SAR-OSL dating studies of Romanian, Serbian and Chinese loess using fine and coarse quartz have previously resulted in a series of controversial issues. We extend here the investigations using fine (4–11 μm) and different coarse quartz (>63 μm) grains extracted from aeolianites from a site on Eivissa Island (southwestern Mediterranean). Aeolianites were chosen since they contain quartz from a different geological context and have significantly lower environmental dose rates. The dose response curves of the OSL signals for fine and coarse quartz are similar to those for loess and are also represented by the sum of two saturating exponential functions. For doses up to ~200 Gy, the dose response curves of fine and coarse grains from aeolianites can be superimposed and the ages obtained for the different grain sizes are in agreement up to ~250 ka, increasing our confidence in the accuracy of the ages obtained for samples with such doses, irrespective of the magnitude of the environmental dose rate. Particularly for the fine quartz fraction, a mismatch between the SAR dose response curve and the dose response curve obtained when doses are added to the natural is reported, indicating that the application of the SAR protocol in the high dose range is problematic. This dose dependent deviation is much less pronounced for coarse grains. Thus, it seems reasonable to infer that the dose response curves for the coarse grains, although saturating earlier can be regarded as more reliable for equivalent dose calculation than those for the fine grains.
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Recent developments in our understanding of the limitations of optically stimulated luminescence as a dating tool are presented alongside summaries of results obtained on other luminescence signals measured in sedimentary quartz grains.
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This study investigates lacustrine and fluvial sediments on the Sala Us River in the Mu Us Desert in central north China. Significant changes in environmental dose rate in part of the section could be shown to have occurred from measurements of the present day radioactivity and by the age reversal for some samples that had been dated by optically stimulated luminescence (OSL) measurements on quartz. These changes in dose rate can be attributed to recent uptake of radioactive elements found in the sediments; this resulted in significant underestimation of the OSL ages. In this study, the new isochron method using K-feldspar grains has been applied to overcome the effects of changes in dose rate. Calculations are used to show that changes in the environmental dose rate factors, i.e. K, U, Th, water content and cosmic ray flux, and disequilibrium in the U and Th decay chains, e.g. radon escape, have a negligible effect on the isochron age. After applying the new isochron method, the effects of changes in dose rate caused by recent uptake of radioactive elements and changes in past water content were effectively overcome and true ages are obtained; this was verified by repeating the luminescence isochron measurements on samples of overlying and underlying sediments.
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