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1 Bulletin of the Polish Academy of Sciences. Technical Sciences

1 2014

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Synthesis, characterization and catalytic properties of SAPO-11 molecular sieve synthesized in hydrothermal media using di-isopropylamine as template

Chellappa T., Costa M. J. F., Nascimento W. A., Ferreira De Lima L., Bassan I. A., Tavares M., Fernandes V. J., Menezes A., Guilherme Meira L., Telesforo Nóbrega De Medeiros J., Maribondo Do Nascimento R.

Bulletin of the Polish Academy of Sciences. Technical Sciences

2014

Vol. 62, nr 3

481--488

A microporous SAPO-11 Molecular sieve was successfully synthesized by the hydrothermal method, using a single agent, as an organic template: di-isopropylamine (DIPA). The obtained solid was calcined at 550◦C for three hours, after which the flow of nitrogen was exchanged for that of synthetic air and submitted for another ten hours of calcination, so as to remove the single agent: di-isopropylamine, which after the removal of the template could be observed by the high crystallization of the sample. Furthermore, the molecular sieve was characterized by XRD, SEM, TG-DTG and N2 adsorption desorption (BET analysis). The obtained catalyst proved to have a high potential catalytic activity and selectivity, through the obtained characterization results, exhibiting good hydrothermal stability. The catalytic performance of SAPO-11 was tested by the deactivation/regenerability of the coked sample, furthered by cracking of n-hexane reaction and high olefins selectivity was obtained.