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1 2021

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Determination of acrylamide in foods by automatic accelerated solvent extraction and gas chromatography-mass spectrometry

Kang Cuicui, Ma Haijian, Li Yuan, Zhang Chizhong, Hong Yueqin, Shao Minghua

Acta Chromatographica

2021

Vol. 33, no. 1

64--72

The aim of the experiment is to establish a method for the determination of acrylamide in food by automatic accelerated solvent extraction-gas chromatography-mass spectrometry. D3-acrylamide was used as isotope internal standard, crushed samples were extracted and purified by automatic accelerated solvent, acrylamide was derivatized into 2,3-dibromopropanamide by potassium bromide and potassium bromate under acidic conditions, and then the derivative was extracted by ethyl acetate and detected by gas chromatography-mass spectrometry. The method had a good linear relationship in the concentration range of 10–2000 ng/mL, and the coefficient of determination (R2) was 0.9997. The detection limit of the method was 3 mg/kg. The quantification limit of the method was 10 mg/kg. The standard addition recovery of acrylamide was between 105 and 120%, and the relative standard deviation of the recovery of acrylamide was less than 3.0%. The experimental result showed that the method was simple, sensitive, efficient and accurate, and could be used for the determination of acrylamide in food.