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The internal dose rate in quartz grains: experimental data and consequences for luminescence dating

Szymak Agnieszka, Moska Piotr, Poręba Grzegorz, Tudyka Konrad, Adamiec Grzegorz

Geochronometria

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2022

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Vol. 49, no. 1

9--17

EN

This work considers the impact of the internal alpha and beta dose rates in quartz grains obtained from sandy sediments on the results of luminescence dating. The internal dose rates reported here (ca. 0.01–0.21 Gy · ka−1) play a particularly important role, because of low (ca. 0.8–0.9 Gy · ka−1) or very low (ca. 0.4–0.6 Gy · ka−1) external dose rates. In these cases, the internal dose rates form a significant fraction of the total dose rates, often exceeding 10%. Ignoring this contribution would have made the considered luminescence ages artificially older. In our study, we measure both the internal alpha and beta contributions as the latter is usually neglected in the case of quartz. The dose rate measurements were performed using the innovative μDose system.

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Evaluating the effect of hydrofluoric acid etching on quartz grains using microscope image analysis, laser diffraction and weight loss particle size estimate

Poręba Grzegorz, Tudyka Konrad, Szymak Agnieszka, Pluta Julia, Rocznik Joanna, Świątkowski Jakub, Osadnik Rafał, Moska Piotr

Geochronometria

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2022

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Vol. 49, no. 1

1--8

EN

In this work we investigate the quartz etching process using hydrofluoric acid for trapped charge dating (TCD) applications. It is done using material collected from an active sand mine in Bełchatów Nowy Świat, central Poland. Approximately 20 kg of material was collected and prepared using routine procedures that are applied in TCD laboratories. The material was sieved using 180–200 μm meshes, and the selected fraction was etched for various time intervals. Sieved samples were etched for durations from 0 min up to 180 min and measured with microscope image analysis (IA), laser diffraction (LD), and mass loss which were used to estimate the depths of etching. Our results show statistical data on how non-uniform the etching process is. We estimate this as a function of etching time from IA, LD and mass loss. In our investigation, mass loss measurements with the assumption of spherical grains correspond to the decrease of radius of ca. 0.151 ± 0.003 μm ˑ min–1. In case of LD, a rough etch depth estimation corresponds to a range 0.06–0.18 μm ˑ min–1 with median at 0.13 μm ˑ min–1. Microscope IA gives a 0.03–0.09 μm ˑ min–1 with a median at 0.05 μm ˑ min–1. Moreover, quartz grains are fractured into smaller pieces while etching. It means that assumptions that are used in etch depth estimation from mass loss are not correct. They incorrect not only because grains are not spheres but also because the number of grains is not constant. Therefore, the etch depth estimated from mass loss might be overestimated. Using microscope IA we report etch depth ranges that might be used to roughly estimate the etch depth uncertainty.

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Luminescence dating procedures at the Gliwice Luminescence Dating Laboratory

Moska Piotr, Bluszcz Andrzej, Poręba Grzegorz, Tudyka Konrad, Adamiec Grzegorz, Szymak Agnieszka, Przybyła Aleksandra

Geochronometria

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2021

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Vol. 48, no.1

1--15

EN

The Gliwice Luminescence Laboratory (GLL) is a part of the Institute of Physics – Centre for Science and Education at the Silesian University of Technology, which has gradually evolved since the 1980s. To date, nearly 3500 samples have been dated using luminescence from materials such as ceramics, bricks, and sediments from archaeological and geological sites. Currently, the laboratory is equipped with four luminescence readers and three gamma spectrometers, allowing luminescence dating of approximately 300 samples annually for the needs of research projects. This article focuses on the laboratory procedures used in GLL to obtain luminescence ages. Recent improvements of the GLL's facilities and new equipment, as well as the performance spanning the Laboratory's 30 years of activity, are discussed in terms of obtained results and the involvement in national and international projects.

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Fluvial response to environmental conditions during MIS 4-3 : a sedimentary record at the Brześnica site, central-western Poland

Moskalewicz Damian, Tylmann Karol, Woźniak Piotr Paweł, Kopyść Natalia, Moska Piotr

Geological Quarterly

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2020

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Vol. 64, No. 4

915--930

EN

Fluvial deposits subjected to this study are exposed at the Brześnica site, in the south-western part of the Wielkopolska region in Poland, which was close to the ice-sheet limit during the Last Glacial Maximum (LGM). Sedimentological analyses, including lithofacies descriptions, palaeocurrent measurements, grain size and rounding analyses and heavy mineral compositions indicate that the fluvial deposits at Brześnica were deposited in braided river environment. The following fluvial sedimentary processes were inferred: (1) shallow, rapid flow alternating with waning flow, (2) infilling of erosional channels with fluvial sediments during flood events, (3) changes from supercritical to subcritical flows, and (4) shallow sheet floods. The results of OSL dating indicated sediment deposition ~65.2 ±1.5 ka, i.e. in MIS 4, that was here characterized by cold environmental conditions and a general shift from meandering to braided fluvial sedimentation style. This finding contrasts with accumulation/erosion phases interpreted previously in this region for that time interval; however, it is consistent with recent studies of fluvial systems functioning during MIS 5-2 and of factors responsible for sedimentation style.

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Erosion and accumulation phases during the last glacial-interglacial cycle : a case study of the terrace system of the Odra and Osobłoga rivers (southern Poland)

Wójcicki Krzysztof Jan, Pawelec Halina, Malik Ireneusz, Woskowicz-Ślęzak Beata, Moska Piotr

Geological Quarterly

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2020

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Vol. 64, No. 1

104--119

EN

In the Odra and Osobłoga River valleys in the vicinity of the town of Krapkowice, a system of morphological levels is present which is exceptionally extensive compared to other such systems in southern Poland. The extent, origins and chronology of these levels have been the subject of many controversies. In the light of current research, the terraces, which are situated on average 14.5-13, 12-10, 8-6, 6-4 and 3-1 metres above the river level, were formed in the post-Wartanian interval. The main factor driving their development was erosion, which compensated for the effects of large-scale aggradation that had occurred during the anaglacial phase of the Odranian Glaciation (MIS 8) dated to 261 ±15 ka. The impact of climatic conditions on the trends towards fluvial erosion or accumulation was only of secondary importance. According to OSL dating, successive phases of vertical stabilisation of the valley floor occurred ~118.8 ±8.3, 87.7 ±5.7 and 42.0 ±2.0 ka. In the meantime, erosion intensified, which resulted in the formation of lower terrace levels. During the climatic minimum of the Upper Plenivistulian (21.5 ±1.5 ka), under conditions of the delivery of sheet-wash-generated sediment, the aggradation of distal reaches of the Odra River valley was locally marked. During the Late Vistulian and Holocene, erosive tendencies continued, which were reflected by the fact that the surfaces of subsequent inset alluvial fills were situated ever lower. In the light of dating results, it can be concluded that during the colder periods correlated with the Rederstall Stadial (MIS 5b) and with the Hasselo Stadial (MIS 3), a braided river was present in the river valleys examined, which was most probably accompanied by permafrost. During the Eemian Interglacial (MIS 5e), during the Late Vistulian Interstadials and in the Holocene, it was a meandering river.

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Chronostratigraphy of Late Glacial aeolian activity in SW Poland – A case study from the Niemodlin Plateau

Moska Piotr, Jary Zdzisław, Sokołowski Robert Jan, Poręba Grzegorz, Raczyk Jerzy, Krawczyk Marcin, Skurzyński Jacek, Zieliński Paweł, Michczyński Adam, Tudyka Konrad, Adamiec Grzegorz, Piotrowska Natalia, Pawełczyk Fatima, Łopuch Michał, Szymak Agnieszka, Ryzner Kamila

Geochronometria

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2020

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Vol. 47, no.1

124--137

EN

The stratigraphy of Late Pleniglacial and Late Glacial fluvio-to-aeolian succession was investigated in two sites located at the Niemodlin Plateau, SW Poland. Lithofacial analysis was used for the reconstruction of sedimentary environments. An absolute chronology for climatic change and the resulting environmental changes were determined based on optically stimulated luminescence (OSL – nine samples) and radiocarbon (three samples) dating methods. Four phases of changes in sedimentary environments were established. The first depositional phase correlates with the Last Permafrost Maximum (24−17 ka) based on the type and size of the periglacial structures, which aggraded under continuous permafrost conditions. During 17.5−15.5 ka (upper Late Pleniglacial), a stratigraphic gap was detected, owing to a break in the deposition on the interfluve area. The second depositional phase took place during 15.5−13.5 ka. During this phase, the first part of the dune formation (Przechód site) and fluvio-aeolian cover (Siedliska site) was deposited. The sedimentary processes continued throughout the entire Bølling interstadial and Older Dryas. In the third phase (Allerød interstadial), soil formation took place. At the Siedliska site, palaeosol represented Usselo soil type, whereas at the Przechód site, there was a colluvial type of soil. The last phase (Younger Dryas) is represented by the main phase of dune formation in both sites. After the Younger Dryas, no aeolian activity was detected. High compliance with both absolute dating methods was noticed.

7

Luminescence dating of Quaternary sediments – some practical aspects

Moska Piotr

Studia Quaternaria

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2019

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Vol. 36, Nr 2

161--169

EN

Luminescence dating is based mainly on the dosimetric properties of quartz and feldspar. These minerals are among the most popular found on Earth, resulting in the possibility of using luminescence methods in practically any environment. Currently, quartz remains the best recognized mineral in terms of dosimetric properties, particularly with regards to results obtained for quartz grains, which are regarded as being the most reliable in luminescence dating. Supporters of luminescence methods are constantly growing, however, these groups do not always have sufficient knowledge to avoid even the most basic of issues that may be encountered overall – from the process of sampling through to the awareness of what a single luminescence result represents. The present paper provides an overview of several practical aspects of luminescence dating such as correct sampling procedures and all necessary information regarding the calculation of the dose rate and equivalent dose with particular reference to potential problems that occur when the age of the sample is being determined. All these aspects are crucial for obtaining a reliable dating result, on the other hand, they remain a potential source of uncertainty.

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Chronology of the last ice sheet decay on the southern Baltic area based on dating of glaciofluvial and ice-dammed lake deposits

Uścinowicz Szymon, Adamiec Grzegorz, Bluszcz Andrzej, Jegliński Wojciech, Jurys Leszek, Miotk-Szpiganowicz Grażyna, Moska Piotr, Pączek Urszula, Piotrowska Natalia, Poręba Grzegorz, Przezdziecki Piotr, Uścinowicz Grzegorz

Geological Quarterly

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2019

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Vol. 63, No. 1

193--208

EN

The paper presents the results of the first OSL dating of glaciofluvial and ice-marginal lake sediments which occur between end moraines of the Słupsk Bank and the Polish coast. The sand and gravel of glaciofluvial deltas on the Słupsk Bank were deposited most likely during a period from 14.3 ±1.2 to 16.6 ±1.4 ka ago. The deposition of silty-sandy sediments of the ice-marginal lake is dated at 14.51 ±0.81 and 14.6 ±1.4 ka years. Likewise, dates ranging from 13.74 ±0.84 to 16.70 ±1.1 ka obtained from low sandy ridges, related to the southern range of the ice-marginal lake in the Gardno-Łeba Lowland, indicate the most likely timing of their deposition. It can be concluded that a short stop of the ice sheet on the Słupsk Bank took place approximately 15.2 ka ago, which could be correlated with the position of the ice sheet front in central Skåne and in northern Lithuania at that time. Older and younger results were also obtained, except the dates mentioned above. The older ages show little sunlight exposure of sediments during their deposition. The younger dates indicate a marine origin of the sediments and show that some parts of glaciofluvial sediments were redeposited and exposed to sunlight at a later stage, most probably when dead-ice blocks were melting.

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Interpretation of soil erosion in a Polish loess area using OSL, 137Cs, 210Pbex, dendrochronology and micromorphology – case study: Biedrzykowice site (s Poland)

Poręba Grzegorz, Śnieszko Zbigniew, Moska Piotr, Mroczek Przemysław, Malik Ireneusz

Geochronometria

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2019

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Vol. 46, no. 1

57--78

EN

Loess areas used for agriculture are susceptible to soil erosion. The intensive process of soil erosion in Polish loess areas began with the onset of the Neolithic and has continued intermittently until today. This work presents the results of soil erosion from simultaneous use of the 137Cs and 210Pbex methods on an agricultural field located on loess slope. Moreover, to establish the age of accumulated sediment connected with water slope erosion, OSL dating, selected physicochemical and micromorphological analyses were applied. The reference values of the 137Cs and 210Pbex fallout for the studied site (Biedrzykowice, the Proszowice Plateau, Małopolska Upland) equal 2627 (45% connected with Chernobyl) and 4835 Bq·m–2, respectively. The results of the 137Cs and 210Pbex inventories measured for the agricultural field range from 730 to 7911 and from 1615 to 11136 Bq·m–2, respectively. The mean soil erosion is about 2.1 kg·m–2·a–1 (about 1.4 mm·a–1). The accumulation of the colluvial sediments started in the Neolithic and drastically increased in the Middle Ages. The examined gully catchment in Biedrzykowice has probably developed quite rapidly as a result of increased erosion. This resulted in the abandonment of this area as farmland and, consequently, in the minimization of water erosion on the slope due to the entrance of woody vegetation in this area. Erosion processes were highly intensified during the last 70 years as a result of deforestation after World War II and intensive agricultural reuse of this area after a break, as indicated by isotope measurements and dendrochronology.