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1

Performance tests of paint coatings used for masking armaments and military equipment

Radek Norbert

Technical Transactions

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2023

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Vol. 120, iss. 1

art. no. e2023008

EN

The paper presents an analysis of the operational properties of paint coatings for use in military technology in the field of masking. The assessment of the properties was performed on the basis of measurements of the surface geometric structure and adhesion using the peel method. The measurements of specular gloss, colour in the range of 400-700 nm and reflectance in the range of 350-1200 nm were made in relation to the requirements of the Polish Defence Standard NO-80-A200. Coating systems are characterised by their low roughness and good adhesion. Due to their operational properties, the developed coating systems can be used on armaments and military equipment.

2

Niestabilność reologiczna węglanowych mieszanek powlekających zawierających skrobię modyfikowaną

Stanisławska Anna, Gapiński Artur

Przegląd Papierniczy

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2023

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R. 79, nr 2

102--109

PL

Celem niniejszej pracy było zbadanie wpływu dodatku skrobi modyfiko-wanej na stabilność reologiczną mieszanek powlekających zawierających węglan wapnia. Wyznaczone zostały krzywe lepkości i krzywe płynięcia z uwzględnieniem czynnika czasu zarówno dla mieszanek, jak i roztworu skrobi modyfikowanej oraz dyspersji węglanu wapnia. Zawartość skrobi modyfikowanej w mieszankach powlekających wpływa na właściwości reologiczne tych mieszanek, zwiększając ich lepkość i naprężenie ścinające. Wykazano, że mimo reostabilnego charakteru roztworu skrobi i dyspersji węglanu wapnia przygotowane mieszanki powlekające okazały się być płynami reoniestabilnymi. Ich lepkość i naprężenie ścinające zmniejszały się przy wydłużeniu czasu ścinania, co świadczy o właściwościach tiksotropowych. Im większy był dodatek skrobi, tym większa była rozpiętość ramion pętli histerezy krzywych płynięcia i lepkości. A zatem, reologiczna niestabilność mieszanek powlekających wzrastała z dodatkiem skrobi.

EN

The rheological properties of coating color affect its flow behavior during technological process. If upon constant shearing, fluid properties do not change with time, the fluid exhibits rheological stability (rheo-stability). On the other hand, a fluid is said to exhibit rheological instability (rheo-instability) if shear time (for a given shearing conditions) affects its flow behavior. The objective of the conducted research was to examine the effect of modified starch on rheological instability of the coating colors. For this purpose, viscosity curves and flow curves were determined considering the time factor. Such experiments enabled to determine time-dependent rheology. Rheological tests were carried out for calcium carbonate-based coating colors with different starch content (1 pph, 2 pph, 5 pph and 10 pph) as well as for the raw materials used for their preparation, i.e. 10% solution of modified starch and 60% calcium carbonate dispersion. During the research, the rotary rheometer Brookfield RVDV - III+ with the Rheocalc V2.3 control software was used. The measurement principle is based on the determination of the torque for a given shear rate or rotational speed. The measuring element (e.g. spindle, coaxial cylinders), immersed in the test fluid, is set in rotation. A viscous liquid resists the measuring element by generating a torque which is a function of the apparent viscosity of the liquid. During the tests, both RV spindles and DIN coaxial cylinders were used, with the rotating inner cylinder and the stationary outer one. Programs in the B.E.A.V.I.S (Brookfield Engineering Advanced Viscometer Instruction Set) programming language were developed to control the rheometer and collect measurement results. This enabled the experiments to be performed automatically. In order to examine the influence of shear time on the flow and viscosity curves, measurements were made at time intervals of 10, 30 and 60 seconds (the measurement was carried out after 10, 30 or 60 s from the moment of changing the shear conditions, i.e. shear rate or rotational speed). The effect of time on viscosity for constant shear conditions was also investigated. Measurements were made within 4 minutes, and data were collected every 2 seconds. Time factor studies enabled to research rheo-stability and/or rheo-instability (time-dependent rheology). For all tested properties, at least 7 measurements were carried out, and the coefficients of variation did not exceed 4.75%. The starch solution exhibited rheo-stable shear-thinning behavior, whereas calcium carbonate dispersion was a rheo-stable shear thickening fluid. This means that the rheological properties of these liquids depended on shear field but did not depend on shear time (for a given shearing conditions). The content of modified starch in coating colors affects the rheological properties of these liquids, increasing their viscosity and shear stress. It was found that despite the rheo-stable character of both the starch solution and the calcium carbonate dispersion, the prepared coating colors were rheologically unstable as they exhibited time-dependent flow behavior. The viscosity of the coating colors decreased not only with the increase in rotational speed, but also with the increase in shear time. The decrease in their viscosity and shear stress with increasing shear time proves that the tested coating colors exhibited rheo-unstable thixotropic flow behaviors. Additionally, the higher the addition of starch was, the wider was the span of the hysteresis loop arms for both the flow and viscosity curves. Thus, the rheological instability increased with increasing starch content.

3

Influence of prophylactic fluoride agents on the color changes and surface roughness of polymer and rhodium coated nickel-titanium orthodontic archwires

Alsarani Majed M., Alaida Wedad Saud, Ajwa Nancy, Alaqeel Samer M., Almutairi Naseer Meshal, Alanazi Khalid Jamal, Durgesh Pavithra, Durgesh Bangalore

Polimery

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2023

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Vol. 68, nr 11-12

607--616

EN

The effect of fluoride use on the color change and surface characteristics of coated nickel and titanium (NiTi) orthodontic archwires was investigated. Epoxy resin, PTFE or rhodium-coated archwires were exposed to acidulated phosphate fluoride (APF) or sodium fluoride (NaF) or artificial saliva (AS), simulating three-month clinical trials. Color changes (ΔE) were assessed using a laboratory spectrophotometer in the three-dimensional CIELab color space. The roughness (Ra) and surface structure of the archwires were examined using a non-contact profilometer and scanning electron microscopy (SEM), respectively. Data were analyzed using two-way and one-way variance (ANOVA) and post-hoc Bonferroni test (α=0.05). The average values of ΔE and Ra were the highest for epoxy-APF archwires and the lowest for rhodium-AS archwires. A significant relationship was found between the archwires surface treatment method and the ΔE and Ra values. After three months, greater changes in color and roughness were observed with APF than with AS.

PL

Zbadano wpływ stosowania fluorków na zmianę koloru i charakterystykę powierzchni powlekanych łuków ortodontycznych z niklu i tytanu (NiTi). Łuki powlekane żywicą epoksydową, PTFE lub rodem poddano działaniu zakwaszonego fluorku fosforanu (APF) lub fluorku sodu (NaF) lub sztucznej śliny (AS), symulując trzymiesięczne próby kliniczne. Zmianę koloru (ΔE) oceniano za pomocą spektrofotometru laboratoryjnego w trójwymiarowej przestrzeni kolorów CIELab. Chropowatość (Ra) i strukturę powierzchni łuków badano za pomocą odpowiednio bezkontaktowego profilometru i skaningowej mikroskopii elektronowej (SEM). Do analizy danych zastosowano dwuczynnikową i jednoczynnikową wariancję (ANOVA) oraz test Bonferroniego post-hoc (α=0,05). Wartości średnie ΔE i Ra były największe dla łuków epoksydowych-APF, a najmniejsze dla rodowych-AS. Stwierdzono istotną zależność pomiędzy metodą obróbki powierzchni łuków a wartością ΔE i Ra. Po trzech miesiącach większe zmiany koloru i chropowatości zaobserwowano w przypadku działania APF niż AS.

4

Effectiveness of polyethylene glycol-coated silica on ions adsorption in industrial wastewater

Maryudi Maryudi, Rahayu Aster, Hakika Dhias Cahya

Polimery

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2023

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Vol. 68, nr 5

259--263

EN

The effect of coating silica with polyethylene glycol on the adsorption of iron and phosphate ions in industrial wastewater was investigated. Variable factors were temperature and time of coating, PEG concentration, and PEG to silica ratio. Infrared spectroscopy and scanning electron microscopy were used to evaluate the chemical structure and morphology of PEG-coated silica. Optimum iron and phosphate ions removal efficiency was obtained using a coating temperature of 50°C, a coating time of 15 min, a PEG concentration of 20%, and a PEG to silica ratio of 1:3.

PL

Zbadano wpływ powlekania krzemionki glikolem polietylenowym na adsorpcję jonów żelaza i fosforanów ze ścieków przemysłowych. Czynnikami zmiennymi były temperatura i czas powlekania, stężenie PEG oraz stosunek PEG do krzemionki. Do oceny budowy chemicznej i struktury krzemionki powlekanej PEG stosowano spektroskopię w podczerwieni i skaningową mikroskopię elektronową. Optymalną skuteczność usuwania jonów żelaza i fosforanów uzyskano stosując temperaturę powlekania 50°C, czas powlekania 15 minut, stężenie PEG 20% oraz stosunek PEG do krzemionki 1:3.

5

Development of a Nanoscale (Mg/Al)-LDH Coated Waterworks Sludge Sorbent for Efficient Congo Red Dye Removal – Batch Kinetics and Isotherm Studies

Salih Sudad Adil, Naife Tariq M.

Journal of Ecological Engineering

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2023

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Vol. 24, nr 7

145--155

EN

The study’s aim was to develop a novel sorbent for removing the color Congo red (CR) from water by precipitating (Mg/Al)-layered double hydroxide (LDH) at the nanoscale onto the waterworks sludge surface as a byproduct. To achieve an effective sorbent with the removal of over 91.19%, The utilization of nanoparticles, the addition of 1 g of sludge to 50 mL of water, and a molar ratio of 2 (Mg/Al) were the optimal production conditions for sorbent. In batch experiments, the optimal operating parameters were found to be 0.5 g of adsorbent in 50 mL of CR, pH of CR solution equal to 3, and a contact time of 3 hours at 200 rpm with 25 mg/L dyes. According to the study, the adsorption capacity was 23.576 mg/g. Additionally, the pseudo-second-order and Langmuir models provided accurate descriptions of the sorption data.

6

Innowacyjność rozwiązań technologicznych piwniczek ekologicznych

Partyka Jacek, Kokocińska-Pakiet Elżbieta, Przybyłko Grzegorz

Inżynieria i Budownictwo

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2023

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R. 79, nr 7-8

421--427

PL

W pracy przedstawiono ogólną charakterystykę piwniczek (ziemianek) jako obiektów podziemnych z głównym przeznaczeniem do przechowywania produktów spożywczych w celu przedłużenia ich trwałości. Wskazano na zalety funkcjonowania obiektów i korzyści związane z ich eksploatacją. Zwrócono uwagę na budowę obiektów w środowisku naturalnym i ciągłym kontakcie z naturą. Ponadto poruszono kwestie związane z trudnościami w jednoznacznym określeniu podstawowych wymagań formalnych dla piwniczek lub ziemianek, uwzględniając aktualnie obowiązujące przepisy w tym zakresie. W pracy dokonano także przeglądu technologii stosowanych podczas budowy podziemnych obiektów magazynowych typu ziemianka. Na przykładzie piwniczek wykonywanych w technologii PwK, wskazano na innowacyjność rozwiązań materiałowo-technicznych stosowanych w realizacjach piwniczek. W związku z dużym potencjałem technologii PwK przedstawiono interesujące tendencje rozwojowe i plany producentów. Całość opracowania podsumowano wnioskami, które dotyczą rozwoju i doskonalenia rozwiązań materiałowo-technicznych, wykorzystywanych przy budowie piwniczek w technologii PwK.

EN

The paper presents the general characteristics of cellars (dugouts) as underground facilities with the main purpose of storing food products in order to extend their durability. The advantages of the functioning of the facilities and the benefits associated with their operation were indicated. Attention was paid to the construction of objects in a natural environment and continuous contact with nature. Moreover, issues related to the difficulties in clearly defining the basic formal requirements for cellars or dugouts were raised, taking into account the current regulations in this regard. The work also reviews the technologies used during the construction of underground storage facilities of the dugout type. On the example of cellars made in the PwK technology, it was indicated on the innovativeness of materiaI and technical solutions used in the construction of cellars. Due to the great potential of the PwK technology, interesting development trends and manufacturers plans were presented. The entire study is summarized with conclusions regarding the development and improvement of material and technical solutions used in the construction of cellars (dugouts) in PwK technology.

7

Research on the Performance of Polypyrrole Coated Conductive Fabrics Prepared from Different Base Materials

Liu Yuanjun, Xue Huangyu, Liu Yanyan, Zhao Jiaqi, Wu Haiying, Zhao Xiaoming

Fibres & Textiles in Eastern Europe

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2023

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Vol. 31, no. 2

75--81

EN

In this paper, polypyrrole coated conductive fabrics were prepared using pyrrole as the monomer, p-toluene sulfonic acid as the doping agent and ammonium persulfate as the oxidant, adopting the simple method of situ polymerization of the liquid phase. Six types of conductive polypyrrole coated fabrics were prepared adopting polyester-cotton blended fabrics, nylon fabrics, wool fabrics, silk fabrics, basalt fabrics and aramid fabric respectively as base materials and using the same process conditions; its electrical conductivity was compared, and the distribution and resistance of the washing fastness of polypyrrole on the surface of those fabrics were studied. Results showed that under the same process conditions, the conductivity of polypyrrole coated terylene fabrics was the best, followed by the polypyrrole coated nylon fabrics and polypyrrole coated wool fabrics. Observed by electron microscope, the distribution of polypyrrole was more homogeneous on different base cloths. After washing, it was concluded that the combination fastness of polypyrrole with polyester-cotton, nylon and wool was better, while the combination fastness of polypyrrole with basalt and aramid was poor.

8

Properties of Ni60/SiO2 Coating Prepared by the Pyrolysis Products of Rice Husk

Wei Chunxue, Li Hongbing

Archives of Metallurgy and Materials

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2023

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Vol. 68, iss. 1

37--42

EN

Surface coating technology, as the main technology to improve the fatigue life of mechanical systems, has been well applied in mechanical equipment. The present study aimed to explore low-cost surface coating preparation technology using inexpensive rice husk as the research object, and the pyrolysis process behavior of rice husk was analyzed. The Ni60/SiO2 coating was prepared on the surface of the 45# steel substrate using the pyrolysis product SiO2 fiber as the reinforcing phase and supersonic plasma-spraying equipment. The results showed no defects such as cracks, pores, and inclusions in the prepared coating. The nanohardness of the Ni60/SiO2 coating reached 6506 μN, and the average friction coefficient reached 0.42. In the friction-and-wear experiment, the Ni60/SiO2 coating was manifested as an abrasive wear mechanism.

9

Adhesion of titanium coatings applied by cold spraying on selected metal substrates

Makrenek M.

Archives of Materials Science and Engineering

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2023

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Vol. 123, nr 2

49--54

EN

Purpose: Measurement of the adhesion of a Ti coating applied by cold spraying on metal substrates with different elastic modulus. An attempt to analytically describe the experimental results, considering cold gas spray parameters such as working gas, pressure p and temperature T. Design/methodology/approach: Ti coating was sprayed on flat bars made of metal: copper, magnesium, brass, titanium, Al 7075, Al 2024 and steel with dimensions of 4x50x400 mm. All coatings were applied under the same spray conditions (p = 3.8 MPa, T = 800ºC, spray distance l = 50 mm, and spray spead V = 400 mm/s). The state of plastic deformation of coatings and substrates was examined using optical methods, and the adhesion strength was measured with the POSITEST tester. Findings: The experimental results are presented graphically. The adhesion force as a function of the relative modulus of elasticity showed a maximum. At this time, the mutual penetration depth of the coating and the substrate showed a minimum. The extremes of the relationships mentioned above occurred for points where the relative modulus of elasticity took the value one. The curve described by formula (1) was fitted to the distribution of adhesion points as a function of the relative elastic modulus. The function parameter described by formula (1) is related to the spray parameters (p, T). Research limitations/implications: To achieve a better accuracy of the analytical description of the adhesion of coatings deposited with cold gas, tests should be carried out on a larger number of substrates. The validity of the presented interpretation should be checked by applying coatings from other materials. Practical implications: In coating technologies, adhesion is a key concept. A coating with high adhesion strength is used primarily in regeneration and anti-corrosion protection processes. The analytical relationship between adhesion, relative modulus of elasticity and cold gas spray parameters will significantly speed up the selection of optimal spray parameters. Cold spray technology is a cost-intensive technology, so the economic element is not without significance. Originality/value: The article presents a method for limiting the number of variables on which the quality of the applied coatings depends. The relationship between the adhesion force, the relative elastic modulus and the selected spray parameters are indicated.

10

Tribology Characteristics of Heatproof Alloys at a Dynamic Pin Ladening in the Variable Temperature Field

Bembenek Michał, Tsyganov Volodymyr, Sakhniuk Nataliia, Lazarieva Olha, Machnik Ryszard, Ropyak Liubomyr

Advances in Science and Technology. Research Journal

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2023

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Vol. 17, no 5

140--152

EN

An analysis of the operating conditions of gas turbine engines, their components, and the destruction causes was carried out. The designer problems of tribo-joints operating under difficult conditions of force and temperature loads are singled out. The study aimed at obtaining the comparable quantitative dependences of blade material wear, taking into account the role of both cyclical changes in the temperature of the gas flow under the conditions close to real ones, and their frictional characteristics. Deformable heat-resistant nickel alloys and foundry heat-resistant nickel alloys from which T-shaped samples were made, were chosen for the research. The tests were carried out on the developed gas dynamic stand, which simulates the working conditions of the bandage joints of the bladed turbomachines of gas turbine installations. The intensity of wear was determined as the ratio of the worn material volume to the number of load cycles under different temperature conditions. The wear resistance of three-way connections operating under the conditions of non-stationary thermal loads and fluctuations in the contact was considered. It was shown that thermal cycling leads to a decrease in the wear resistance of heat-resistant nickel alloys by 2–3 times and depends on the average temperature of the cycle. It was found that resistance to the wear, and also the character of change of coefficient of friction is mainly determined by the terms of education and destruction of the protective superficial layer. Basic factors managing tribology processes in the zone of contact were determined.

11

Postharvest treatments influenced the incidence of internal browning, phenol, aba, and GA3 contents of two pineapple clones

Chandra David, Widodo Soesiladi Esti, Kamal Muhammad, Waluyo Sri

Acta Innovations

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2023

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no. 50

74--80

EN

Phenol is an internal browning (IB) enzymatic reaction substrate and endogenous abscisic acid (ABA) used to suppress IB incidence in the Comte de Paris cultivar (Queen type). There is no information on the correlation between pineapple IB to endogenous total phenol content (TPC), ABA, and gibberellic acid 3 (GA3) after postharvest applications of decrowning. Therefore, this research aimed to analyze the relationship of IB incidence to total TPC, ABA, and GA3 after postharvest treatments of decrowning and coating in GP3 and MD2 pineapple clones. The structure was based on a completely randomized design with 3 factors, namely clone (GP3 and MD2), decrowning (crown and crownless), and coating [50 mg L-1 ABA, 1% chitosan, ABA+Chitosan mixture, and control (H2O)]. The results showed that the MD2 had a lower IB incidence and higher TPC than the GP3 stored at 7°C for 37 days. The increased TPC was positively correlated with IB incidence. TPC was also negatively correlated with ABA but positively with endogenous GA3 2 weeks earlier. Coating with 50 mg L-1 ABA and 1% chitosan on MD2 decreased IB incidence. Pineapple crown pruning decreased ABA and increased TPC, GA3, and IB incidence.

12

Effects of fruit maturities, coatings, and storage temperatures on the qualities and green-life of Cavendish banana

Fahri Alamanda Katartika, Widodo Soesiladi Esti, Waluyo Sri, Zulferiyenni

Acta Innovations

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2023

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no. 47

56--63

EN

Cavendish banana is a climacteric fruit with a fast response to ethylene and a very high respiration rate during storage. Previous studies revealed that these characteristics shortened the green-life and fastened fruit damage, affecting the economic value. Therefore, this study aims to examine the effects of fruit maturity levels, coatings, and storage temperatures on the qualities and green-life of Cavendish banana. The result showed that the level of fruit maturity significantly increased the green-life duration, as well as maintained firmness, diameter loss, acidity, and starch content, but it had no effect on weight loss, oBrix, and glucose. Meanwhile, low temperature was able to delay senescence, promote starch degradation, as well as detain firmness and diameter loss. The results also showed that the combined application of maturity levels + temperatures affected all parameters, while maturities + coatings as well as coatings + storage had effects on firmness, acidity, and starch content. The 1% chitosan coating coverage was analyzed with a Scanning Electron Microscope (SEM), which showed fully covered surface of M1 finger rind tip and some crack points on finger rind base. Furthermore, there was full coverage on M2, and some crack points on M3.

13

Tribological Properties of the Friction Pair with a-C:H Coating under the Conditions of Lubrication with 10W40 Biodegradable Engine Oil

Hadło Krystian, Lubas Janusz

Tribologia

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2022

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nr 2

15--22

EN

The present study discusses the influence of an a-C:H coating on the tribological parameters of sliding pairs under mixed friction. Using the PVD method, the a-C:H coating was formed on specimens made from AISI 4337 steel. The sliding friction and wear process was carried out on the pairs of AISI 4337 steel and SAE48 bearing alloy, which were lubricated with 10W40 biodegradable engine oil. The investigation showed significant differences in the friction coefficient and temperature in the tested pairs with the steel surface layer and the a-C:H coating. In the friction pairs with the a-C:H coating, the tested parameters of friction were higher than in pairs with the steel surface layer. The pairs with the a-C:H coating showed more intensive wear of the SAE-48 bearing alloy than those with a steel surface. The surface layer used in a friction pair leads to the deterioration of the lubricating properties of engine oil and reduces its resistance to scuffing.

PL

W pracy przedstawiono wpływ powłoki a-C:H na parametry tribologiczne par ciernych w warunkach tarcia mieszanego. Powłoka a-C:H została wytworzona na próbkach wykonanych ze stali AISI 4337 metodą PVD. Proces tarcia ślizgowego i zużycia realizowano w skojarzeniu stal AISI 4337 i stop łożyskowy SAE-48 smarowanych biodegradowalnym olejem silnikowym 10W40. Badania wykazały istotne różnice w wartości współczynnika tarcia i temperatury w badanych parach ze stalową warstwą wierzchnią i powłoką a-C:H. W parach z powłoką a-C:H rejestrowane parametry tarcia były wyższe niż w parach ze stalową warstwą wierzchnią. Pary z powłoką a-C:H wykazywały intensywniejsze zużycie stopu łożyskowego SAE-48 niż pary z powierzchnią stalową. Warstwa wierzchnia zastosowana w parze ciernej prowadzi do pogorszenia właściwości smarnych oleju silnikowego i zmniejsza jego odporność na zacieranie.

14

Influence of a Steel Substrate Surface Roughness on the Mechanical Properties of a Peek Coating Deposited with the Electrophoretic Method

Otto Mateusz, Fiołek Aleksandra, Zimowski Sławomir

Tribologia

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2022

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nr 2

33--44

EN

The mechanical properties, adhesion and roughness of polymer coatings depend on many factors, including the unevenness of the substrate surface. Nevertheless, the influence of the substrate surface roughness is related to the coating type and substrate material and the used deposition method. Therefore, the effect of the surface roughness of a structural steel substrate on the mechanical properties of a PEEK coating is ambiguous. The indentation tests conducted show that, at a specific load of the indenter, the roughness of the steel substrate surface does not significantly affect the Vicker’s hardness of the tested PEEK coatings. The average Vicker’s hardness and elastic modulus are approximately 300 MPa and 5.6 Gpa, respectively, at the lowest of the applied loads, regardless of the surface roughness level of the steel substrate. Nevertheless, the surface roughness of the steel substrate after fine grinding of Ra = 0.21 μm, compared to the polished one with Ra = 0.005 μm, meant that adhesion improved, and the scratch hardness increased by approximately 130 to 370 [MPa] of the PEEK coating.

PL

Właściwości mechaniczne, przyczepność oraz chropowatość powłok polimerowych zależą od wielu czynników, a w tym od nierówności powierzchni podłoża. Niemniej jednak wpływ wielkości chropowatości powierzchni podłoża okazuje się być związany z rodzajem materiału powłokowego i podłoża oraz zastosowaną metodą osadzania. Wobec tego oddziaływanie chropowatości powierzchni podłoża ze stali konstrukcyjnej na właściwości mechaniczne powłoki PEEK osadzanej elektroforetycznie nie jest jednoznaczny. Przeprowadzone badania indentacyjne wskazują, że przy określonym obciążeniu wgłębnika chropowatość powierzchni stalowego podłoża nie wpływa znacząco na twardość Vickers’a badanych powłok PEEK. Średnia twardość Vickers’a i modułu sprężystości wynosi odpowiednio ok. 300 MPa i 5.6 GPa przy najmniejszym z zastosowanych obciążeń, niezależnie od mikronierówności powierzchni stalowego podłoża. Nie mniej jednak większa chropowatość powierzchni stalowego podłoża po szlifowaniu dokładnym rzędu Ra = 0.21 μm, względem polerowanego o Ra = 0.005 μm, przełożyła się na polepszanie adhezji i spowodowała wzrost twardości zarysowania powłoki PEEK z ok. 130 do 370 [MPa].

15

Nowa zaawansowana powłoka dla powierzchni dachowych, zapewniająca całoroczny komfort cieplny i oszczędność energii w budynkach

Szkło i Ceramika

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2022

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R. 73, nr 1

67--68

16

Formation of coatings with technologies using concentrated energy stream

Radek Norbert, Kalinowski Artur, Pietraszek Jacek, Orman Łukasz J., Szczepaniak Marcin, Januszko Adam, Kamiński Janusz, Bronček Jozef, Paraska Olga

Production Engineering Archives

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2022

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Vol. 28, Iss. 2

117--122

EN

A number of modern surface processing methods use an energy flux. The examples include electro-spark deposition (ESD) and laser beam processing (LBP). The work concerns the study of Cu-Mo coatings deposited on C45 carbon steel, which were then eroded with a laser beam. The analysis included the analysis of the microstructure, measurements of macrogeometry and microhardness, corrosion resistance tests of selected areas after laser treatment. The coatings were applied with ELFA-541 and subjected to Nd:YAG laser treatment with variable laser parameters. The problem presented in the work can be used to extend the knowledge of the areas of application of ESD coatings, especially in sliding friction pairs.

17

Aging behavior of the three-proof polyurethane coating under UV radiation

Wang Jianfa, Gu Zheng, Zhao Jie, Zhang Susu, Li Peiyao, Meng Chao, Sui Jinyong, Zhang Xiaoyi, Hu Shaokai, Pan Jiaying, Li Junyi

Polimery

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2022

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Vol. 67, nr 9

433--437

EN

The influence of UV radiation on the gloss, structure (SEM, FTIR), thermal (TGA, DTG) and mechanical properties of polyurethane resins and the three-layer protective coating made of them was investigated. The gloss of the resins was greater than that of the protective coating. UV radiation has been proven to reduce gloss (at 1,200 hours irradiation, 81.3° to 8.9° for resins, and 61.1° to 2.8° for coating).The tensile strength of the resins decreased during aging, and the relative elongation at break after reaching the minimum was increased (at the irradiation time of 100 h). In the case of coating, both the tensile strength and elongation decreased during aging and, after reaching the minimum they increased (at the irradiation time of 800 h), reaching the maximum (at the irradiation time of 1000 h), and then decreased.

PL

Zbadano wpływ promieniowania UV na połysk, strukturę (SEM, FTIR), właściwości termiczne (TGA, DTG) i mechaniczne żywic poliuretanowych oraz wykonanej z nich trójwarstwowej powłoki ochronnej. Połysk żywic był większy niż powłoki ochronnej. Potwierdzono, że promieniowanie UV zmniejsza połysk (przy naświetlaniu przez 1200 godzin, w przypadku żywic z 81,3° do 8,9°, a w przypadku powłok z 61,1° do 2,8°). Wytrzymałość na rozciąganie żywic zmniejszała się w trakcie starzenia, a wydłużenie względne przy zerwaniu po osiągnięciu minimum zwiększało (przy czasie naświetlania 100 h). W przypadku powłoki zarówno wytrzymałość na rozciąganie, jak i wydłużenie zmniejszały się w trakcie starzenia i po osiągnięciu minimum zwiększały (przy czasie naświetlania 800 h), osiągając maksimum (przy czasie naświetlania 1000 h), a następnie zmniejszały.

18

Enhancement of corrosion resistance of stainless steel with Zn doped silane coatings

Owczarek Edyta

Ochrona przed Korozją

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2022

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nr 12

373--377

EN

Blank silane films are not able to provide long-term corrosion protection. As is known, dopants with corrosion inhibiting properties can be added to the silane sol-gel network in order to increase their corrosion resistance. The present work investigates the protective properties of air-aged films obtained from a solution of isobutyltriethoxysilane (IBTES) doped with 0.01 mol/l and 0.1 mol/l zinc nitrate Zn(NO3)2 ∙ 6H2O prepared on an X20Cr13 stainless steel substrate. The surface morphologies, adhesion to the substrate and the corrosion resistance of the obtained films in an 0.5 M Cl− solution were examined. The experimental results showed that IBTES films doped with 0.01 mol/l zinc nitrate deposited on the surface of stainless steel had better protective properties, while those doped with 0.1 mol/l of the inhibitor had worse protective properties against local corrosion compared to blank IBTES film.

PL

Powłoki silanowe nie są w stanie zapewnić długotrwałej ochrony przed korozją. Jak wiadomo, do sieci zol-żel silanu można dodawać domieszki o właściwościach hamujących korozję w celu zwiększenia ich odporności na korozję. W pracy zbadano właściwości ochronne starzonych w powietrzu powłok otrzymanych z roztworu izobutylo- trietoksysilanu (IBTES) domieszkowanych 0,01 mol/l i 0,1 mol/l azotanu cynku Zn(NO3)2 ∙ 6H2O wytworzonych na podłożu ze stali nie- rdzewnej X20Cr13. Zbadano morfologię powierzchni, przyczepność do podłoża oraz odporność korozyjną otrzymanych filmów w 0,5M roztworze Cl−. Badania eksperymentalne wykazały, że powłoki IBTES domieszkowane 0,01 mol/l azotanu cynku osadzone na powierzchni stali nierdzewnej miały lepsze właściwości ochronne przed korozją lokalną w porównaniu z powłoką IBTES, natomiast domieszkowane 0,1mol/l inhibitora – gorsze.

19

Wpływ pigmentów luminescencyjnych na trwałość systemu powłokowego

Michalski Marek, Szczepaniak Marcin

Obróbka Metalu

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2022

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Nr 4

37--41

PL

W artykule przedstawiono rezultaty badań dotyczących cech użytkowych powierzchni pokrytych powłokami, przy czym nanoszenie powłok przyjęto jako jeden z rodzajów obróbki przyrostowej. Analizowano wpływ obecności i sposobu dozowania pigmentów na trwałość nanoszonych powłok w systemach transportowych.

EN

In this paper the results of a study on the performance characteristics of coated surfaces was presented, where coating was chosen as a type of additive treatment. Analysis of the influence of pigments and dosage on the durability of the coatings applied In transport systems was carried out.

20

Antimicrobial Efficiency of Novel Active Packaging Based on Iron Nanoparticles Biosynthe-sized by Oregano Leaves Extract

Mikołajczak Anna, Ligaj Marta

Journal of Research and Applications in Agricultural Engineering

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2022

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Vol. 67, nr 1

5--7

EN

The main function of packaging materials for food is to ensure the safety and maintain appropriate, required quality. The use of active packaging, including those containing antibacterial materials or substances with antimicrobial properties, may extend the shelf life. Many of the available and used solutions are based on the application of polymer films with the addition of metal nanoparticles such as silver, gold, copper or metal oxides of magnesium, zinc and titanium. However, the aspect related to the use of iron nanoparticles is rarely found in research or publications. The aim of the research was to determine the antimicrobial effectiveness of packaging materials (parchment and foil) modified with the active layer based on an iron preparation by reducing iron salts with the use of oregano extract. Prototype packaging materials were used to carry out storage tests with the cottage cheese. The pieces of cheese were kept refrigerated for 6 weeks. During the storage tests, microbiological inoculations were performed from the surface of the packaging in contact with the product. The obtained results confirmed the antimicrobial effectiveness of the tested packages.