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Flotation behaviour and surface characteristic of anosovite in a sodium oleate solution

Wang Y., Wen S., Zhang J., Wu D., Xian Y., Shen H.

Physicochemical Problems of Mineral Processing

2017

Vol. 53, iss. 2

714--723

Properties of anosovite in titanium slag, anosovite flotation response in a collector solution of sodium oleate, and adsorption behaviour of sodium oleate on the mineral surface were studied in the present work using XRD, Raman spectra, flotation tests, zeta potential analysis, FTIR and XPS. The results show that the anosovite crystal contains magnesium, and its chemical composition is Mg0.09Ti2.91O5. The chemical bonds on the anosovite surface mainly comprise Ti-O bonds. Micro-flotation tests indicate that anosovite has better floatability at a wide pH range and the recovery reaches 88% at pH=6, when the dosage of sodium oleate is only 4·10−6 mol/dm3. The point of zero charge of anosovite was determined near pH 3.2 by the zeta potential measurement. In the flotation process, chemical adsorption occurs between the carboxyl of sodium oleate and the titanium sites on the anosovite surface.

Deashing and desulphurization of fine oxidized coal by falcon concentrator and flotation

Zhu X., Tao Y., Sun Q., Man Z., Xian Y.

Physicochemical Problems of Mineral Processing

2016

Vol. 52, iss. 2

634--646

Flotation and enhanced gravity separation based on different separation principles were carried out to investigate the desulphurization and deashing efficiency of fine oxidized coal. Surface properties of fresh and oxidized coals were tested by XPS and results showed that the contents of hydrophobic functional groups decreased while the content of hydrophilic functional groups increased after oxidization. Floatability and density analysis results showed that the floatability of coal samples decreased sharply because of oxidation, however, density composition of coal sample only had slight changes. Separation results showed that yields of gravity concentrates outclassed that of flotation concentrates, meanwhile, ash contents and sulfur contents of gravity concentrates were far lower than that of flotation concentrates. Yields and ash contents increased with the collector dosage and achieved to be 17.83 and 26.94% respectively when the collector dosage was 1600 g•Mg-1. Yields and ash contents of gravity concentrates decreased with the centrifugal force and increased with the recoil water flow with similar sulfur content. Clean coal with yield of 53.86%, ash content of 9.81%, sulfur content of 1.47% and with a corresponding desulphurization efficiency of 44.53% was achieved at centrifugal force of 107 g and recoil water flow of 13.3 dm3•min-1. For fine oxidized coal, enhanced gravity separation has a significant advantage of the separation efficiency compared with flotation.