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1
Content available Microstructures and Tensile Properties of Fe-Cr-Al Oxide Dispersion Strengthened Ferritic Alloys for High Temperature Service Components
Park Minha, Bae Jaeyoon, Kim Byung-Jun, Kim Bu-Ahn, Noh Sanghoon
Archives of Metallurgy and Materials
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2023
|
Vol. 68, iss. 1
85--88
EN
In present study, Fe-22Cr-4.5Al oxide dispersion strengthened ferritic alloys were fabricated using a pre-alloyed powder with different minor alloying elements, and their microstructures and tensile properties were investigated to develop the advanced structural materials for high temperature service components. Planetary-typed mechanical alloying and uniaxial hot pressing processes were employed to fabricate the Fe-Cr-Al oxide dispersion strengthened ferritic alloys. Microstructural observation revealed that oxide dispersion strengthened ferritic alloys with Ti, Zr additions presented extremely fine micro-grains with a high number density of nano-scaled oxide particles which uniformly distributed in micro-grains and on the grain boundaries. These oxide particles were confirmed as a fine complex oxide, Y2Zr2O7. These favorable microstructures led to superior tensile properties than commercial ferritic stainless steel and oxide dispersion strengthened ferritic alloy with only Ti addition at elevated temperature.
2
Content available Effect of Milling Duration on Oxide-Formation Behavior of Oxide-Dispersion-Strengthened High-Entropy Alloys
Song Yongwook, Kim Daeyoung, Nam Seungjin, Lee Kee-Ahn, Choi Hyunjoo
Archives of Metallurgy and Materials
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2021
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Vol. 66, iss. 3
735--740
EN
Oxide-dispersion-strengthened high-entropy alloys were produced by hot-pressing a ball-milled mixture of Y2O3 and atomized CoCrFeMnNi powder. The effect of milling duration on grain size reduction, oxide formation behavior, and the resulting mechanical properties of the alloys was studied. Both the alloy powder size and Y2O3 particle size decreased with milling time. Moreover, the alloy powder experienced severe plastic deformation, dramatically generating crystalline defects. As a result, the grain size was reduced to ~16.746 nm and in-situ second phases (e.g., MnO2 and σ phase) were formed at the defects. This increased the hardness of the alloys up to a certain level, although excessive amounts of in-situ second phases had the reverse effect.
3
Content available Difference of Microstructures and Mechanical Properties between 9Cr-1W Ferritic/martensitic Steel and ODS Steel
Kim Ga Eon, Kim Tae Kyu, Noh Sanghoon
Archives of Metallurgy and Materials
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2020
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Vol. 65, iss. 1
337--341
EN
Ferrtic/martensitic and ODS steels were fabricated by the mechanical alloying process, and their microstructures and mechanical properties were investigated. The 9Cr-1W and 9Cr-1W-0.3Ti-0.35Y2 O3 (in wt.%) steels were prepared by the same fabrication process such as mechanical alloying, hot isostatic pressing, and hot rolling processes. A microstructural observation of these steels indicated that the Ti and Y2 O3 additions to 9Cr-1W steel were significantly effective to refine the grain size and form nano-sized Y-Ti-O oxide particles. As a result, the tensile strengths at room and elevated temperatures were considerably enhanced. Considerable improvement of the creep resistances at 700°C was also evaluated. It is thus concluded that 9Cr-1W ODS steel with Ti and Y2 O3 additions would be very effective in improving the mechanical properties especially at elevated temperatures.
4
Content available Microstructures and Mechanical Properties of ODS Ferritic Stainless Steels for High Temperature Service Applications
Noh Sanghoon, Kang Suk Hoon, Kim Tae Kyu
Archives of Metallurgy and Materials
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2019
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Vol. 64, iss. 3
921--924
EN
In this study, ODS ferritic stainless steels were fabricated using a commercial alloy powder, and their microstructures and mechanical properties were studied to develop the advanced structural materials for high temperature service applications. Mechanical alloying and uniaxial hot pressing processes were employed to produce the ODS ferritic stainless steels. It was revealed that oxide particles in the ODS stainless steels were composed of Y-Si-O, Y-Ti-Si-O, and Y-Hf-Si-O complex oxides were observed depending on minor alloying elements, Ti and Hf. The ODS ferritic stainless steel with a Hf addition presented ultra-fine grains with uniform distributions of fine complex oxide particles which located in grains and on the grain boundaries. These favorable microstructures led to superior tensile properties than commercial stainless steel and ODS ferritic steel with Ti addition at elevated temperature.
5
Content available The Effect of Additive Element on the Properties of Mechanically Alloyed Fe-Y2O3 Alloys
Ahn J.-H., Kim T. K., Ahn J.
Archives of Metallurgy and Materials
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2017
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Vol. 62, iss. 2B
1043--1046
EN
In the present work, we have examined the effect of Ti on the properties of Fe-Y2O3 alloys. The result showed that the addition of Ti was effective for improving mechanical properties. This is due to the reduction of oxides by Ti during mechanical alloying and hot-consolidation. In particular, iron oxides are effectively reduced by the addition of Ti. Compared to the pristine Fe-Y2O3 alloys, titanium-added alloys exhibited fine and uniform microstructures, resulting in at least 60% higher tensile strength.
6
Content available Effect of Heat Treatment on the Microstructure and Tensile Deformation Behavior of Oxide Dispersion Strengthened Alloys Manufactured by Complex Milling Process
Kim Y.-K., Kim J.-H., Gwon J.-H., Lee K.-A.
Archives of Metallurgy and Materials
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2017
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Vol. 62, iss. 2B
1335--1340
EN
This study attempted to manufacture an ODS alloy by combining multiple milling processes in mechanical alloying stage to achieve high strength and fracture elongation. The complex milling process of this study conducted planetary ball milling, cryogenic ball milling and drum ball milling in sequential order, and then the microstructure and tensile deformation behavior were investigated after additional heat treatment. The oxide particles distributed within the microstructure were fine oxide particles of 5~20 nm and coarse oxide particles of 100~200 nm, and the oxide particles were confirmed to be composed of Cr, Ti, Y and O. Results of tensile tests at room temperature measured yield strength, tensile strength and elongation as 1320 MPa, 2245 MPa and 4.2%, respectively, before heat treatment, and 1161 MPa, 2020 MPa and 5.5% after heat treatment. This results indicate that the ODS alloy of this study gained very high strengths compared to other known ODS alloys, allowing greater plastic zones.
7
Content available remote Application of LENS method in Fe40Al + n-Al2O3 composite materials fabrication
Durejko T., Żuchowska E., Łazińska M.
Composites Theory and Practice
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2012
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R. 12, nr 2
81-85
EN
The present study examines the impast of nanoceramics on the structure and selected mechanical properties of intermetallic alloys. In order to determine the grain size in the different variants of materials, with LENS fabricated Fe40Al, an equivalent mean diameter was determined. Resistance against oxidation of the material with and without the addition of nanoceramics was also determined. Observations of the microstructure and phasal analysis did not reveal the presence of nanoceramics in the bulk of the material. However, it was found that the addition of nano-oxide ceramics, increases the grain size and a 4-fold increased heat resistance compared to the reference material. For the alloy without the addition of the oxide nanoceramics, a relative deformation of 2% at a lower yield than the 2% composite Fe40Al vol. n-Al2O3 was reported. An attempt to explain the situation it was based on research using the Thermal Imager, which is equipped with a LENS MR-7. It allowed permanent registration of the temperature distribution and weld puddle determining a number of thermodynamic dependences. It additionally drew attention to the fact that during the manufacturing process, differences between the width of the liquid metal mesh for the alloys with and without nanoceramics was observed. It indirectly proves the existence of ceramics on the surface of powder particles at the time of melting the base material, and probably there where an increase in the width of the weld puddle was observed.
PL
W opracowaniu przeanalizowano wpływ nanoceramiki na strukturę i wybrane właściwości mechaniczne stopów na osnowie intermetalicznej fazy Fe40Al wytworzonych techniką LENS. W celu określenia wielkości ziarna w poszczególnych wariantach materiałowych wyznaczono średnią średnicę ekwiwalentną. Określono odporność na utlenianie materiału bez i z dodatkiem nanoceramiki. Obserwacje mikrostruktury oraz analiza fazowa nie ujawniły występowania nanoceramiki w objętości materiału. Stwierdzono jednak, że dodatek nanometrycznej ceramiki tlenkowej wpływa na wzrost wielkości ziaren oraz 4-krotnie podwyższa żaroodporność w stosunku do materiału odniesienia. Dla stopu bez dodatku nanoceramiki tlenkowej odnotowano odkształcenie względne na poziomie 2% przy niższej granicy plastyczności niż kompozyt Fe40Al+2%obj.n-Al2O3. Próbę wyjaśnienia zaistniałej sytuacji podjęto w oparciu o badania z wykorzystaniem Thermal Imagera, w który wyposażony jest LENS MR-7. Umożliwia on permanentną rejestrację rozkładu temperatury jeziorka ciekłego metalu i wyznaczania szeregu zależności termodynamicznych. Uwagę zwrócił fakt, że w trakcie procesu wytwarzania zauważono różnice pomiędzy szerokością oczka ciekłego metalu dla stopów z nanoceramiką i bez. Świadczy on pośrednio o istnieniu ceramiki na powierzchni cząstek proszku w momencie przetapiania materiału bazowego i prawdopodobnie tam, gdzie się ona znajduje, obserwuje się wzrost szerokości jeziorka ciekłego metalu.
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