Determination of active components in Chinese medicinal preparations by capillary electrophoresis

• Autorzy: Huitao Liu , Yuan Gao
• Języki publikacji: EN

Abstrakty

EN

The determination of paeoniforin, paeonol, and censenoside Rg1 in traditional Chinese medicinal preparations, Tze Po San Pien pills and Liuwen Dihuang pills has been investigated by micellar electrokinetic capillary electrophoresis with borate buffer (20 mM), sodium dodecylsulfate (30 mM) and acetonitrile (20%) as background electrolytes (pH 9.30), 20 kV applied voltage and 203 nm UV detection. The effects of SDS concentration, borate, buffer pH, and organic modifier on electrophoretic behavior and separation are discussed. Regression equations revealed linear relationships between the peak-area of each component and the content with the correlation coefficients from 0.9982 to 0.9999. In addition, the levels of the active compounds in two kinds of traditional Chinese medicinal preparations were easily determined with the recoveries from 93.1% to 108.2%. [...]

Słowa kluczowe

EN

Micellar electrokinetic capillary electrophoresis; paeonol; paeoniforin; censenoside Rg1; Chinese medicinal preparations

• Czasopismo: Open Chemistry
• Rocznik: 2007
• Tom: 5
• Numer: 1
• Strony: 221-229

Daty

wydano

2007-03-01

online

2007-03-01

Twórcy

autor

Huitao Liu

• Department of Applied Chemistry, Yantai University, Yantai, 264005, P.R. China,

autor

Yuan Gao

• College of Environment and Material Engineering, Yantai University, Yantai, 264005, P.R. China

Bibliografia

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Identyfikatory

DOI

10.2478/s11532-006-0059-4