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Nitration of Calixcrown 6 Influence on Extracting Abilities. Use of Cesium Salts for Detection of Crown Ether Macrocycles with the Electrospray Ionization Mass Spectrometry Technique

Jankowski C., Dozol J. F., Allain F., Tabet J. C., Ungaro R., Casnati A., Vicens J., Asfari A., Boivin J.

Polish Journal of Chemistry

2002

Vol. 76 / nr 5

701-711

Two organic synthetic reactions - mononitration and phosphorylation of crown-6 compounds were performed under Cs+ cation monitoring via in situ complexation using electrospray ionization mass spectrometry (ESI-MS). Formation of Cs+ complexes is a rapid analytical tool for characterization of complex reaction mixtures.