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2 Physicochemical Problems of Mineral Processing

2 2021

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Sequential recovery processes of tungsten from hubnerite mineral concentrate of Qash Amir mineralized quartz veins, South Eastern Desert, Egypt

Abu Khoziem Hanaa Abdelaal

Physicochemical Problems of Mineral Processing

2021

Vol. 57, iss. 5

91--105

A hubnerite (MnWO4) mineral concentrate was prepared from the mineralized quartz veins of Gabal Qash Amir muscovite granite. This W- concentrate was chemically processed to obtain the more economic highly pure tungsten oxide. To accomplish this goal, two successive atmospheric agitation leaching processes were conducted. The first includes HCl acid agitation leaching to breakdown hubnerite mineral structure. The purpose was also to get rid of the associated Mn and Fe contents from one hand, and to prepare the more important intermediate tungstic acid from the other hand. From the latter, a sodium tungstate (Na2HWO4) leach liquor was adequately prepared after applying the second atmospheric NaOH agitation leeching process using the optimum conditions of 40% caustic soda concentration at solid/ liquid ratio of 1/3, 180oC for 2h. Finally, 7% Alamine 336 in kerosene was used for extracting 93.7% of W content under the studied optimum conditions of O/A ratio of 1/1, contact time 7 min at room temperature (20±5oC) and pH of 8.

Physical and chemical processes of Abu Rusheid cataclastic rocks for recovering niobium, zirconium and uranium compounds

Abdellah Walid Mahmoud, Khalafalla Mahmoud Sayed, Abu Khoziem Hanaa Abdelaal, El Hussain Omneya Mouhamed

Physicochemical Problems of Mineral Processing

2021

Vol. 57, iss. 5

137--152

Cataclastic rocks of Abu Rushied area (South Eastern Desert, Egypt) characterized by the presence of niobium, tantalum, zirconium minerals as well as uranium-thorium minerals. Physical upgrading process was applied using gravity and magnetic separation techniques to concentrate these economic minerals mainly to obtain the magnetic niobium concentrate at 0.2- 0.5 ampere, beside the non-magnetic Zr and U at 1.5 ampere. The chemical processing upon niobium concentrate was performed using NH4F roasting process at 250ºC followed by selective precipitation of Nb as Nb-sulfide. An alkaline fusion using NaOH was applied upon zirconium concentrate at the optimum conditions of: zircon concentrate/ NaOH mass ratio 1/2, fusion temperature of 650ºC and 2.5h fusion time followed by selective precipitation of Zr as Zr- tartrate. Finally, two flowsheets were drawn summarizing the whole recovery processes.