Thermally- and deformation-induced nanocrystallization has been investigated in marginally glass forming Al-rich alloys. Conventional calorimetry and microcalorimetry results coupled with detailed and quantitative microstructure analyses using dark-field and high-resolution transmission electron microscopy yielded a quantitative description of the kinetics of nanocrystallization in its earliest stages. These results form the basis for the development of advanced processing strategies to synthesize amorphous/nanocrystalline composite structures with even higher nanocrystal number densities, potentially giving rise to increased stability and improved performance of these new materials.
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