W pracy przedstawiono proces regeneracji matryc do wyciskania profili aluminiowych, które klasycznie w firmie Albatros Aluminium są poddawane zazwyczaj wielokrotnemu azotowaniu gazowemu, aż do końcowego zużycia. W artykule starano się wyjaśnić przyczynę zwiększonej trwałości matryc po trzecim lub czwartym azotowaniu. Struktura i twardości oceniane podczas badania matryc wykonanych aktualnie stosowaną technologią azotowania pozwalają stwierdzić, że uzyskana grubość warstwy oraz przede wszystkim budowa warstwy (np. stężenie azotu, rodzaj węglikoazotków).
EN
In this work, the regeneration process of dies used in the extrusion of aluminium profiles has been presented. Traditionally, at the Albatros Aluminium company, dies are usually subjected to multiple gas nitriding until they are ultimately worn out. In the article, it was sought to explain the cause of increased die durability after the third or fourth nitriding. The structure and hardness assessed during tests of dies made with current nitriding technology make it possible to state that the causes are: the obtained thickness of the layer, and above all, the structure of the layer (e.g. nitrogen concentration, type of carbonitrides).
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A new method of obtaining a ZnO-SiO2 synthetic composite from emulsion systems is described. The reagents were solutions of sodium silicate and zinc sulphate, cyclohexane was used as an organic solvent and non-ionic surfactants as modifiers. The influence of the mode of reagents dosing and type of emulsifiers on the physicochemical properties, structure and particle size of ZnO-SiO2 was evaluated. The choice of the optimum emulsifier or mixture of emulsifiers and their amounts needed for the process of precipitation and ensuring getting products of uniform particles and the smallest possible size was proposed. The ZnO-SiO2 composite obtained was characterised by micrometric particle size. The oxide composites obtained were subjected to thorough analyses to determine their physicochemical properties, dispersion and morphology. Particle size distributions were evaluated by the NIBS technique and laser diffraction method. The products were also characterised by sedimentation profiles, wettability with water and colorimetric analyses, determination of bulk density or ZnO and SiO2 contents.
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