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Wpływ stopowania laserowego z użyciem nanorurek węglowych stopu Ti13Nb13Zr do zastosowań biomedycznych na jego wybrane własności mechaniczne

Rogala-Wielgus D., Majkowska-Marzec B., Bartmański M.

Przegląd Spawalnictwa

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2018

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R. 90, nr 7

18--23

PL

Do eksperymentu użyto stopu tytanu Ti13Nb13Zr, który ze względu na swój skład chemiczny i właściwości mechaniczne stanowi materiał do zastosowań w inżynierii medycznej. Celem pracy była ocena wpływu stopowania laserowego stopu Ti13Nb13Zr z powłoką z wielościennych nanorurek węglowych na jego właściwości mechaniczne (chropowatość, nanotwardość, moduł Younga). Do wytworzenia powłoki węglowej wykorzystano metodę osadzania elektroforetycznego (EDP). Modyfikację laserową przeprowadzono przy użyciu impulsowego lasera Nd:YAG. Zastosowano moc impulsu 800 W i czas impulsu 0,5 ms oraz 1 ms. Właściwości mechaniczne zmierzono za pomocą nanoindentera, zaś chropowatość z użyciem mikroskopu sił atomowych (AFM). Zastosowanie powłoki z wielościennych nanorurek węglowych do stopowania laserowego stopu Ti13Nb13Zr oraz odpowiedni dobór parametrów procesu pozwoliły na podwyższenie właściwości mechanicznych (nanotwardość wzrosła ponad dwukrotnie) w stosunku do własności materiału rodzimego, nastąpiło również ujednolicenie właściwości w obrębie badanej powierzchni.

EN

The titanium alloy Ti13Nb13Zr was used as a substrate, because of its chemical composition and good mechanical properties in application of tissue engineering. The aim of the wark was the assessment of the influence of laser alloying of Ti13Nb13Zr coated with multi-walled carbon nanotubes for mechanical properties (roughness, nanohardness, Young modulus). Electrophoretic deposition (EOP) method was used to prepare carbon coating. Laser modification was carried out with Nd:YAG laser in pulsed mode operating system. The power of the impulse was 800 Wand the time 0,5 ms and 1 ms. Mechanical properties were checked with nanoindenter and roughness of the surface with Atomic Force Microscope (AFM). The improvement of mechanical properties (the nanohardness increases more than twice) and its homogeneity within tested area (in the comparisan to the native material) was seen after implementation of carbon nanotube coating with appropriate parameters of the process.

2

The properties of nanosilver – doped nanohydroxyapatite coating

Bartmański M.

Engineering of Biomaterials

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2018

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Vol. 21, no. 148

74

3

Potential degradation of bone cement used in maxillo-facial surgery

Wekwejt M., Świeczko-Żurek B., Bartmański M.

Engineering of Biomaterials

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2017

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Vol. 20, no. 143 spec. iss.

31

4

The determinants of morphology and properties of the nanohydroxyapatite coating deposited on the Ti13Zr13Nb alloy by electrophoretic technique

Bartmański M., Berk A., Wójcik A.

Advances in Materials Science

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2016

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Vol. 16, nr 3(49)

56--66

EN

The titanium and its alloys belong at present to the most preferred and commonly applied biomaterials for load-bearing implants. The surfaces of biomaterials are subjected to modification, including the hydroxyapatite coatings deposited in order to ensure corrosion resistance and better joining between an implant and a bone through the possibility of ingrowth bone into the coating. In this paper, the morphology and properties of the nanohydroxyapatite coating deposited on the Ti13Zr13Nb flat surfaces using electrophoretic method are presented. Electrophoretic deposition at two different current values and two electrolytes (first – ethanol with nanoHAp, second – methanol with nanoHAp) was applied. The scanning electron microscopy examinations and wettability angle measurements showed an increase in the coating thickness, the surface coverage and decrease in biocompatibility with increasing voltage. The surface condition and biocompatibility of coatings were better when using methanol/nanoHAp solution as compared to the ethanol/nanoHAp one.

5

Investigations of titanium implants covered with hydroxyapatite layer

Świeczko-Żurek B., Bartmański M.

Advances in Materials Science

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2016

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Vol. 16, nr 2(48)

78--86

EN

To reduce unfavorable phenomena occurring after introducing an implant into human body various modifications of the surface are suggested. Such modifications may have significant impact on biocompatibility of metallic materials. The titanium and it's alloys are commonly used for joint and dental implants due to their high endurance, low plasticity modulus, good corrosion resistance as well as biocompatibility. Special attention should be given to titanium alloys containing zirconium, tantalum and niobium elements. These new generation alloys are used by worldwide engineering specialists. The experiments were performed with hydroxyapatite layer on titanium specimens with the use of electrophoresis method (different voltage and time).

6

Project of hip joint endoprosthesis for an individual patient with materials selection

Bartmański M., Świeczko-Żurek B.

Advances in Materials Science

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2015

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Vol. 15, nr 1(43)

30--36

EN

Nowadays the joint replacement orthopaedic surgery is most frequently performed surgery associated with the damage of the join surface. The implantation is mainly placed in hip and knee area. This work includes the hip replacement design, based on the patient's medical records, the description of creation process and materials used for individual components.

7

Energetyka morska - nowy dział gospodarki

Gutkowski B., Bartmański M., Skalska K.

Czysta Energia

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2008

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Nr 5

24-25

8

Szanse rozwoju energetyki wiatrowej na przybrzeżnych wodach Bałtyku

Bartmański M., Gutkowski B.

Czysta Energia

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2007

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Nr 11

60-61