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TiO2 immobilised on biopolymer nanofibers for the removal of bisphenol A and diclofenac from water

Kudlek E., Silvestri D., Wacławek S., Padil V. V. T., Stuchlík M., Voleský L., Kejzlar P., Černík M.

Ecological Chemistry and Engineering. S

2017

Vol. 24, nr 3

417--429

Recently electrospinning has gained significant attention due to unique possibilities to produce novel natural nanofibers and fabrics with controllable pore structure. The present study focuses on the fabrication of electrospun fibres based on gum karaya (GK), a natural tree gum, with polyvinyl alcohol (PVA), and functionalization of the membrane with TiO2 nanoparticles with further methane plasma treatment. The GK/PVA/TiO2 membrane was analyzed with several techniques including: fourier-transform infrared spectroscopy (FTIR), thermogravimetric analysis (TGA), scanning electron microscopy with energy dispersive X-ray spectroscopy (SEM-EDX), and water contact angle, in order to characterize its morphological and physicochemical properties. The GK/PVA/TiO2 membrane was further successfully used for the degradation (under UV irradiation) of bisphenol A and diclofenac from aqueous solution. It was also observed that the degradation kinetics of these compounds are faster in comparison to the UV treatment alone.

Non Destructive Evaluation of Surface Integrity Produced by Milling and Grinding Using Barkhausen Noise Signals

Neslusan M., Kejzlar P., Cllikova M., Micietova A.

Journal of Machine Engineering

2015

Vol. 15, No. 2

82--91

This paper deals with investigation of hard milled and ground surfaces via non destructive Barkhausen noise (BN) technique. The paper compares the raw BN signals, extracted BN features such as effective (rms) values and appearance of hysteresis loops produced by grinding and milling cycles. Information about surface state is correlated and confronted with metallographic observations, SEM readings as well as residual stress state. The paper also discusses the specific character of BN signals (and the corresponding BN features) produced by hard milled surface as a result of the magnetic shape memory effect when the machined surface undergoes severe plastic deformation at elevated temperatures.