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1

Microstructural study of the composite nickel based, containing different Al amounts, sintered by an unconventional technique and forged

Bendriss Houceme, Boudebane Said, Lemboub Samia, Benselhoub Aissa

Inżynieria Materiałowa

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2024

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Vol. 45, nr 3

8--17

EN

The aluminum-enriched composite with the composition of Udimet 720 alloy was developed using an unconventional two-step sintering process. The first occurred at 1380°C for 0.5 h and the second at 1180°C for 3 h. The sintered material was then forged at 1200°C under a load of 50 kG and with a fall height of 220 mm, in order to achieve the clusters fragmentation of hard components, followed by the homogenization annealing at 800°C for 1.5 h. The consolidation technique included solution treatment at 1080°C and aging at 800°C with various holding times. The investigation techniques by X-ray diffraction analysis (XRD) and observations under a scanning electron microscope (SEM) with semi-quantitative analyses (EDS) have offered the possibility to reveal the aluminum addition’s impact and the holding time aging on the material’s microstructural evolution. The sintered alloy with a high Al content (5.25 %) exhibits a complex structure composed of metallic matrix γ, the chromium carbide Cr23 C6 , and a large variety of binary intermetallics. Despite this, the solution treatment caused an almost complete dissolution of these compounds, and consequently, a saturation of the nickel cubic lattice. An increase in precipitation phenomenon was, due to the formation of the intermetallic γ’ (Ni, Co)3 (Al, Ti), and then, the alloyed chromium carbide (Cr, Co, Ni, Mo, Ti)23 C6 , led to a noticeable hardening of the metal matrix, reaching a microhardness of 700 HV0.1.

PL

Opracowano kompozyt wzbogacony aluminium o składzie stopu Udimet 720 w niekonwencjonalnym dwuetapowym procesie spiekania. Kompozyt spiekano w temp. 1380°C przez 0,5 h, a następnie w temp. 1180°C przez 3 h. Spiekany materiał poddano kuciu w temp. 1200°C pod obciążeniem 50 kG i wysokości opadania 220 mm, w celu uzyskania fragmentacji skupień twardych składników, a następnie wyżarzaniu homogenizującym w temp. 800°C przez 1,5 h. Technika konsolidacji obejmowała obróbkę przesycającą w temp. 1080°C i starzenie w temp. 800°C z różnymi czasami przetrzymywania. Techniki badawcze polegające na analizie dyfrakcji promieni rentgenowskich (XRD) i obserwacje pod skaningowym mikroskopem elektronowym (SEM) wraz z analizami półilościowymi (EDS) umożliwiły ujawnienie wpływu dodatku aluminium i czasu utrzymywania starzenia na ewolucję mikrostruktury materiału. Spiekany stop o wysokiej zawartości Al (5,25%) wykazywał złożoną strukturę, na którą składały się: metaliczna osnowa γ, węglik chromu Cr23 C6 i duża różnorodność binarnych związków międzymetalicznych. Mimo to obróbka roztworowa spowodowała niemal całkowite rozpuszczenie tych związków, a w konsekwencji nasycenie sześciennej sieci niklu. Nasilenie zjawiska strącania osadów spowodowane utworzeniem się międzymetalicznego γ' (Ni, Co)3 (Al, Ti), a następnie stopowego węglika chromu (Cr, Co, Ni, Mo, Ti)23 C6 , doprowadziło do zauważalnego utwardzenia osnowy metalicznej, osiągającego mikrotwardość 700 HV0,1.

2

Effect of graphite nanoparticles on mechanical properties of FSPed aluminum surface composite

Kumar Dinesh, Singh Satnam

Composites Theory and Practice

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2024

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R. 24, nr 1

33--38

EN

Friction stir processing (FSP) is a manufacturing technique that can be employed to produce aluminum 6082 surface composites (ASCs). These ASCs display considerable increases in hardness and tensile strength, which makes them ideal for a wide variety of automotive applications. One example is piston skirts that are used in the cylinder chamber. The primary emphasis of this research is to investigate the accumulative impact that several passes have on Al 6082 surface composites that were filled with graphite nanopowder. The mechanical properties and microstructure of the fabricated composites were studied in order to accomplish this goal. The microstructural investigation showed that the graphite nanopowder particles were evenly distributed throughout the Al-6082 alloy. In addition, better dispersion of the graphite nanopowder was seen throughout the matrix material as the number of passes made during friction stir processing was increased. This may be explained by the reduction in grain size that occurs inside the aluminum metal matrix composites (AMMCs) that are produced as a consequence. According to the results of the research, the microhardness of the material grew to 105.3 HV after the third pass of the tool, and its maximum tensile strength rose to 215±3 MPa. In the ASCs that fabricated after three passes of friction stir processing, the smallest grain size that was measured was 24 micrometers.

3

Powłoki ochronne na warstwach wierzchnich stopów magnezu otrzymywane w procesie natryskiwania cieplnego

Jonda Ewa

Stal, Metale & Nowe Technologie

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2023

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nr 5-6

76--83

PL

Stopy metali lekkich, w tym magnezu, stanowią przedmiot badań w licznych ośrodkach badawczo-naukowych, zarówno w kraju, jak i za granicą. Są również istotnym elementem współpracy z przedstawicielami przemysłu, którzy poszukują konkretnych rozwiązań technologicznych dla swoich produktów.

4

Effect of various factors on the measurement error of structural components of machine parts materials microhardness using computer vision methods

Vlasovets Vitaliy, Vlasenko Tatiana, Kovalyshyn Stepan, Kovalyshyn Olesy, Kovalyshyn Oleg, Kurpaska Sławomir, Kiełbasa Paweł, Bilovod Oleksandra, Shulga Lyudmila

Przegląd Elektrotechniczny

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2023

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R. 99, nr 1

323--329

EN

To assess the causes of failure of parts in operation, it is often necessary to assess the degradation of the structural and phase composition of the material and determine the cause of its change. Microhardness test is used to evaluate the mechanical properties of microvolumes of the material. Microhardness of structural components of steels and cast irons (armco iron ferrite, austenitic component of steel 12Х18Н10Т and cementite of centrifugally cast chrome-nickel cast iron (cast coating Ø910 mm)) was determined by restored four-sided pyramid impression with a square base and a top angle of 136±1. The paper evaluates the influence of the main factors on the micro-hardness error of ferritic, austenitic and carbide component of steels and cast irons: the amount and speed of the indenter load, the stiffness of the substrate, the field of distribution of plastic deformations around the impression, the quality of the surface preparation, the influence of grain boundaries and the relaxation of the impression shape over time. The main factors affecting the accuracy of measurements by the reconstructed impression method have been determined for each of the investigated phases: ferrite, austenite, and cementite.

PL

Aby ocenić przyczyny awarii części w eksploatacji, często konieczna jest ocena degradacji składu strukturalnego i fazowego materiału oraz określenie przyczyny jego zmiany. Do oceny właściwości mechanicznych mikroobjętości materiału stosuje się test mi-rotwardości. Mikrotwardość składników strukturalnych stali i żeliwa (ferryt żelaza armco, austenityczny składnik stali 12Х18Н10Т i cementyt odśrodkowo odlewanego żeliwa chromowo-niklowego (powłoka odlewu Ø910 mm)) określono przez przywrócony wycisk piramidy czterobocznej o podstawie kwadratowej i kącie wierzchołkowym 136±1. W pracy oceniono wpływ głównych czynników na błąd mikrotwardości ferrytycznego, austenitycznego i węglikowego składnika stali i żeliwa: wielkości i prędkości obciążenia wgłębnika, sztywności podłoża, pola rozkładu odkształceń plastycznych wokół wycisku, jakości przygotowania powierzchni, wpływu granic ziaren oraz relaksacji kształtu wycisku w czasie. Określono główne czynniki wpływające na dokładność pomiarów metodą zrekonstruowanego wycisku dla każdej z badanych faz: ferrytu, austenitu i cementytu.

5

Impact of orthodontic adhesive magnets on the mechanical properties and degree of conversion of a photopolymerized orthodontic adhesive

Al-Hayali Saud Khalil, Abed Mazin Ahmed, Al Qassar Sarmad Salih

Ochrona przed Korozją

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2023

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nr 10

329--334

EN

The purpose of this study was to calculate the effects of magnetic field (MF) on the degree of conversion (DC%) and mechanical properties of a photopolymerized orthodontic adhesive. In this investigation, Vega Ortho UV orthodontic adhesive was employed. The applied magnetic field had varying intensities (fixed at 0.01 T, 0.03 T, 0.05 T, 0.1 T, 0.15 T, and 0.2 T and a duration of 5 minutes) and a fixed frequency of 50 Hz. Vickers microhardness and DC% were investigated utilizing the specimens, which were created using circular molds and prepared for compression strength (CS) testing in accordance with ISO 4049. To evaluate DC% before and after MF exposure, Fourier-transform infrared spectroscopy (FTIR/ ATR) was performed. A microhardness tester was used to quantify the samples’ initial VHN while subjecting them to a 500 g load for 15 seconds. After that, properties were evaluated. With the aid of scanning electron microscopy (SEM), the surfaces were evaluated. The one-way analysis of difference and Tukey significant difference tests were used to evaluate the data. Analyses of statistical data showed that DC% tends to rise up to 0.05 T. When compared to the control, VHN and compression strength were considerably decreased after 0.03 T MF (p ≤ 0.05). However, there was a significant difference between the VHN and CS as their values increased with increasing magnetic field intensity. The surfaces of the Vega Ortho were deteriorated, as shown by SEM scans. It was found that the effect of the magnetic field caused changes in the physical and chemical properties.

PL

Celem badania było określenie wpływu pola magnetycznego (MF) na stopień konwersji (DC%) i właściwości mechaniczne fotopolimeryzowanego kleju ortodontycznego. W badaniu zastosowano klej ortodontyczny Vega Ortho UV. Zastosowane pole magnetyczne miało różne natężenia (0,01 T, 0,03 T, 0,05 T, 0,1 T, 0,15 T i 0,2 T przez 5 minut) i stałą częstotliwość 50 Hz. Mikrotwardość Vickersa i DC% ustalono z wykorzystaniem próbek, które zostały wykonane przy użyciu okrągłych form i przygotowane do badania wytrzymałości na ściskanie (CS) zgodnie z normą ISO 4049. Do oceny DC% przed ekspozycją na działanie pola magnetycznego i po niej wykorzystano spektroskopię w podczerwieni z transformacją Fouriera (FTIR/ATR). Do ilościowego określenia początkowej wartości VHN próbek użyto mikrotwardościomierza, poddając je obciążeniu 500 g przez 15 sekund. Następnie dokonano oceny właściwości. Ocenę powierzchni przeprowadzono za pomocą skaningowej mikroskopii elektronowej (SEM). Dane poddano jednokierunkowej analizie różnic i testowi istotnej różnicy Tukeya. Analizy danych statystycznych wykazały, że DC% ma tendencję do wzrostu do poziomu 0,05 T. W porównaniu z próbką kontrolną wartości VHN i wytrzymałości na ściskanie uległy znacznemu zmniejszeniu po oddziaływaniu 0,03 T MF (p ≤ 0,05). Istniała jednak znacząca różnica między VHN i CS, ponieważ ich wartości rosły wraz ze wzrostem natężenia pola magnetycznego. Powierzchnie Vega Ortho uległy degradacji, jak wykazały skany SEM. Stwierdzono, że wpływ pola magnetycznego spowodował zmiany właściwości fizykochemicznych.

6

Effects of thermo-chemical treatment and grinding process of external cylindrical surfaces on residual stresses in 13CrMo4-5 steel

Wójcik R., Sawicki J.

Journal of Achievements in Materials and Manufacturing Engineering

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2023

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Vol. 120, nr 1

10--21

EN

Purpose: This paper presents a study aimed at determining the effect of the carburizing treatment process and the subsequent grinding process on the residual stresses occurring in ring-shaped specimens made of 13CrMo4-5 steel. Design/methodology/approach: During the tests, vacuum carburizing was used, achieving an effective case depth ECD = 0.5 mm. Subsequently, the cylindrical outer surfaces of the samples were ground by conventional plunge grinding and with innovative kinematics using a test stand based on a conventional flat-surface grinding machine. As part of the study, microhardness and residual stresses were measured before and after grinding. Measurements were carried out to a depth of 1 mm. The main component of the stand is an original special device that allows the cylindrical specimen to be clamped. Then the angle between its axis of rotation and the axis of rotation of the grinding wheel is set with respect to the plane of the grinding machine’s magnetic table. In the described tests, the axis of rotation of the cylindrical specimen was deviated from its original position by 15° and set at an angle of 75° to the axis of rotation of the grinding wheel. The specimens were ground with a grinding wheel of noble electro-corundum marked 38A60K8V. In both kinematic cases of the grinding process, a machining allowance of 0.01 mm was removed. Findings: Grinding using innovative kinematics did not cause any significant changes in the microhardness distribution, either for vacuum or conventional carburizing. In addition, residual stress measurements using the Dawidenkov-Sachs method showed that innovative grinding enables a more favourable distribution than those obtained after conventional plunge grinding. Research limitations/implications: Further research will focus on, among others, selecting the angular settings of the workpiece axes relative to the grinding wheel axes depending on their dimensions. Grinding guidelines should include coverage ratio, infeed value, grinding time, and peripheral speeds. In addition, the plan for future research includes measuring the components of the grinding force and the geometric structure of the surface. Practical implications: Grinding process is a crucial stage of steel treatment in almost every industrial branch. In sustainable manufacturing, it is extremely important to produce high-quality items while reducing the cost of manufacturing and taking care of the environment and workers’ health. Originality/value: The proposed test stand, together with the authors’ device, makes it possible to conduct machining of the external surfaces of cylindrical workpieces on a flat surface grinder. In this case, the innovation of the grinding process consists of the non-parallel alignment of the cylindrical rotational axis of the specimen and the rotational axis of the grinding wheel with respect to the plane of the magnetic grinding table.

7

Wpływ parametrów wytwarzania na mikrostrukturę i właściwości spiekanych kół zębatych wykonanych na bazie proszku Distaloy AQ

Sułowski Maciej, Dąbrowski Robert, Żarów Martyna

Inżynieria Materiałowa

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2023

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Vol. 44, nr 1

6--11

PL

Zbadano wpływu parametrów wytwarzania, tzn. infiltracji miedzią, na mikrostrukturę i właściwości mechaniczne kół zębatych wytworzonych techniką metalurgii proszków na bazie proszku żelaza Distaloy AQ. Zakres badań obejmował określenie zmiany wymiarów kół oraz ich gęstości, przed i po procesie infiltracji, pomiar wytrzymałości na statyczne zginanie zębów, pomiar mikrotwardości kół zębatych oraz analizę ich mikrostruktury. Koła zębate podzielono na cztery grupy; jedna z nich nie była infiltrowana miedzią, pozostałe trzy infiltrowano kolejno jednym (1,4% Cu), dwoma (2,8% Cu) i trzema (4,2% Cu) miedzianymi pierścieniami. Stwierdzono, że infiltracja miedzią powoduje wzrost wytrzymałości na zginanie badanych spieków, lecz tylko w przypadku zawartości 1,4% Cu. Większa ilość miedzi powoduje obniżenie wytrzymałości na zginanie zębów kół. Badania wykazały również, że infiltracja miedzią nie wpływa korzystnie na mikrotwardość kół zębatych.

EN

The influence of production parameters i.e., copper infiltration, on the microstructure and mechanical properties of gear wheels initially manufactured by powder metallurgy was investigated. Distaloy AQ iron powder was used for production these gears. The scope of research included the determination of changes in the dimensions of the gear wheels and their density, before and after the infiltration process, measurement of the strength to static bending, measurement of the microhardness of the gear wheels and analysis of their microstructure. The gear wheels are divided into four groups; one of them was not infiltrated with copper, the remaining three were infiltrated successively with one (1.4% Cu), two (2.8% Cu) and three (4.2% Cu) copper rings. It was found that copper infiltration increases the bending strength of the tested sinters, but only in the case of 1.4% Cu content. The greater amount of copper reduces the bending strength of the gear wheels. Research has also shown that copper infiltration does not have a positive effect on the microhardness of gear wheels.

8

Analytical versus experimental investigation of physical and mechanical characteristics of stir cast hybrid aluminium nanocomposite

Kumar Dinesh, Singh Satnam, Angra Surjit

Composites Theory and Practice

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2023

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R. 23, nr 3

136--144

EN

Aluminium alloys have good mechanical and physical properties and are lightweight, easy to cast, and simple to machine. Aluminium alloys are widely used in the aviation industry, auto sector, defence sector, and structural industries because of their promising abilities. The fundamental aim of this study was to investigate the mechanical properties and physical characteristics of a stir cast hybrid aluminium nanocomposite reinforced with 1-3 wt.% cerium oxide (CeO2) and graphene nanoplatelets (GNPs). Utilizing SEM, microstructural analysis was carried out. The existence of the elements of the reinforcement in the manufactured nanocomposite specimens was verified using EDAX. With an increase in the reinforcement wt.%, improvements in the mechanical and physical properties were seen. In the hybrid nanocomposites reinforced with 3 wt.% GNPs and 3 wt.% CeO2, a low porosity of 1.06% was observed. The best results for tensile strength, yield strength, and microhardness were 398 MPa, 247 MPa, and 119.6 HV, respectively. The SEM micrographs of the studied materials showed that the reinforcement particles were uniformly dispersed and refined into ultrafine grains.

9

Evolution of zinc coatings during drawing process of steel wires

Suliga Maciej, Wartacz Radosław, Hawryluk Marek

Archives of Civil and Mechanical Engineering

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2023

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Vol. 23, no. 2

art. no. e120, 2023

EN

The paper shows a significant influence of the multi-stage wire drawing technology on deformability and phase transformations in the zinc coating. SEM tests proved that the coating after hot-dip galvanizing consists of a number of thin layers, ranging from 1 to 5 μm, and differing in thickness, chemical composition and properties. When pulled through the drawing die the zinc coating heats up (as a result of friction between the material and the tool) and its dynamic plastic deformation. It resulted in the fracture and partial crushing of the hard-intermetallic phases. It has been proven that as the wire passes through successive drawing dies, the coating is thinned and diffusion as well as phase remodelling of individual structural components occurs; in the place of phase ζ, the intermetallic phase δ1 develops, increasing its share in the diffusion layer. The crystals of intermetallic phases located on the border of the diffusion and outer layers break up and remain dispersed in the zinc. An analysis of the microhardness of the coating has proven that the level of the increase in the microhardness of the zinc coating is contingent on percentage of iron in particular layers of coating.

10

Porównanie mikrostruktury i odporności na korozję powłok natryskiwanych metodą HVOF (high velocity oxy fuel) na podłoże ze stopu magnezu

Jaworska Justyna, Gruszka Magdalena, Nabrdalik Monika, Marcinkowski Marcin, Mikołejko Wojciech, Augustyn Ewelina, Jonda Ewa, Maciej Artur, Kiljan Anna

Ochrona przed Korozją

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2022

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nr 4

112--123

PL

Stopy magnezu ze względu na korzystny stosunek niskiej masy do dobrych własności mechanicznych coraz powszechniej są stosowane w przemyśle. Przeszkodę w ich aplikacji może stanowić reaktywność chemiczna magnezu, a więc jego wysoka podatność na korozję. Powłoki natryskiwane cieplnie metodą HVOF (high velocity oxy fuel) pozwalają wytworzyć szczelną barierę pomiędzy materiałem podłoża a środowiskiem, dzięki czemu mogą stanowić skuteczną ochronę stopów magnezu. W artykule przedstawiono wyniki badań mikrostruktury oraz wybranych własności dwóch powłok natryskiwanych przy wykorzystaniu komercyjnych proszków WC-Co i WC-Cr3C2-Ni metodą HVOF na podłożu ze stopu magnezu AZ91. Celem pracy było porównanie mikrostruktury, wybranych własności oraz odporności na korozję wytworzonych powłok. Na podstawie wyników badań mikroskopowych stwierdzono, że powłoki charakteryzują się zwartą mikrostrukturą, a twarde cząstki WC oraz Cr3C2 są równomiernie rozłożone w całej objętości powłoki. Powłoka WC-Co charakteryzuje się ponadto wyższą odpornością korozyjną oraz mikrotwardością, jednak cechuje ją mniejsza wydajność natryskiwania i chropowatość w porównaniu z powłoką WC-Cr3C2-Ni.

EN

Due to the promising ratio of low weight to good mechanical properties, magnesium alloys are more and more widely used in industry. An obstacle in their application may be the chemical reactivity of magnesium, and therefore its high susceptibility to corrosion. Thermal sprayed coatings with the HVOF (high velocity oxy fuel) method allow creating a tight barrier between the base material and the environment, which can effectively protect magnesium alloys. The article presents the results of research on the microstructure and selected properties of two sprayed coatings with the use of commercial WC-Co and WC-Cr3C2-Ni powders using the HVOF method on the substrate made of AZ91 magnesium alloy. The work aimed to compare the microstructure, selected properties, and corrosion resistance of the produced coatings. Based on the results of the metallographic research, it was found that the coatings are characterized by a dense microstructure, and the hard particles of the WC and Cr3C2 are evenly distributed throughout the entire volume of the coating. Also the WC-Co coating is characterized by higher corrosion resistance and microhardness however, it has a lower spray efficiency and roughness compared to the WC-Cr3C2-Ni coating.

11

Influence of heat treatment on the properties of explosively welded Cu-Al joint

Lokaj Jan, Sahul Miroslav, Sahul Martin, Čaplovič Ľubomír

Materiały Wysokoenergetyczne

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2022

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T. 14

4--13

EN

Explosive welding of copper C10200 to aluminium alloy AW 5083 was performed. C10200 was proposed as a flyer plate due to its suitable plastic properties. A parallel layout of welded metals was selected to attain a more stable welding process. Welding parameters and conditions were determined. The surfaces of both materials were mechanically machined and degreased prior to welding which was performed using Semtex S30. The bimetals were characterized by a regular wavy interface. The aim of the research was to establish the influence of heat treatment on both the structure and microhardness at the interface of the explosively welded bimetal Al-Cu. Heat treatment was performed at 250, 300 and 350 °C over 2, 3 and 4 h. After heat treatment, an increase in Inter Metallic Compounds (IMC) was observed, proportional to the increasing temperature. An analysis of chemical composition carried out by EPMA (Electron Probe Micro Analysis) confirmed the presence of Inter Metallic Phases (IMP) such as θ (Al2Cu), η2 (Al2Cu), ξ2 (Al3Cu4), δ (Al2Cu3), γ1 (A14Cu9). The microhardness decreased after the heat treatment in the bimetal but significantly increased at the interface as a consequence of IMC formation.

PL

Wykonano zgrzewanie wybuchowe stopu aluminium miedź C10200 i AW 5083. C10200 został zaproponowany jako płyta napędzana ze względu na jego odpowiednie właściwości plastyczne. Wybrano równoległy układ zgrzewanych metali, aby uzyskać bardziej stabilny proces łączenia. Określono parametry i warunki łączenia. Powierzchnie obu materiałów zostały poddane obróbce mechanicznej i odtłuszczeniu przed zgrzewaniem wykonanym przy użyciu Semtex S30. Bimetale charakteryzowały się regularną falistą powierzchnią styku. Celem badań było określenie wpływu obróbki cieplnej zarówno na strukturę, jak i mikrotwardość na granicy faz bimetalu Al-Cu zgrzewanego wybuchowo. Obróbkę cieplną przeprowadzono w 250, 300 i 350 °C przez 2, 3 i 4 godziny. Po obróbce cieplnej zaobserwowano wzrost związków międzymetalicznych (IMC), który był proporcjonalny do wzrostu temperatury. Analiza składu chemicznego przeprowadzona przez EPMA (Electron Probe Micro Analysis) potwierdziła obecność IMP takich jak θ (Al2Cu), η2 (AlCu), ξ2 (Al3Cu4), δ (Al2Cu3), γ1 (Al4Cu9). Mikrotwardość zmniejszyła się po obróbce cieplnej w bimetalu, ale znacznie wzrosła na granicy faz w wyniku tworzenia IMC.

12

Parametric optimisation of microhardness on heat-treated electroless Ni-YSZ cermet coating

Bahiyah Baba N., Ghazali A. S., Abdul Rahman A. H., Sharif S

Journal of Achievements in Materials and Manufacturing Engineering

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2022

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Vol. 112, nr 1

33--41

EN

Purpose: The paper discusses the parametric optimisation of the electroless Ni-YSZ cermet coating microhardness upon heat treatment. Heat treatment is a process to increase the mechanical properties of the electroless nickel coating and it can be enhanced by manipulating its parameters. Parametric optimisation is conducted by the design of experiment full factorial 3x3 with 27 runs. Treating temperature, treating time and ceramic particle size parameters at 3-level are evaluated using statistical tool ANOVA in Minitab20. Design/methodology/approach: Ni-YSZ cermet coating is deposited onto a high-speed steel substrate using the electroless nickel co-deposition method. The temperature and time were varied in a range of 300-400°C and 0-2 hours respectively. The microhardness measurements were carried out using a Vickers microhardness tester (Shimadzu) according to ISO 6507-4. The surface characterisation was analysed using Cambridge Stereoscan 90 Scanning Electron Microscope (SEM) coupled with Energy Dispersive X-ray Analysis (EDXA). Findings: The optimum condition in obtaining high microhardness on Ni-YSZ cermet coating is evaluated by statistical tool ANOVA in Minitab20 software. It is found that the most significant parameter for high microhardness is at the treating temperature of 400°C followed by treating time at 2 hours using nano-sized YSZ particles. The ceramic particle size is found not a significant parameter in obtaining a high microhardness, however it has effect on interaction between treating temperature and treating time. Research limitations/implications: The paper only limits to the optimisation condition of microhardness on Ni-YSZ cermet coating hardness property by varying heat treatment parameters. Practical implications: The optimisation condition obtained might only applicable to the electroless Ni-YSZ cermet coating with similar electroless nickel solution and treatments. Originality/value: The value of this work is the heat treatment parametric optimisation to obtain high microhardness on electroless Ni-YSZ cermet coating by using the design of experiment 3-level full factorial.

13

Effect of heat treatment on microhardness of electroless Ni-YSZ cermet coating

Bahiyah Baba N., Ghazali A. S., Abdul Rahman A. H., Sharif S.

Journal of Achievements in Materials and Manufacturing Engineering

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2022

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Vol. 113, nr 1

5--12

EN

Purpose: The paper discussed the effect of heat treatment on electroless nickel-yttria-stabilised zirconia (Ni-YSZ) cermet coating. Ni-YSZ cermet coating has potential applications such as cutting tools, thermal barriers, solid oxide fuel anode, and various others. The compatibility of ceramic YSZ and metallic nickel in terms of the mechanical properties such as hardness by varying the heating temperature, time and ceramic particle size is highlighted. Design/methodology/approach: Ni-YSZ cermet coating was deposited onto a highspeed steel substrate using the electroless nickel co-deposition method. The temperature and time were varied in a range of 300-400°C and 1-2 hours, respectively. The microhardness measurements were carried out using a Vickers microhardness tester (Shimadzu) according to ISO 6507-4. The surface characterisation of the cermet coating was carried out using JOEL Scanning Electron Microscope (SEM) coupled with Energy Dispersive X-ray (EDX) JSM 7800F. The crystallographic structure of materials was analysed by X-ray diffraction (XRD) Bruker D8 Advance instrument. Findings: It was found that the microhardness of Ni-YSZ cermet coating with the ratio of 70:30, respectively, is directly proportional to the heating temperature and time. Heating the Ni-YSZ cermet coating at 300°C from room temperature (rtp) to 1 hour shows a 12% microhardness increment, while from 1 to 2 hours gives a 19% increment. Compared to heating at 350°C and 400°C, the increment is more significant at 33% and 49% for rtp to 1 hour and 8% and 16% for 1 to 2 hours, respectively. In addition, the effect of varying YSZ particle size in the Ni-YSZ cermet gave response differently for heating temperature and heating time. Research limitations/implications: The paper is only limited to the discussion of the heat treatment effect on Ni-YSZ cermet coating hardness property. The tribological effect will be in future work. Practical implications: The microhardness data may vary due to the Vickers microhardness force applied and the amount of ceramic particle incorporation and phosphorus content in the nickel matrix. Originality/value: The value of this work is the compatibility of the ceramic YSZ and metallic nickel matrix in terms of mechanical properties, such as hardness, upon heat treatment.

14

The influence of workpiece speed on microhardness and residual stresses in vacuum-carburised 20MnCr5 steel using the single-piece flow method

Sawicki J., Januszewicz B., Sikora M., Witkowski B.

Archives of Materials Science and Engineering

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2022

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Vol. 115, nr 2

66--75

EN

Purpose: To determine the impact of selected conditions of abrasive treatment on the value and distribution of microhardness and residual stresses in layers carburised by a continuous single-piece flow method. Design/methodology/approach: Reference pieces were low pressure carburised at 920°C and then heat-treated in a 4D Quench heat treatment chamber at a pressure of 7 bar and tempered at 190ºC for 3 hours. In the next stage, samples were ground at various vw piece speeds, introducing grinding fluid into the cutting zone using the WET spraying method or using the MQL method at a minimum flow rate. The distribution of microhardness and residual stresses generated in the technological outer layer of the pieces following heat and chemical treatment and the grinding process was measured. Findings: Results of the tests indicated that the vw piece speed and method used to supply cooling and lubricating fluid to the grinding zone had an impact on selected parameters of the technological outer layer of flat samples made of 20MnCr5 steel. The process of grinding using an electrocorundum grinding wheel results in a deterioration of residual stresses in the material. For each of the three analysed vw piece speeds, reduced changes in material microhardness prior to cutting occur in the outer layer of samples ground using GF supplied at a minimum flow rate using the MQL method. Research limitations/implications: Environmental considerations and having to conform to increasingly stringent regulations related to environmental protection and employee safety motivate researchers and businesses to entirely eliminate or reduce the use of grinding fluids in the grinding process and, therefore, to optimise grinding technology. Practical implications: Modern manufacturing industry requires the grinding process, which follows heat and chemical treatment, to be performed with the highest possible efficiency. However, retaining high parameters of the technological outer layer in comparison to the sample material following vacuum carburisation (before grinding) is extremely difficult. An optimised configuration of parameters of the grinding process and method of supplying grinding fluids enables meeting the current and future high expectations of the industry in this regard. Originality/value: The tests have enabled us to determine the impact of the applied vw workpiece speed and method of supplying grinding fluid on microhardness and residual stresses. Generally speaking, grinding with an electrocorundum grinding wheel results in a deterioration of residual stresses. For both methods of supplying GF (WET and MQL), the distribution of microhardness in the material of the samples ground with the highest workpiece speed (18.0 m/min) indicated no significant differences with regard to the distribution of microhardness in the material of the samples following heat and chemical treatment.

15

Effects of B addition on the microstructure and microhardness of melt-spun Al-7075 alloy

Kilicaslan Muhammed Fatih, Elburni Saad Ibrahim, Yilmaz Yasin, Akkaş Mehmet

Advances in Materials Science

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2022

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Vol. 22, nr 2(72)

5--18

EN

Main aim of this study is to examine change of microstructural and the mechanical properties of Al-7075 alloy depending on B content added with different proportions. Rapid solidification process used to produce the alloys was carried out with a single roll melt spinner via a wheel with a rotational speed of 25 m/s. For the microstructural characterization of the alloys, a scanning electron microscope and X-ray diffraction analyzes were used. According to obtained results, it can be said that B addition led to modification of dimensions and shapes of both α−Al and intermetallic phases occurred, it reduced average grain size from 0.45 μm to 0.34 μm in the microstructure. The B addition also led to dramatically increase in microhardness of the Al-7075 alloy. The microhardness of the alloy with 0.4 wt. % B is 0.19 GPa, this is clearly one times higher than that of the alloy without B addition. The microhardness of the alloy with 1 wt. % B is 0.21 GPa, this is also slightly higher than that of the alloy with 0.4 wt. % B.

16

Głębokościowa charakterystyka odporności korozyjnej azotowanego stopu Ti6Al4V

Jagielska-Wiaderek Karina

Ochrona przed Korozją

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2021

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nr 2

34--37

PL

W pracy przedstawiono elektrochemiczną ocenę odporności korozyjnej azotowanego stopu tytanu Ti6Al4V. Badania korozyjne wykonano w 0,5M roztworze siarczanowym zakwaszonym do pH = 2 wykreślając krzywe potencjokinetyczne na różnych głębokościach warstwy wierzchniej. Grubość powstałej warstwy wierzchniej oceniono na podstawie badań strukturalnych oraz zmiany mikrotwardości na przekroju poprzecznym obrobionego powierzchniowo materiału. Stwierdzono, że przeprowadzona obróbka azotująca poprawia odporność korozyjną oraz znacznie utwardza powierzchnie badanego materiału. Uzyskana warstwa wierzchnia posiada budowę strefową przy czym najwyższą odporność korozyjną jak i najwyższą mikrotwardość wykazuje najbardziej zewnętrzna strefa azotków.

EN

The paper reports the electrochemical assessment of the corrosion resistance of the titanium alloy Ti6Al4V. Corrosion tests were carried out in a 0.5M sulphate solution acidified to pH = 2, while plotting potentiometric curves at varying depths of the top layer. The thickness of the produced top layer was assessed based on structural examination and change in microhardness over the cross-section of the surface treated material. It has been found that the nitriding treatment improves the corrosion resistance and considerably hardens the surface of the material under study. The obtained top layer exhibits a zonal structure, with the greatest corrosion resistance and the highest microhardness being shown by the outermost nitride zone.

17

Forecasting process parameters on weld nugget hardness of filler added friction stir welded dissimilar aluminium alloys 5052 and 6082 joints

Sasikumar A., Gopi S., Mohan Dhanesh G.

Journal of Mechanical and Energy Engineering

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2021

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Vol. 5, No 2

103--112

EN

This article deals with the optimization of friction stir welding process parameters with filler ratios on dissimilar Aluminium alloy groups. For this purpose, 6 series Aluminium alloy 6082 and 5 series Aluminium alloy 5052 were taken. Microhardness property was conducted under various rotational speeds, welding speed, plunge depth, Center distance between the holes and filler mixing ratio. The Central Composite Design (CCD), the most commonly used Response Surface Methodology (RSM), is considered to develop the prediction equation. A validation analysis is carried out, and the results were compared with the relative impact of input parameters on weld nugget microhardness. It is observed that the increase in welding speed with plunge depth and filler ratio result in the increase of weld nugget microhardness up to a maximum value. The maximum weld nugget hardness of fabricated joint was obtained with the welding process parameters combination of 1000 rpm rotational speed, 125 mm/min welding speed, 0.15 mm plunge depth, 2 mm centre distance between the holes, and filler ratio of 95% Mg and 5% Cr.

18

Hardness investigation of conventional, bulk fill and flowable dental composites

Georgiev G., Dikova T.

Journal of Achievements in Materials and Manufacturing Engineering

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2021

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Vol. 109, nr 2

68--77

EN

Purpose: of the present paper is to investigate the micro-hardness of three types of resin-based composites – conventional, bulk fill and flowable. Design/methodology/approach: Cylindrical specimens with a diameter of 5 mm and thicknesses of 2, 3 and 4 mm were made from each composite. They were light cured for 20, 40 and 60 s with light intensity of 600, 1000 or 1500 mW/cm2. The Vickers micro-hardness was measured on the top and bottom surface of the specimens. Findings: The highest micro-hardness was measured in bulk fill composite, followed by conventional and the lowest was measured in the flowable one. Increasing the light intensity leads to increase of the micro-hardness on both surfaces of the three composites. The increase of the irradiation time results in increase of the micro-hardness mainly on the bottom surface of the composites. The change of the layer thickness influences the conventional and the flowable composites and almost does not affect the hardness of the bulk fill composite. Research limitations/implications: The limitations of this study concerns to the values of the light intensity, which are defined by the light curing unit (LCU) used. There are many LCUs on the market; consequently, constant investigations of dental composites micro-hardness are needed. Practical implications: The investigation of the micro-hardness of the three types of composites in different modes would be very helpful for clinicians to obtain successful polymerization of composite restorations in their everyday practice. Originality/value: The micro-hardness of three types resin-based dental composites – conventional, bulk fill and flowable is investigated and compared in varying of three mode parameters – light intensity, curing time and layer thickness.

19

Distribution of microhardness in polypropylene/talc microcomposite

Bechikhi Youcef, Bouiadjra Bachir Bachir, Bouziane Mohamed Mokhtar, Bouiadjra Bel Abbes Bachir, Benbarek Smail

Composites Theory and Practice

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2021

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R. 21, nr 4

141--148

EN

In this study the distribution of microhardness in a polypropylene microcomposite reinforced with talc microparticles was measured experimentally. The microhardness was measured at different points of the composite material to try to observe the effects of the talc particles and their proportion in the composite on the hardness of the reinforced polymer. Four proportions of talc were used: 5,40 and 50 wt.%, in addition to virgin polypropylene, which was taken as the reference. Statistical analysis was performed on the distribution of the microhardness in the PP+talc composites to determine the average microhardness and the standard deviation. The obtained results reveal a random distribution of the microhardness of the composite, but in general the presence of talc particles increases the microhardness of the polypropylene.

20

Effects of yttria content and sintering temperature on the microstructure and tendency to brittle fracture of yttria-stabilized zirconia

Kulyk V.V., Duriagina Z.A., Vasyliv B.D., Vavrukh V.I., Lyutyy P.Ya., Kovbasiuk T.M., Holovchuk M.Ya.

Archives of Materials Science and Engineering

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2021

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Vol. 109, nr 2

65--79

EN

Purpose: The purpose of this work is to evaluate the propensity to brittle fracture of YSZ ceramics stabilized by the various amount of yttria, based on a study of changes in the microstructure, phase composition, and fracture micromechanisms. Design/methodology/approach: The series of 3YSZ, 4YSZ, and 5YSZ ceramic specimens were sintered in an argon atmosphere. Three sintering temperatures were used for each series: 1450°C, 1500°C, and 1550°C. Microhardness measurements were performed on a NOVOTEST TC-MKB1 microhardness tester. The configuration of the imprints and cracks formed was studied on an optical microscope Neophot-21. The fracture toughness of the material was estimated using both the Vickers indentation method and a single-edge notch beam (SENB) test performed under three-point bending at 20°C in air. The microstructure and morphology of the fracture surface of the specimens were studied using a scanning electron microscope Carl Zeiss EVO-40XVP. The chemical composition was determined using an INCA ENERGY 350 spectrometer. Findings: Peculiarities of changes in the microstructure, the morphology of specimens fracture surface, and mechanical characteristics of YSZ ceramic materials of different chemical and phase compositions sintered in a temperature range of 1450°C to 1550°C are found. Research limitations/implications: To study the actual behaviour of YSZ ceramic materials under operating conditions, it is necessary to evaluate their Young’s moduli, strength, microhardness, and fracture toughness in an operating environment of the corresponding parameters (temperature, pressure, etc.).Practical implications: Based on the developed approach to estimating the propensity to brittle fracture of the formed YSZ ceramic microstructure, it is possible to obtain YSZ ceramic material that will provide the necessary physical and mechanical properties of a wide variety of precision ceramic products. Originality/value: An approach to estimating the propensity to brittle fracture of YSZ ceramics stabilized by the various amount of yttria is proposed based on two methods of evaluating crack growth resistance of materials, namely, the Vickers indentation method and SENB method.