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Graphene based porous coatings with antibacterial and antithrombogenous function - Materials and design

Major R., Sanak M., Mzyk A., Lipinska L., Kot M., Lacki P., Bruckert F., Major B.

Archives of Civil and Mechanical Engineering

2014

Vol. 14, no. 4

540--549

The studies considered graphene-based biomaterials dedicated for cardiovascular therapy. Reduced graphene oxide flakes were introduced into the porous structure of the polyelectrolyte based coatings. TEM analysis showed the presence of graphene flakes arranged parallel to the substrate surface, firmly connected to the porous coating. Biomaterials were subjected to a comprehensive diagnosis of the biological and material properties. The material behavior was simulated using finite element method. The coatings were deposited using layer by layer method. Mechanical analysis was done using Berkovich indenter geometry. They confirmed theoretical FEA based calculations, it was observed the coating stiffness incensement under the influence of introduced particles of graphene. The endanger of the bacteriology film formation was verified based on the E-coli and Staphylo coccus bacteria. Blood–material interaction was examined in the dynamic flow conditions. Bacteriological analysis showed reduced presence of bacteria after contact with the surface with introduced graphene flakes. Dynamic analyzes on blood showed high activation of the coagulation, strong platelets consumption and a strong immune response. It is caused by sharp edge of the single plane of the graphene flake.

The sensitivity of sensor structures with oxide graphene exposed to selected gaseous atmospheres

Pustelny T., Drewniak S., Setkiewicz M., Maciak E., Urbańczyk M., Procek M., Gut K., Opilski Z., Jagiello J., Lipinska L.

Bulletin of the Polish Academy of Sciences. Technical Sciences

2013

Vol. 61, nr 3

705--710

The paper presents the results of investigations on the resistive structure with a graphene oxide (GO) sensing layer. The effects of dangerous gases (hydrogen and nitrogen dioxide) on the structure were studied; the resistance changes were examined during the flow of the selected gas in the atmosphere of synthetic air. Measurements were performed with a special emphasis on the detection of low concentrations of the analyzed gases. The reactions of the sensing structure to the effect of nitrogen and synthetic air at different humidity were also tested. Much attention was also paid to the fast response of the sensor to the changes in the gas atmosphere. The thin palladium layer (~2 nm) has been applied in order to improve the sensing properties of the structure. The investigations were performed in the temperature range from RT to 120°C and the analyzed gases in synthetic air were batched alternately with pure synthetic air.