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Hydrothermal Synthesis and Structures of Two Isostructural Mixed Complexes of Cd and Mn with 2,3-Dicarboxylatopyrazine and Phenanthroline

Zhang M. -S., Sun B. -W., Fang R. -B., Zhao Q. -H.

Polish Journal of Chemistry

2009

Vol. 83, nr 10

1701-1706

Two polyaromatic acid transition metal complexes: {[Cd(phen)(O2C)2C4N2H2]źH2O}n (1), and {[Mn(phen)(O2C)2C4N2H2]źH2O}n (2) (phen = 1,10-phenanthroline) have been hydrothermally synthesized and characterized by elemental analyses, IR spectroscopy, and single-crystal X-ray diffraction. The structural analysis reveals that compound 1 and compound 2 are almost isostructural. The metal atoms are linked by bridging 2,3-di -carboxylatopyrazine ligands to form 2-D layer network, and have a coordination number six.