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Charakterystyki wzbudzeniowo-emisyjne nanometrycznych proszków tlenku cyrkonu domieszkowanych jonami itru, europu i prazeodymu

Mierczyk Z., Kałdoński G., Mierczyk J., Łojkowski W., Fidelus J. D., Opalińska A.

Biuletyn Wojskowej Akademii Technicznej

2011

Vol. 60, nr 1

7-14

W pracy przedstawiono wyniki badań materiałów luminescencyjnych na osnowie dwutlenku cyrkonu, domieszkowanych jonami itru, europu i prazeodymu, przeznaczonych do nowoczesnych półprzewodnikowych źródeł światła białego. Przeprowadzono pomiary charakterystyk wzbudzeniowo-emisyjnych i wyznaczono podstawowe parametry optyczne luminoforów.

In this paper we focus on high-impact luminescence of Eu²⁺ or Pr²⁺doped ZrO₂ nanocrystals stabilized by Y₂O₃. As a class of inorganic luminescent phosphor, wide-band gap ZrO₂ has received considerable attention because of its utility for existing and future optoelectronic devices as a suitable host for rare-earth ions. In the article were gathered Exciting-emitting spectra of nanocrystals obtained by the hydrothermal microwave-driven process are presented. All investigated characteristics indicate the usability of studied materials as red luminescent phosphors.

Positron-annihilation and photoluminescence studies of nanostructured ZrO2

Fidelus J. D., Karbowski A., Mariazzi S., Brusa R. S., Karwasz G.

Nukleonika

2010

Vol. 55, No. 1

85-89

In the present work, photoluminescence and Doppler broadening depth-resolved positron annihilation spectroscopy was performed on pure zirconia nanopowders. Zirconia nanopowders were grown by a hydrothermal microwave-driven process followed by annealing in oxygen atmosphere. Photoluminescence under 274 nm wavelength excitation from a 150 W high-pressure Xe exhibits similar spectra, in the region from 320 to 820 nm, although its intensity depends on the annealing. Positron annihilation Doppler-broadening spectra show low values of the normalized S-parameter, varying little with the depth, from 0.495 on the surface to 0.47-0.49 in bulk. Both high the annealing temperature and oxygen concentrations, lead to low bulk S-values. The ortho-positronium (o-Ps) fraction is about 10-11% for all samples on the surface, whereas it is reduced to 7-8% in the bulk for samples annealed at 700°C and 5-6% for samples annealed at 800°C. Both photoluminescence (PL) and positron studies show the presence of defects in all samples. The o-Ps signal suggests a high porosity of samples, particularly at a depth down to 10 nm.