative analysis was carried out by high performance liquid chromatography (HPLC). These methods were applied to Alchemilla vulgaris - common lady’s-mantle (aerial part), Allium ursinum - bear’s garlic (leaves), Acorus calamus - common sweet flag (roots), Solidago virga-aurea - goldenrod (aerial part). Obtained results indicated that methanol extracts (96%, 80%) have a gallic acid content ranging between 0.0011–0.0576 mg mL−1 extract while the ethanol extracts (96%, 60%) exhibit a gallic acid concentration that varies between 0.0010–0.0182 mg mL−1 extract. [...]

Słowa kluczowe

EN

Gallic acid; HPLC; Chip-ESI MS; Hydro-alcoholic extracts; Plantae

• Czasopismo: Open Chemistry
• Rocznik: 2010
• Tom: 8
• Numer: 3
• Strony: 530-535

Daty

wydano

2010-06-01

online

2010-04-25

Twórcy

autor

Dumitru Condrat

• Department of Chemical and Biological Sciences, Aurel Vlaicu University, Arad, 310330, Romania

autor

Cristina Mosoarca

• National Institute for Research and Development in Electrochemistry and Condensed Matter, Timisoara, 300224, Romania,

autor

Alina Zamfir

autor

Florin Crişan

• County Lab for Pesticides Quality Control, Arad, 310059, Romania

autor

Maria Szabo

• Department of Chemical and Biological Sciences, Aurel Vlaicu University, Arad, 310330, Romania

autor

Alfa Lupea

• Faculty of Industrial Chemistry and Environmental Engineering, Politehnica University, Timişoara, 300006, Romania

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Identyfikatory

DOI

10.2478/s11532-010-0012-4