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Quantitative X-Ray Diffraction Analysis of Zn-Al Based Alloys

Gogola P., Gabalcová Z., Suchánek H., Babinec M., Bonek M., Kusý M.

Archives of Metallurgy and Materials

2020

Vol. 65, iss. 2

959--966

The paper describes modification to Fm3 ̅m (space group no. 225) lattice of aluminium based α-solid solution observed in Zn-Al alloys required to properly correlate quantitative data from X-ray diffraction analysis with results obtained from quantitative scanning electron microscopy image analysis and those predicted from Zn-Al binary phase diagram. Results suggests that 14 at.% of Zn as a solute atom should be introduced in crystal lattice of aluminium to obtain correct estimation of phase quantities determined by quantitative X-ray diffraction analysis. It was shown that this modification holds for Cu mould cast as well as annealed and water-cooled samples of Zn-3wt.%. Al and Zn-5wt.% Al.