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Coordination compounds of Pd(II) and Pt(II) with 3,4,5,6-tetrahydro-2-pyrimidinethiol

Wiśniewski M. Z., Głowiak T., Surga W.J.

Polish Journal of Chemistry

1998

Vol. 72, nr 10

2226-2231

Coordination compounds of Pd(II) and Pt(II) with 3,4,5,6-tetrahydro-2-pyrimidinethiol (THPT) of the general formula M(THPT)4Cl2 H2O, where stands for Pd and Pt, have been obtained and characterized by elemental analysis, X-ray diffraction patterns, derivatography (TG, DTG, DTA), magnetic measurements, and the IR and far-IR spectroscopy. Crystal and molecular structure of the Pd(THPT)4Cl2 H2O have been determined. This compound crystalizes in the monoclinic system with a=8.555(2), b=14.999(3), c=23.324(5) A, beta=91.05(3) degree, V=2832.7(11) A(3) and Z=4; space group P2-1/c. The two compounds have been found to be isostuctural.