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Efficiency of linear and non-linear classifiers for gas identification from electrocatalytic gas sensor

Kalinowski P., Woźniak Ł., Strzelczyk A., Jasinski P., Jasinski G.

Metrology and Measurement Systems

2013

Vol. 20, nr 3

501--512

Electrocatalytic gas sensors belong to the family of electrochemical solid state sensors. Their responses are acquired in the form of I-V plots as a result of application of cyclic voltammetry technique. In order to obtain information about the type of measured gas the multivariate data analysis and pattern classification techniques can be employed. However, there is a lack of information in literature about application of such techniques in case of standalone chemical sensors which are able to recognize more than one volatile compound. In this article we present the results of application of these techniques to the determination from a single electrocatalytic gas sensor of single concentrations of nitrogen dioxide, ammonia, sulfur dioxide and hydrogen sulfide. Two types of classifiers were evaluated, i.e. linear Partial Least Squares Discriminant Analysis (PLS-DA) and nonlinear Support Vector Machine (SVM). The efficiency of using PLS-DA and SVM methods are shown on both the raw voltammetric sensor responses and pre-processed responses using normalization and auto-scaling.

Electrocatalytic sensor based on Nasicon with auxiliary layer

Strzelczyk A., Jasiński G., Jasiński P., Chachulski B.

Elektronika : konstrukcje, technologie, zastosowania

2012

Vol. 53, nr 1

72-74

In this study properties of Nasicon solid state gas sensors working in electrocatalytic mode are investigated. The principle of operation of such sensors is based on the excitation with a periodic potential signal, while current response is recorded. The sensors are prepared in ceramic technology with two different constructions. One construction is a symmetrical, sandwich type structure with electrolyte between two identical gold electrodes. In the second, the same structure is used, but the electrodes are covered with auxiliary layer of sodium nitrite. Nitrogen dioxide sensing properties of both sensors are determined and compared.

W pracy zostały przedstawione wyniki pomiarów czujnika na bazie Nasiconu pracującego w trybie elektrokatalitycznym. Czujniki takie pobudzane są zmieniającym się napięciem przy jednoczesnym pomiarze odpowiedzi prądowej. Przygotowano czujniki ceramiczne o dwóch różnych typach. Pierwszy z nich to czujnik posiadający dwie identyczne elektrody złote, pomiędzy którymi znajduje się elektrolit stały. Drugi czujnik posiada złote elektrody dodatkowo pokryte warstwą azotanu (III) sodu. Zmierzono i porównano odpowiedzi obu czujników dla różnych stężeń dwutlenku azotu w mieszaninie z powietrzem.