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Thermoelectric properties of bismuth-doped magnesium silicide obtained by the self-propagating high-temperature synthesis

Bucholc Bartosz, Kaszyca Kamil, Śpiewak Piotr, Mars Krzysztof, Kruszewski Mirosław J., Ciupiński Łukasz, Kowiorski Krystian, Zybała Rafał

Bulletin of the Polish Academy of Sciences. Technical Sciences

2022

Vol. 70, nr 3

art. no. e141007

Doping is one of the possible ways to significantly increase the thermoelectric properties of many different materials. It has been confirmed that by introducing bismuth atoms into Mg sites in the Mg2Si compound, it is possible to increase career concentration and intensify the effect of phonon scattering, which results in remarkable enhancement in the figure of merit (ZT) value. Magnesium silicide has gained scientists’ attention due to its nontoxicity, low density, and inexpensiveness. This paper reports on our latest attempt to employ ultrafast self-propagating high-temperature synthesis (SHS) followed by the spark plasma sintering (SPS) as a synthesis process of doped Mg2Si. Materials with varied bismuth doping were fabricated and then thoroughly analyzed with the laser flash method (LFA), X-ray diffraction (XRD), scanning electron microscopy (SEM) with an integrated energy-dispersive spectrometer (EDS). For density measurement, the Archimedes method was used. The electrical conductivity was measured using a standard four-probe method. The Seebeck coefficient was calculated from measured Seebeck voltage in the sample subjected to a temperature gradient. The structural analyses showed the Mg2Si phase as dominant and Bi2Mg3 located at grain boundaries. Bismuth doping enhanced ZT for every dopant concentration. ZT = 0.44 and ZT=0.38 were obtained for 3wt% and 2wt% at 770 K, respectively.

Porous volumetric structures obtained by additive manufacturing technologies

Kaszyca Kamil, Danilczuk Wojciech, Zybała Rafał

Materiały Elektroniczne

2019

T. 47, nr 1-4

15--21

The goal of our work was to develop bulk structures characterized by a variable, controlled porosity, using additive manufacturing techniques (3D printing). A technology for the fabrication of bulk materials with controllable porosity has been developed. For that purpose, the samples with constant porosity were designed and then prepared, which allowed us to learn the possible limit values. Thus, we were able to optimize the design process at the stage of the preparation of the gradient structures.

Niniejsza praca przedstawia proces opracowanie struktur przestrzennych charakteryzujących się zmienną, sterowaną porowatością, z wykorzystaniem technik wytwarzania przyrostowego (druku 3D). W ramach pracy opracowana została technologia wytwarzania materiałów o sterowanej porowatości. W tym celu zaprojektowane i wykonane zostały próbki o stałej porowatości. Pozwoliło to na poznanie możliwych do uzyskania wartości granicznych, co w konsekwencji skutkowało możliwością optymalizacji procesu projektowania na etapie tworzenia struktur gradientowych.